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NASA NTRS1981

Double layers and electrostatic shocks

It is shown that it is useful to define double layers and shocks so that the ion phase spaces of double layers are the mirror image (about zero ion velocity) of the ion phase spaces for laminar electrostatic shocks. The distinguishing feature is the direction of the free ion velocity. It is also shown that double layers can exist without the presence of trapped ions. The Bohm condition for double layers, that the ion drift velocity on the high potential side must be greater than the ion sound velocity, is shown to be related to a requirement of a lower limit on the Mach number of laminar electrostatic shocks

Hershkowitz, N.↗

NASA NTRS1983

Particle simulations of electrostatic emissions near the lower hybrid frequency

The linear instability and nonlinear saturation of electrostatic emission near the lower hybrid frequency is examined for model cold and warm ion ring distributions and auroral zone parameters. In the cold ring case, a single coherent mode near omega (LH) evolves, and saturates by ion trapping. In the warm ring case, a discrete spectrum of unstable modes separated by the ion gyrofrequency is generated near and above omega (LH). The latter instability saturates by quasilinear diffusion.

Roth, I.↗

NASA NTRS1982

Generation of X-rays and neutrons with a RF-discharge

An experimental study concerning disk shaped plasma structures was performed. Such disk-shaped structures can be obtained using an rf discharge in hydrogen. The applied frequency was 1-2 Mhz. In case of operation in deuterium it was found that the discharge emits neutrons and X-rays, although the applied voltage is only 2 kV. This phenomenon was explained by assuming formation of plasma cavitons which are surrounded by high electric fields. The condition for formation of these cavitons is that the applied rf frequency is equal to the plasma frequency. The ions trapped in these resonance structures acquire sufficient energy that they can undergo fusion reactions with the ions in the surrounding gas.

Schneider, R. T.↗

DOE OSTI2025

High-precision mass measurement of 103 Sn restores smoothness of the mass surface

As a step towards the ultimate goal of a high-precision mass measurement of doubly magic 100 Sn, the mass of 103 Sn was measured at the Low Energy Beam and Ion Trap (LEBIT) located at the Facility for Rare Isotope Beams (FRIB). Utilizing the time-of-flight ion cyclotron resonance technique, a mass uncertainty of 3.7 keV was achieved, an improvement by more than an order of magnitude compared to a recent measurement performed in 2023 at the Cooler Storage Ring (CSRe) in Lanzhou. Although the LEBIT and CSRe mass measurements of 103 Sn are in agreement, they diverge from the experimental mass value reported in the 2016 version of the Atomic Mass Evaluation (AME2016), which was derived from the measured 𝑄 𝛽 + value and the mass of 103 In. In AME2020, this indirectly measured 103 Sn mass was classified as a “seriously irregular mass” and replaced with an extrapolated value, which aligns with the most recent measured values from CSRe and LEBIT. As such, the smoothness of the mass surface is confidently reestablished for 103 Sn. Here, LEBIT's mass measurement of 103 Sn enabled a significant reduction in the mass uncertainties of five parent isotopes which are now dominated by uncertainties in their respective 𝑄 values.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2023

Examining Interactions of Uranyl(VI) Ions with Amino Acids in the Gas Phase

Gas-phase experiments, using electrospray ionization quadrupole ion trap mass spectrometry (ESI-QIT/MS), were conducted to probe basic interactions of the uranyl(VI) ion, UO 2 2+ , with selected natural amino acids, namely, L-cysteine (Cys), L-histidine (His), and L-aspartic acid (Asp), which strongly bind to metal ions. The simplest amino acid, glycine (Gly), was also studied for comparison. Cys, His, and Asp have additional potentially coordinating groups beyond the amino and carboxylic acid functional groups, specifically thiol in Cys, imidazole in His, and a second carboxylate in Asp. Gas-phase experiments comprised collision-induced dissociation (CID) of uranyl–amino acid complexes and competitive CID to assess the relative binding strength of different amino acids in the same uranyl complex. Reactivity of selected uranyl–amino acid complexes with water provided further insights into relative stabilities. In positive ion mode, CID and ensuing reactions with water suggested that uranyl–neutral AA binding strength decreased in the order His > Asp > Cys > Gly, which is similar to amino acid proton affinities. In negative ion mode, CID revealed a decreasing dissociation tendency in the order Gly >> His ≈ Cys > Asp, presumably reflecting a reverse enhanced binding to uranyl of the doubly deprotonated amino acids formed in CID.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

NASA NTRS1992

Summary of ionizing radiation analysis on the Long Duration Exposure Facility

The ionizing radiation measurements flown on the Long Duration Exposure Facility (LDEF) were contained in 15 experiments which utilized passive detectors to pursue objectives in astrophysics and to measure the radiation environment and dosimetric quantities. The spacecraft structure became sufficiently radioactive to permit additional important studies. The induced activity allows extensive radiation mapping in the structure, and independent comparison with experiment dosimetric techniques, and significant studies of secondary effects. The long exposure time, attitude stability, and number and types of measurements produced a unique and critical set of data for low Earth orbit that will not be duplicated for more than a decade. The data allow an unprecedented test, and improvement if required, of models of the radiation environment and the radiation transport methods that are used to calculate the internal radiation and its effects in spacecraft. Results of measurements in the experiments, as well as from radioactivity in the structure, have clearly shown effects from the directional properties of the radiation environment, and progress was made in the dosimetric mapping of LDEF. These measurements have already influenced some Space Station Freedom design requirements. Preliminary results from experiments, reported at this symposium and in earlier papers, show that the 5.8 years exposure considerably enhanced the scientific return of the radiation measurements. The early results give confidence that the experiments will make significant advances in the knowledge of ultra heavy cosmic rays, anomalous cosmic rays, and heavy ions trapped in the radiation belts. Unexpected phenomena were observed, which require explanation. These include stopping iron group ions between the energy ranges anticipated for anomalous and galactic cosmic rays in the LDEF orbit. A surprising concentration of the Be-7 nuclide was discovered on the 'front' surface of LDEF, apparently transported up from the stratosphere with exceptional efficiency.

Parnell, T. A.↗

NASA NTRS1990

A study of the influence of Hg(6(3)P2) population in a low-pressure discharge on mercury ion emission at 194.2 nm

A low-pressure mercury-argon discharge, similar to the type existing in the mercury lamp for the trapped-ion standard, is probed with a new technique of laser spectroscopy to determine the influence of the Hg(6 3P(sub 2)) population on discharge emission. The discharge is excited with inductively coupled rf power. Variations in the intensity of emission lines in the discharge were examined as lambda = 546.1 nm light from a continuous wave (CW) laser excited the Hg(6 3P(sub 2)) to (7 3S (sub 1)) transition. The spectrum of the discharge viewed in the region of laser irradiation showed increased emission in lambda = 546.1, 435.8, 404.7, 253.7, and 194.2 nm lines. Other lines in Hg I exhibited a decrease in emission. When the discharge was viewed outside the region of laser irradiation, all lines exhibited an increased emission. Based on these results, it is concluded that the dominant mechanism for the excitation of higher lying levels of mercury is the the electron-impact excitation via the 3P(sub 2) level. The depopulation of this metastable is also responsible for the observed increase in the electron temperature when the laser irradiates the discharge. It is also concluded that the 3P(sub 2) metastable level of mercury does not play a significant role in the excitation of the 3P(sub 1/2) level of mercury ion.

Maleki, L.↗

NASA NTRS1975

Plasma wave interactions with energetic ions near the magnetic equator

An intense band of electromagnetic noise is frequently observed near the magnetic equatorial plane at radial distance from about 2 to 5 Re. Recent wideband wave-form measurements with the IMP-6 and Hawkeye-1 satellites have shown that the equatorial noise consists of a complex superposition of many harmonically spaced lines. Several distinctly different frequency spacings are often evident in the same spectrum. The frequency spacing typically ranges from a few Hz to a few tens of Hz. It is suggested that these waves are interacting with energetic protons, alpha particles, and other heavy ions trapped near the magnetic equator. The possible role these waves play in controlling the distribution of the energetic ions is considered.

Gurnett, D. A.↗

DOE OSTI2025

First simultaneous observation of co- and counter-current fast-ion losses in the ASDEX Upgrade tokamak

In ITER and future fusion power plants, the source of the fusion born alpha particles is almost isotropic in pitch angle, thus having co- and counter-current populations. For trapped ions, the co-current side of the orbit corresponds to its outer leg, while the counter-current side corresponds to the inner leg. Understanding the mechanisms responsible for the fast-ion losses (FILs) is critical for future magnetically confined fusion power plants. To further study the interplay of fast ions with plasma instabilities, a double pinhole collimator has been developed for a Fast-Ion Loss Detector (FILD) in the ASDEX Upgrade tokamak (AUG). This new FILD opens the operational window to simultaneous measurements of the co- and counter-current ion velocity-space. In this paper, the first results for the AUG double collimator FILD detector are shown. The commissioning of this new probe is carried out in H-mode plasmas with an on-axis magnetic field $B_0 = -2.5$ T, and a plasma current $I_{\textrm{p}} = 0.7$ MA. Simultaneous co- and counter-current FILs have been measured. Both have shown a similar dependence on Ion Cyclotron Resonance Heating (ICRH) power, where the main difference is the intensity of the losses, with the co-losses being an order of magnitude larger. Toroidal Alfvén eigenmode-coherent ICRH-only losses have been identified for the co-current ions. Additionally, the presence of Edge Localized Modes during the discharge were shown to increment Neutral Beam Injection prompt losses, while partially mitigating ICRH-driven losses on both co- and counter- sides of the velocity-space. Finally, a very trapped and high gyroradius losses, with an unclear origin, have been measured in the co- and counter-current velocity-space. The computed ion trajectories show that these ions remain permanently near the vessel wall, suggesting that they are accelerated within the scrape-off layer.

ELM↗

DOE OSTI2023

Microstructure and defect engineering of graphite anodes by pulsed laser annealing for enhanced performance of lithium-ion batteries

We report nanosecond pulsed laser annealing significantly improves cyclability and current carrying capacity of lithium-ion batteries (LIBs). This improvement is achieved by engineering of microstructure and defect contents present in graphite in a controlled way by using pulsed laser annealing (PLA) to increase the number density of Li + ion trapping sites. The PLA treatment causes the following changes: (1) creates surface steps and grooves between the grains to improve Li + ion charging and intercalation rates; (2) removes inactive polyvinylidene difluoride (PVDF) binder from the top of graphite grains and between the grains which otherwise tends to block the Li + migration; and (3) produces carbon vacancies in (0001) planes which can provide Li + charging sites. From X-ray diffraction data, we find upshift in diffraction peak or reduction in planar spacing, from which vacancy concentration was estimated to be about 1.0%, which is higher than the thermodynamic equilibrium concentration of vacancies. The laser treatment creates single and multiple C vacancies which provide sites for Li + ions, and it also produces steps and grooves for Li + ions to enter the intercalating sites. It is envisaged that the formation of these sites enhances Li+ ion absorption during charge and discharge cycles. The current capacity increases from an average 360 mAh/g to 430 mAh/g, and C–V shows significant reduction in SEI layer formation after the laser treatment. If the vacancy concentration is too high and charge-discharge cycles are long, then trapping of electrons by Li + may occur, which can lead to Li 0 formation and Li plating causing reduction in current capacity.

25 ENERGY STORAGE↗

NASA NTRS1976

Plasma wave interactions with energetic ions near the magnetic equator

An intense band of electromagnetic noise is frequently observed near the magnetic equatorial plane at radial distance from about 2 to 9 earth radii. Recent wide band wave form measurements with the Imp 6 and Hawkeye 1 satellites have shown that the equatorial noise consists of a complex superposition of many harmonically spaced lines. Several distinctly different frequency spacings are often evident in the same spectrum. The frequency spacing typically ranges from a few hertz to a few tens of hertz. The purpose of this paper is to suggest that these waves are interacting with energetic protons, alpha particles, and other heavy ions trapped near the magnetic equator. The possible role that these waves play in controlling the distribution of the energetic ions is considered.

Gurnett, D. A.↗

NASA NTRS1990

Inhomogeneous electric field effects in a linear RF quadruple trap

The exact potential corresponding to confining fields inside a linear rf quadrupole particle trap of finite length is presented. The analytic expressions for the trapping potential is derived by introducing a linear trap employing a relatively simple cylindrical geometry and solving Laplace's equation for the trap electrodes. The finite length of linear traps results in field distortion near the trap ends. An exact analytic determination of the fields is useful because the profile of the trapped ion cloud is highly dependent on the fields confining it. It is shown that near the ends of the trap, the effective potential arising from the rf fields acts to propel particles out of the trap, and further, that the addition of a dc bias generates an inhomogeneous in the trap that influences the particles both perpendicularly to and along the trap's long axis.

Melborne, R. K.↗

NASA NTRS2005

Overview of Results from the Cassini Magnetospheric Imaging Instrument (MIMI) During the First Year of Operations

The MIMI investigation comprises three sensors covering the indicated energy ranges: the Ion and Neutral Camera (INCA) -- 7 keV/nuc 3 Mev) and protons (1.6 < E < 160 Mev) from the back end of the dual field-of-view telescope. The Saturn observation sequences began in January, 2004 and culminated in Saturn Orbit Insertion on July 1, 2004. The MIMI sensors observed substantial activity in interplanetary space for several months prior to SOI, including several interplanetary shocks associated with corotating interaction regions, numerous increases most likely originating from particle streams in the vicinity of the Saturnian bow shock and energetic neutral atoms (ENA) emanating from Saturn s magnetosphere. Results following SOI revealed: a dynamical magnetosphere with a day-night asymmetry and an 11-hour periodicity; several water-product ions (O+, OH+, H2O+), but little N+; inferred quantities of neutral gas sufficient to cause major losses in the trapped ions and electrons in the middle and inner magnetosphere; a Titan exosphere that is a copious source of ENA; INCA imaging through ENA has also revealed a previously unknown radiation belt residing inward of the D-ring that is most likely the result of double charge-exchange between the main radiation belt and the upper layers of Saturn s exosphere. Finally, there is ample evidence for the presence of substorm-like injections of plasma that subsequently corotates for a number of days before dissipating on the night-side magnetotail. The observations will be presented and discussed in the context of current theoretical models.

Krimigis, S. M.↗

NASA NTRS1991

Determining the solar-flare photospheric scale height from SMM gamma-ray measurements

A connected series of Monte Carlo programs was developed to make systematic calculations of the energy, temporal and angular dependences of the gamma-ray line and neutron emission resulting from such accelerated ion interactions. Comparing the results of these calculations with the Solar Maximum Mission/Gamma Ray Spectrometer (SMM/GRS) measurements of gamma-ray line and neutron fluxes, the total number and energy spectrum of the flare-accelerated ions trapped on magnetic loops at the Sun were determined and the angular distribution, pitch angle scattering, and mirroring of the ions on loop fields were constrained. Comparing the calculations with measurements of the time dependence of the neutron capture line emission, a determination of the He-3/H ratio in the photosphere was also made. The diagnostic capabilities of the SMM/GRS measurements were extended by developing a new technique to directly determine the effective photospheric scale height in solar flares from the neutron capture gamma-ray line measurements, and critically test current atmospheric models in the flare region.

Lingenfelter, Richard E.↗

DOE OSTI2021

Method and apparatus for ion mobility separations utilizing alternating current waveforms

Methods and apparatuses for ion manipulations, including ion trapping, transfer, and mobility separations, using traveling waves (TW) formed by continuous alternating current (AC) are disclosed. An apparatus for ion manipulation includes a surface to which are coupled a first plurality of continuous electrodes and a second plurality of segmented electrodes. The second plurality of segmented electrodes is arranged in longitudinal sets between or adjacent to the first plurality of electrodes. An RF voltage applied to adjacent electrodes of the first plurality of electrodes is phase shifted by approximately 180° to confine ions within the apparatus. An AC voltage waveform applied to adjacent electrodes within a longitudinal set of the second plurality of segmented electrodes is phase shifted on the adjacent electrodes by 1°-359° to move ions longitudinally through the apparatus for separation.

Garimella, Venkata B. S.↗

DOE OSTI2023

Method and apparatus for ion mobility separations utilizing alternating current waveforms

Garimella, Venkata B. S.↗

NASA NTRS1965

Evidence for temperature stratification in the e region.

Ion kinetic temperature measured in E region by ion trap aboard Nike-Apache rocket

TEMPERATURE PROFILE↗

NASA NTRS1990

Collisional electrostatic ion cyclotron waves as a possible source of energetic heavy ions in the magnetosphere

A new mechanism is proposed for the source of energetic heavy ions (NO/+/, O2/+/, and O/+/) found in the magnetosphere. Simulations using a multispecies particle simulation code for resistive current-driven electrostatic ion cyclotron waves show transverse and parallel bulk heating of bottomside ionospheric heavy ion populations. The dominant mechanism for the transverse bulk heating is resonant ion heating by wave-particle ion trapping. Using a linear kinetic dispersion relation for a magnetized, collisional, homogenous, and multiion plasma, it is found that collisional electrostatic ion cyclotron waves near the NO(+), O2(+), and O(+) gyrofrequencies are unstable to field-aligned currents of 50 microA/sq m for a typical bottomside ionosphere.

Providakes, Jason↗