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DOE OSTI2025

Peak‐in‐Valley Metal Nano‐Architectures via E‐Beam‐Guided Metal Oxide Redox

Focused electron beams enable nanoscale material modification via localized etching or deposition. In liquid-phase electron-beam-mediated processing, radiolysis-driven redox reactions present an opportunity to control both etching and deposition simultaneously. Here, this duality using a water-ammonia solvent as a tunable redox mediator on copper surfaces is demonstrated. At lower ammonia concentrations, the oxidation process dominates, etching copper to sub-50-nm depths. The copper ions and ion-complexes released during this initial oxidation step are reduced by solvated electrons resulting in metal deposition into the etched sites, over longer e-beam exposures, producing characteristic peak-in-valley nanostructures. Conversely, at higher ammonia concentrations copper-ammine ion complexation and radiolytic oxidizing species scavenging by ammonia occur at higher rates, creating a reducing environment conducive to rapid beam-guided copper deposition. Reaction-transport simulations and experiments are performed to show the effects of ammonia-mediated radiolysis chemistry, describing the direct influence of solvent concentration on redox balance and the outcome of e-beam guided processing. By uniting both etching and deposition within a single framework, this work provides a versatile route for controlled surface nanostructuring.

copper nanostructures↗

DOE OSTI2023

Modernizing Fermilab s Control Hardware

Modernizing the Fermilab accelerator control system is essential to future operations of the laboratory's accelerator complex. The existing control system has evolved over four decades and uses hardware that is no longer available. The Accelerator Controls Operations Research Network (ACORN) Project will modernize the control system and replace end-of-life power supplies to enable future accelerator complex operations with megawatt particle beams. The ACORN project is planning to replace Fermilab’s obsolete CAMAC crate-and-card controls hardware with modern MicroTCA hardware. There are over 2,000 CAMAC cards and over 250 CAMAC crates serving various functions in Fermilab’s control system. We will present an overview of the existing CAMAC hardware and the proposed MicroTCA replacement plan.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2024

Modernizing Fermilab's Accelerator Control Hardware

Modernizing the Fermilab accelerator control system is essential to future operations of the laboratory's accelerator complex. The existing control system has evolved over four decades and uses hardware that is no longer available.The Accelerator Controls Operations Research Network (ACORN) Project will modernize the control system and replace end-of-life power supplies to enable future accelerator complex operations with megawatt particle beams. The ACORN project is planning to replace Fermilab s obsolete CAMAC crate-and-card controls hardware with modern MicroTCA hardware. There are over 2,000 CAMAC cards and over 250 CAMAC crates serving various functions in Fermilab s control system. We will review the existing CAMAC hardware and provide updates on the status of the ACORN project, which includes the conceptual design of the MicroTCA replacement hardware and software tools for supporting the installation of hundreds of MicroTCA crates.

43 PARTICLE ACCELERATORS↗

DOE OSTI2020

Variable voltage electron microscopy: Toward atom-by-atom fabrication in 2D materials

The precisely focused electron beam (e-beam) in scanning transmission electron microscopy has been found to be a versatile tool for patterning matter on the atomic level and enabling atom-by-atom fabrication, however, beam-induced phenomena are known to be extremely sensitive to the e-beam energy and are closely correlated with the proximity of the knock-on threshold. Here we provide a method to control the energy transferred to the sample while facilitating much faster changes in accelerating voltages by maintaining a nearly constant temperature in the electron microscope lenses. We use this method to demonstrate in-situ nano-milling of a graphene film followed rapidly by “gentler” imaging at lower energy. Additionally, the insertion and controlled movement of silicon dopants in graphene is demonstrated by employing a different e-beam energy during each process. We believe the incorporation of variable e-beam energy will broaden the potential for atomic scale e-beam fabrication.

36 MATERIALS SCIENCE↗

DOE OSTI2022

Control of internal transport barriers in magnetically confined tokamak burning plasmas

The initiation, termination, and control of internal transport barriers associated with E × B flow shear near local minima of magnetic shear are examined for burning plasmas to determine if the positive feedback loops between profiles, instability, transport, and flow shear operate in regimes with fusion self-heating. A five-field transport model for the evolution of profiles of density, ion and electron temperature, ion and electron fluctuations, and radial electric field is utilized to examine the efficacy of controls associated with external inputs of heat and particles, including neutral beam injection, RF, pellets, and gas puffing. The response of the plasma to these inputs is studied in the presence of self-heating. The latter is affected by the external inputs and their modification of profiles and is, therefore, not an external control. Provided sufficient external power is applied, internal transport barriers can be created and controlled, both in ion and electron channels. Barrier control is sensitive to the locations of power deposition and pellet ablation, as well as temporal sequencing of external inputs.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2020

Optimal Control for X-Ray Mircroscopes

In this article, a systematic framework for designing the control for fine positioning (scanning) stages of X-ray microscopes is presented. This framework facilitates designs that simultaneously achieve specifications on positioning resolution and tracking bandwidth while guaranteeing robustness of the closed loop device to unmodeled uncertainties. We use robust optimal control techniques for modeling, quantifying design objectives and system-specific challenges, and designing the control laws. The control designs were implemented on a three degree of freedom piezoactuated flexure stages dedicated for fine positioning of X-ray optics. Experimental results demonstrate significant improvements in positioning performance of 134%, 150%, and 132% in tracking bandwidths along the lateral (X), vertical (Y), and beam (Z) directions, respectively, when compared to proportional-integral-derivative controller designs. This was achieved while keeping similar or better positioning resolution and robustness measures. Fast scanning for X-ray imaging was demonstrated in both the step scan and flyscan modes, where bandwidth was improved by over 450 times with flyscan compared to the step scan.

42 ENGINEERING↗

DOE OSTI2023

Proton and electron RLA optics design

We describe optics designs of the key components of proton and electron Recirculating Linear Accelerators (RLAs). They are presented in the context of a high-power hadron accelerator being considered at ORNL and a CEBAF electron energy doubling study, FFA@CEBAF, being developed at Jefferson Lab. Both concepts rely on the Fixed-Field Alternating gradient (FFA) arc optics designs where multiple beam passes are transported by a single beam line. Some of the main challenges of the optics design are in synchronization and orbital and linear optics match of the individual passes with the linac straight. To minimize the complexity of the matching sections and make them more practical, it is preferable to complete as much of the orbital and optical match as possible within a single beam line using the FFA approach. The adiabatic matching technique proposed earlier is one such solution, but it requires a large number of cells. We present a much shorter matching section design based on another approach. A compact dog-leg-type section of several bending dipoles and quadrupoles is used to suppress the orbital offset and dispersion coming out of a periodic cell. Additional quadrupoles are used in the section to keep the beta functions under control and simplify their subsequent match to the linac. Initial beam tracking results are presented.

Benesch, J.↗

DOE OSTI2025

Quantitative Electron Beam‐Single Atom Interactions Enabled by Sub‐20‐pm Precision Targeting

The ability to probe and control matter at the picometer scale is essential for advancing quantum and energy technologies. Scanning transmission electron microscopy offers powerful capabilities for materials analysis and modification, but sample damage, drift, and scan distortions hinder single atom analysis and deterministic manipulation. Materials analysis and modification via electron–solid interactions can be transformed by precise delivery of electrons to a specified atomic location, maintaining the beam position despite drift, and minimizing collateral dose. Here a fast, low-dose, sub-20-pm precision electron beam positioning technique is developed, “atomic lock-on,” (ALO), which offers the ability to position the beam on a specific atomic column without previously irradiating that column. This technique is used to lock onto a single selected atomic location to repeatedly measure its weak electron energy loss signal despite sample drift. Moreover, electron beam-matter interactions in single atomic events are measured with μ s time resolution. This enables observation of single-atom dynamics, such as atomic bistability, revealing partially bonded atomic configurations and recapture phenomena. This opens prospects for using electron microscopy for high-precision measurements and deterministic control of matter for quantum technologies.

2D materials↗

DOE OSTI2023

Dense nuclear matter equation of state from heavy-ion collisions

The nuclear equation of state (EOS) is at the center of numerous theoretical and experimental efforts in nuclear physics. With advances in microscopic theories for nuclear interactions, the availability of experiments probing nuclear matter under conditions not reached before, endeavors to develop sophisticated and reliable transport simulations to interpret these experiments, and the advent of multi-messenger astronomy, the next decade will bring new opportunities for determining the nuclear matter EOS, elucidating its dependence on density, temperature, and isospin asymmetry. Among controlled terrestrial experiments, collisions of heavy nuclei at intermediate beam energies (from a few tens of MeV/nucleon to about 25 GeV/nucleon in the fixed-target frame) probe the widest ranges of baryon density and temperature, enabling studies of nuclear matter from a few tenths to about 5 times the nuclear saturation density and for temperatures from a few to well above a hundred MeV, respectively. Collisions of neutron-rich isotopes further bring the opportunity to probe effects due to the isospin asymmetry. However, capitalizing on the enormous scientific effort aimed at uncovering the dense nuclear matter EOS, both at RHIC and at FRIB as well as at other international facilities, depends on the continued development of state-of-the-art hadronic transport simulations. Furthermore, this white paper highlights the essential role that heavy-ion collision experiments and hadronic transport simulations play in understanding strong interactions in dense nuclear matter, with an emphasis on how these efforts can be used together with microscopic approaches and neutron star studies to uncover the nuclear EOS.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2022

Enzymatic X-ray absorption spectroelectrochemistry

X-ray absorption spectroelectrochemistry has the potential to provide insight into enzyme mechanisms. However, protein loading on the electrode surface must be optimized and controls in place to differentiate electrochemically driven changes from beam induced damage.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2023

Measurements of the L-shell X-ray emission of fluorine-like europium

Measurements of the L-shell X-ray emission of fluorine-like europium ions (Eu 54+ ) were made under controlled laboratory conditions on the EBIT-I electron beam ion trap at Livermore using an X-ray calorimeter, extending such measurements to the middle of the rare earth elements. Comparing the calorimeter spectra with atomic data from the flexible atomic code, we have identified and analyzed several prominent n = 3 → n = 2 transitions, including one two-electron, one-photon core changing transition and one electric quadrupole transition. We find that the measured energies are typically up to several eV higher than predicted.

74 ATOMIC AND MOLECULAR PHYSICS↗

DOE OSTI2025

High-speed fiber-coupled terahertz time-domain spectroscopy system using a bias-free plasmonic source

We demonstrate a high-speed fiber-coupled terahertz time-domain spectroscopy (THz-TDS) system using a bias-free plasmonic terahertz source. The system is powered by a compact, low-power femtosecond fiber laser oscillator that drives a dual-branch fiber amplifier to pump and probe a plasmonic terahertz source and detector, respectively. A polarization-maintaining, fiber-coupled optical delay line is employed to precisely control the temporal offset between the pump and probe beams through a compact, robust platform. Operating in the self-similar amplification regime, the fiber amplifiers are engineered to mitigate nonlinear pulse distortion and dispersion while delivering robust, high-energy pulses at a 1560-nm wavelength, with an output power exceeding 326 mW. In reflection mode, the THz-TDS system achieves a peak dynamic range of 81 dB and a bandwidth greater than 3.5 THz at a scan rate of 3.75 Hz. The utility of the system for rapid sensing is further demonstrated by quantifying the porosity and density of pharmaceutical tablets through measurements of their physical thickness and effective refractive index.

Jiang, Xinghe [University of California, Los Angel↗

DOE OSTI2024

FRIB Beam Power Ramp-up: Status and Plans

After project completion on scope, on cost, and ahead of schedule, the Facility for Rare Isotope Beams began operations for scientific users in May of 2022. The ramp-up to a beam power of 400 kW is planned over a six-year period; 1 kW was delivered for initial user runs from in 2022, and 5 kW was delivered as of February 2023. Test runs with 10 kW 36Ar and 48Ca beams were conducted in July 2023. Upgrade plans include doubling the primary-beam energy to 400 MeV/nucleon for enhanced discovery potential (¿FRIB 400¿). This talk reports on the strategic plans towards high power operations emphasizing challenges and resolutions in beam-interception devices and targetry systems, radiation protection and controls, and legacy system renovation and integration.

43 PARTICLE ACCELERATORS↗

DOE OSTI2021

Observation of Long-Range Wakefield Effects Generated in an Off-Resonance Tesla-Type Cavity

The interest in controlling emittance dilution effects due to off-axis beam transport in accelerator cavities and the resulting dipolar modes is especially important for the facilities with lower emittance beams. The Fermilab Accelerator Science and Technology (FAST) facility has a unique configuration of two single cavities after the photocathode rf gun followed by a cryomodule. The second capture cavity (CC2) was run 15 kHz off resonance and without rf power while a 25-MeV beam was injected into it. The beam centroid effects were tracked by 10 rf button BPMs with bunch-by-bunch position readout capability downstream in a 12-m drift. Possible LRW effects seemed to dominate our previously observed near-resonant HOM effects at mode 14 in this cavity. This mode also shifted in frequency compared to that of the tuned case based on direct measurements. Submacropulse vertical position slewing of 1400 microns at 11 m downstream was observed with a 125 pC/bunch, 50 bunches per macropulse, and 25-MeV beam. The y-position slew amplitudes as a function of z were also measured. Horizontal positions also showed a slew effect. Both are emittance-dilution effects which one wants to mitigate.

Lumpkin, Alex H.↗

DOE OSTI2022

Tunable coherent light filter for optical sensing and imaging

Systems and methods are provided for filtering coherent infrared light from a thermal background for protection of infrared (IR) imaging arrays and detection systems. A Michelson interferometer is used for coherent light filtering. In an implementation, a system includes a fixed mirror, a beam splitter, and a moving mirror which can be controlled translationally, as well as tip/tilt. The Michelson interferometer may be used as an imaging system. For imaging applications, a system may comprise a tunable array of micro-electromechanical systems (MEMS) mirrors. A mid-wave IR interferometer with electronic feedback and MEMS mirror array is provided.

Wasserman, David↗

DOE OSTI2022

A Q-Learning-Based Approach for Distributed Beam Scheduling in mmWave Networks

We consider the problem of distributed downlink beam scheduling and power allocation for millimeter-Wave (mmWave) cellular networks where multiple base stations (BSs) belonging to different service operators share the same unlicensed spectrum with no centralized control or explicit coordination among them. Our goal is to design efficient distributed beam scheduling and power allocation schemes such that the network-level payoff, defined as the weighted sum of the total throughput and a power penalization term, can be maximized. To this end, we propose a distributed scheduling approach to power allocation and adaptation for efficient interference management over the shared spectrum by modeling each BS as an independent Q-learning agent. As a baseline, we compare the proposed approach to the state-of-the-art non-cooperative game-based approach which was previously developed for the same problem. We conduct extensive experiments under various scenarios to verify the effect of multiple factors on the performance of both approaches. Experiment results show that the proposed approach adapts well to different interference conditions by learning from experience and thus can achieve higher payoff than the game-based approach. The proposed approach can also be integrated into our previously developed Lyapunov stochastic optimization framework for the purpose of network utility maximization with optimality guarantee. As a result, the weights in the payoff function can be automatically and optimally determined by the virtual queue values from the sub-problems derived from the Lyapunov optimization framework.

99 GENERAL AND MISCELLANEOUS↗

DOE OSTI2021

Simulations of future particle accelerators: issues and mitigations

The ever increasing demands placed upon machine performance have resulted in the need for more comprehensive particle accelerator modeling. Computer simulations are key to the success of particle accelerators. Many aspects of particle accelerators rely on computer modeling at some point, sometimes requiring complex simulation tools and massively parallel supercomputing. Examples include the modeling of beams at extreme intensities and densities (toward the quantum degeneracy limit), and with ultra-fine control (down to the level of individual particles). In the future, adaptively tuned models might also be relied upon to provide beam measurements beyond the resolution of existing diagnostics. Much time and effort has been put into creating accelerator software tools, some of which are highly successful. However, there are also shortcomings such as the general inability of existing software to be easily modified to meet changing simulation needs. In this paper possible mitigating strategies are discussed for issues faced by the accelerator community as it endeavors to produce better and more comprehensive modeling tools. This includes lack of coordination between code developers, lack of standards to make codes portable and/or reusable, lack of documentation, among others.

43 PARTICLE ACCELERATORS↗

DOE OSTI2022

Verification of a Reduced-Order Extension Spring Model

Adopting reduced order models (ROMs) of springs lowers the computational cost of stronglink simulations. However, ROMs introduce currently unquantified error to such analyses. This study addresses that lack of data by comparing a hexahedral mesh to a commonly used ROM beam mesh. Two types of analyses were performed, a quasi-static displacement-controlled pull and a haversine shock, examining basic spring properties as well as dynamics and stress/strain data. Both tests showed good similarities between the hexahedral and beam meshes, especially when comparing reaction force and stress trends and maximums. Equivalent plastic strain results were not quite as favorable, indicating that the beam model may be less likely to correctly predict spring failure. Despite reducing computation times by over 48 hours in all shock cases, appropriate use of the ROM should carefully balance this advantage with its reduction in accuracy, especially when examining spring failure and outputting variables such as equivalent plastic strain.

42 ENGINEERING↗