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At least 487 records · Page 27

Model 9975 O-Ring Fixture Long-Term Leak Performance (FY2022 Status Report)

Leak testing experiments to monitor the aging performance of Viton® GLT and GLT-S O-rings used in the model 9975 shipping package has been ongoing since 2004 at Savannah River National Laboratory. Seventy tests using mock-up 9975 primary containment vessels (PCVs) with GLT O-rings were assembled and heated to temperatures ranging from 200 to 450 °F. Due to material substitution, fourteen tests with GLT-S O-rings were initiated in 2008 and heated to temperatures ranging from 200 to 400 °F. The conditioning temperatures are elevated compared to the calculated maximum O-ring temperature in a 9975 package in storage, 158 °F, to accelerate aging and enable observations of O-ring failures in a reasonable time frame. The fixtures are leak tested periodically and all GLT O-ring fixtures aging at 350 °F or above have failed to maintain a leak-tight seal. Eight GLT O-ring fixtures aging at 300 °F have failed after 2.8 to 5.7 years at temperature while the remaining fixtures at 300 °F were retired from testing following more than five years without failure. There has been one GLT O-ring fixture which failed after 13.4 years aging at 200 °F. However, 20 other GLT O-rings aging at 200 °F have remained leak-tight for over 14 years and remain in test. No failures have yet been observed in GLT O-ring fixtures aging at 270 °F for 10.4 years. All GLT-S O-ring fixtures aging at 300 °F or above have failed their leak test. No failures have yet been observed in GLT-S O-ring fixtures aging at 250 °F for 12.5 years. This year, one GLT-S O-ring fixture failed after 12.4 years aging at 200 °F. Data from the O-ring fixtures are generally consistent with results from compression stress-relaxation testing, and provide confidence in the predictive models based on those results. However, uncertainty exists in extrapolating these elevated temperature results to the lower temperatures of interest for normal storage in K-Area Complex (KAC). Oxygen consumption testing, which includes results from temperatures near KAC normal storage temperatures, is ongoing to provide further confidence and corroborate these extrapolations. The collective data from these test efforts suggest the minimum O-ring service life at KAC normal storage conditions should be at least 34 years for GLT and GLT-S O-rings. Measurement of compression set in O-rings removed from failed fixtures, compared to that from KAC surveillance O-rings, indicate significant margin remains for O-rings still in service in 9975 packages in KAC. Aging and periodic leak testing will continue for the remaining 25 mock-up PCV fixtures.

36 MATERIALS SCIENCE↗

Model 9975 O-Ring Fixture Long-Term Leak Performance (FY2020 Status Report)

Leak testing experiments to monitor the aging performance of Viton GLT and GLT-S O-rings used in the model 9975 shipping package has been ongoing since 2004 at Savannah River National Laboratory. Seventy tests using mock-up 9975 primary containment vessels (PCVs) with GLT O-rings were assembled and heated to temperatures ranging from 200 to 450 °F. In addition, fourteen tests with GLT-S O-rings were initiated in 2008 and heated to temperatures ranging from 200 to 400 °F. The conditioning temperatures are elevated compared to the calculated maximum O-ring temperature in a 9975 package in storage, 158 °F, to accelerate aging and enable observations of O-ring failures in a reasonable time frame. The fixtures are leak tested periodically and all GLT O-ring fixtures aging at 350 °F or above have failed to maintain a leak-tight seal. Eight GLT O-ring fixtures aging at 300 °F have failed after 2.8 to 5.7 years at temperature while the remaining fixtures at 300 °F were retired from testing following more than five years without failure. No failures have yet been observed in GLT O-ring fixtures aging at 200 °F for 12 to 14 years or aging at 270 °F for 8.5 years. All GLT-S O-ring fixtures aging at 300 °F or above have failed their leak test. No failures have yet been observed in GLT-S O-ring fixtures aging at 200 and 250 °F for 10 to 10.5 years. Data from the O-ring fixtures are generally consistent with results from compression stress-relaxation testing, and provide confidence in the predictive models based on those results. However, uncertainty exists in extrapolating these elevated temperature results to the lower temperatures of interest for normal storage in K-Area Complex (KAC). Oxygen consumption testing, which includes results from temperatures near KAC normal storage temperatures, is ongoing to provide further confidence and corroborate these extrapolations. The collective data from these test efforts suggest the minimum O-ring service life at KAC normal storage conditions should be at least 34 years for GLT and GLT-S O-rings. Measurement of compression set in O-rings removed from failed fixtures, compared to that from KAC surveillance O-rings, indicates margin remains for O-rings still in service. Aging and periodic leak testing will continue for the remaining PCV fixtures.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Controlled-Crack-Growth Testing Of Brittle Materials

Simple design for fixture and specimen significantly improves crack-growth fracture testing of ceramics and other brittle materials. Makes it possible to impose crack-mouth-opening displacement that remains at or close to prescribed value even when crack extends. Important secondary advantages: geometry of specimen is simple, making specimen easy to machine; fit between pin and specimen provides self-aligning grip; contact stresses and probability of failure at or near loading spot reduced.

Calomino, Anthony M.↗

Strain rate characterization of unidirectional graphite/epoxy composite

For an investigation of problems of composites at high strain rates with dominant wave propagation effects, such as dynamically loaded composite jet engine blades, the longitudinal, transverse, and in-plane shear properties of unidirectional SP 288/AS graphite/epoxy were measured at various strain rates ranging from quasi-static to over 500/s. The test specimens were rings 10.16 cm in diameter, 2.54 cm long, 6 to 8 plies thick, and with fibers at 0, 90, and 10 deg off-axis. Quasi-static testing was conducted in a fixture which applies hydraulic pressure to the ring specimens, and dynamic testing was conducted by applying an internal pressure pulse through a liquid in a special fixture. Dynamic stress-strain curves are presented. For the 0-deg specimens, the modulus increases with strain up to 20 percent of the static value. The modulus and strength increase sharply in the 90-deg rings with strain rate reaching values two to three times the corresponding static rate.

Daniel, I. M.↗

Normal-pressure Tests of Circular Plates with Clamped Edges

A fixture is described for making normal-pressure tests of flat plates 5 inches in diameter in which particular care was taken to obtain rigid clamping at the edges. Results are given for 19 plates, ranging in thickness from 0.015 to 0.072 inch. The center deflections and the extreme-fiber stresses at low pressures were found to agree with theoretical values; the center deflections at high pressures were 4 to 12 percent greater than the theoretical values. Empirical curves are derived of the pressure for the beginning of permanent set as a function of the dimensions of the plate and the tensile properties of the material.

CIRCULAR↗

Normal-Pressure Tests of Circular Plates with Clamped Edges

A fixture is described for making normal-pressure tests of flat plates 5 inches in diameter in which particular care was taken to obtain rigid clamping at the edges. Results are given for 19 plates, ranging in thickness form 0.015 to 0.072 inch. The center deflections and the extreme-fiber stresses at low pressures were found to agree with theoretical values; the center deflections at high pressures were 4 to 12 percent greater than the theoretical values. Empirical curves are derived of the pressure for the beginning of the permanent set as a function of the dimensions of the plate and the tensile properties of the material.

Mcpherson, Albert E↗

Environmental exposure effects on composite materials for commercial aircraft

Activities reported include completion of the program design tasks, resolution of a high fiber volume problem and resumption of specimen fabrication, fixture fabrication, and progress on the analysis methodology and definition of the typical aircraft environment. Program design activities including test specimens, specimen holding fixtures, flap-track fairing tailcones, and ground exposure racks were completed. The problem experienced in obtaining acceptable fiber volume fraction results on two of the selected graphite epoxy material systems was resolved with an alteration to the bagging procedure called out in BAC 5562. The revised bagging procedure, involving lower numbers of bleeder plies, produces acceptable results. All required laminates for the contract have now been laid up and cured. Progress in the area of analysis methodology has been centered about definition of the environment that a commercial transport aircraft undergoes. The selected methodology is analagous to fatigue life assessment.

Hoffman, D. J.↗

Evaluating of NASA-Langley Research Center explosion seam welding

An explosion bonding technique to meet current fabrication requirements was demonstrated. A test program was conducted on explosion bonded joints, compared to fusion joints in 6061-T6 aluminum. The comparison was made in required fixtures, non-destructive testing, static strength and fatigue strength.

Otto, H. E.↗

DROP DURABILITY ASSESSMENT OF ELECTRONIC ASSEMBLIES UNDER OFF-AXIS LOADING WITH SKEWED FIXTURES

This thesis studies drop durability of electronic assemblies when the acceleration vector is oriented at 45° to the out-of-plane direction of the circuit card. The off-axis drop tests are accomplished with a skewed fixture and are conducted as a proxy for multiaxial drop testing. Advanced shock testing and vibration test methods have been developed over the last few decades to better represent real-world field environments during ground-based laboratory testing. However, many of these test methods require expensive and specialized equipment not available in most laboratories. An alternative approach for approximating simultaneous loading along multiple axes on conventional equipment utilizes skewed fixtures which have seen use in off-axis random vibration and drop impact testing. These methods generally rely on the conversion of a uniaxial input load from the test equipment (using a uniaxial drop tower or shaker) into a multiaxial load when resolved in the reference frame of the test article (mounted on a skewed fixture). Skewed fixture design is presented and recommendations for conducting skewed angle drop testing are introduced based on local measurements along the skewed face of the fixture to accurately monitor the impact event. Characterization tests were performed with a skewed fixture, at simultaneous acceleration loads from 500 to 3,000 g in two (in-plane and out-of-plane) directions, while meeting standard time domain tolerances. Upon experimental characterization, drop shock durability tests were conducted on a printed circuit assembly (PCA). Mean drops-to-failure were measured and quantified with Weibull statistics. Dominant solder joint failure modes were identified via failure analysis. Prior work on inclined angle impact testing is limited, and the majority of solder joint interconnect level fatigue studies are conducted considering perpendicular loading normal the circuit card. Low-cycle fatigue curves are generated based on plastic strain and plastic work density within the solder joint. A multiscale nonlinear finite element model is used to relate board-level flexure to solder joint interconnect level plastic strain. A high strain rate solder constitutive model allows for accurate modeling of solder plasticity resulting from high-impact drop shock. Fatigue parameters are computed from the Coffin-Manson relation and Palmgren-Miner damage accumulation. This work serves to apply established low-cycle fatigue methods for conventional drop shock loading (impact normal to circuit card) to non-perpendicular loading with a skewed fixture.

Hower, Jonathan [Kansas City National Security Cam↗

SWAS Spacecraft T/V Test, Unique In Chamber Tests Systems Actuation

The Sub-Millimeter Wave Astronomy Satellite (SWAS) is the third mission of the Small Explorer (SMEX) Project at Goddard Space Flight Center (GSFC). It is a path finding mission to study the chemical composition of interstellar galactic clouds to help determine the process of star formation. The spacecraft recently completed a month-long then-nal vacuum/thermal balance test in the Solar Environmental Simulator, the largest thermal vacuum facility at Goddard. Rather extensive fixturing was required for the test, considering the small size of the spacecraft, and two unusual deployments were completed in order to accomplish the goals of the test. This paper discusses the space simulation testing of the fully integrated SWAS spacecraft and the unique fixturing required.

Dunn, Jamie L.↗

RF characterization of monolithic microwave and mm-wave ICs

A number of fixturing techniques compatible with automatic network analysis are presented. The fixtures are capable of characterizing GaAs Monolithic Microwave Integrated Circuits (MMICs) at K and Ka band. Several different transitions are used to couple the RF test port to microstrip. Fixtures which provide chip level de-embedding are included. In addition, two advanced characterization techniques are assessed.

Romanofsky, R. R.↗

A comparison of three shear test methods for composite materials

A graphite-epoxy composite material system is used to evaluate the performance of three popular shear tests - the 10-deg off-axis, the +/-45-deg tension, and the Iosipescu specimen tested in the modified Wyoming fixture. A comparison of the shear stress-strain response for each test method is made using a conventional strain gage instrument and moire interferometry. The uniformity and purity of the strain fields in the test sections of the specimens are discussed, and the shear responses obtained from each test are presented and compared. It is shown that the shear stress-strain responses obtained by instrumenting only one face of the 90-deg Iosipescu specimen could give erroneous results. The +/-45-deg tensile and 0-deg Iosipescu specimens were not affected by front-to-back face shear strain variations. Correction factors could be applied to bring all responses together, within the limits of the material uniformity, which was itself documented in the moire fringe patterns.

Ho, H.↗

A Simple Test Method for Large Deformation Bending of Thin High Strain Composite Flexures

A simple test method for large deformation bending of thin composite laminates is investigated using image processing and full-field strain measurements. The assumptions and kinematic equations that represent the test are used to calculate numerically the laminate bending stiffness and strength as well as the curvature and strains at failure. In order to validate the test methodology, a comparison is performed between analytical model predictions and empirical data in terms of computed surface strains versus digital image correlation data and calculated rotation angles of the fixture arms throughout the test versus measured ones. The new test method is then used to calculate the bending stiffness in the D11 and D22 directions as well as failure strains for various thin-ply laminates of interest. These parameters are ultimately compared with predicted values using micromechanics and classical lamination theory analysis. In general, bending stiffness and strain test results and predictions for 0 degree orientation coupons have a maximum difference of 10% and 35%.

Fernandez, Juan M.↗

Recent Advances to Estimation of Fixed-Interface Modal Models Using Dynamic Substructuring

In 2010, Allen & Mayes proposed to estimate the fixed-interface modes of a structure by measuring the modes of the structure bolted to a fixture and then applying constraints to the fixture using the transmission simulator method. While the method proved useful, and has indeed been used in studies since that point, a few peculiarities were noted. First, in some cases the estimated fixed-base natural frequencies were observed to converge very slowly to the true values (in simulated experiments) as the number of constraints was increased. To formulate these constraints, prior studies used only the free-interface modes of the fixture or the measured modes of the assembly. This work extends that to consider other sets of constraints, showing improved results. Furthermore, in some prior studies it has been observed that there were errors of more than 10% in the natural frequencies even when the fixture motion was hundreds of times smaller than the motion of the structure of interest (and so it had presumably been removed). This work explores this phenomenon, seeking to use the strain energy in the fixture, to the extent that it can be estimated using a test-analysis model for the fixture, as a metric to predict frequency error. The proposed methods are explored by applying them to simulated measurements from a beam and from the NASA Space Launch System coupled to the Mobile Launcher.

Allen, Mathew S.↗

Fatigue crack propagation behavior of the Ni-Ni3Cb eutectic composite

The experimental procedures used in the investigation are considered, taking into account solidification and heat treatment, fatigue testing, questions of test specimen and loading fixture design verification, metallographic techniques, and electron microscopy techniques. Attention is given to the characteristics of the microstructure, aspects of fatigue crack propagation (FCP) in the Ni-Ni3Nb composite, the effect of test variables on FCP, the effect of metallurgical variables on FCP, and fatigue fracture mechanisms. Fractographic and metallographic observations are discussed.

Mills, W. J.↗

Device For Testing Compatibility Of An O-Ring

Fixture designed for use in exposing compressed elastomeric O-ring or other ring seal to test fluid. Made of metal or plastic, with threaded recess into which O-ring placed. Opposite threaded end is opening through which test fluid introduced and placed in contact with O-ring. After exposure, compression set and swell or shrinkage of ring measured. Fixture set to compress ring by selected amount, providing for reproducible compression.

Davis, Dennis D.↗

Variabilities detected by acoustic emission from filament-wound Aramid fiber/epoxy composite pressure vessels

Two hundred and fifty Aramid fiber/epoxy pressure vessels were filament-wound over spherical aluminum mandrels under controlled conditions typical for advanced filament-winding. A random set of 30 vessels was proof-tested to 74% of the expected burst pressure; acoustic emission data were obtained during the proof test. A specially designed fixture was used to permit in situ calibration of the acoustic emission system for each vessel by the fracture of a 4-mm length of pencil lead (0.3 mm in diameter) which was in contact with the vessel. Acoustic emission signatures obtained during testing showed larger than expected variabilities in the mechanical damage done during the proof tests. To date, identification of the cause of these variabilities has not been determined.

Hamstad, M. A.↗

Nickel hydrogen cell tests

Some parametric tests followed by cycling tests are described for the characterization of the service life of nickel hydrogen cells. Three cells were automatically cycled in simulated low Earth orbit in 35 minute discharge, 55 minute charge, with charging voltage limited, temperature compensated. The cells were mounted in a fixture that conducts heat to an aluminum baseplate. The baseplate in turn, is bounded in a temperature controlled bath to remove the heat from the mounted fixture. One cell was tested with a zircar separator, which failed after 2473 cyles. Two other cells were tested one with a zircar separator; the other with asbestos. More than 400 cycles were achieved.

Mueller, V. C.↗