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At least 487 records · Page 27
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Chemical identification of new particle formation and growth precursors through positive matrix factorization of ambient ion measurements

Abstract. In the lower troposphere, rapid collisions between ions and trace gases result in the transfer of positive charge to the highest proton affinity species and negative charge to the lowest proton affinity species. Measurements of the chemical composition of ambient ions thus provide direct insight into the most acidic and basic trace gases and their ion–molecule clusters – compounds thought to be important for new particle formation and growth. We deployed an atmospheric pressure interface time-of-flight mass spectrometer (APi-ToF) to measure ambient ion chemical composition during the 2016 Holistic Interactions of Shallow Clouds, Aerosols, and Land Ecosystems (HI-SCALE) campaign at the United States Department of Energy Atmospheric Radiation Measurement facility in the Southern Great Plains (SGP), an agricultural region. Cations and anions were measured for alternating periods of ∼ 24 h over 1 month. We use binned positive matrix factorization (binPMF) and generalized Kendrick analysis (GKA) to obtain information about the chemical formulas and temporal variation in ionic composition without the need for averaging over a long timescale or a priori high-resolution peak fitting. Negative ions consist of strong acids including sulfuric and nitric acid, organosulfates, and clusters of NO3- with highly oxygenated organic molecules (HOMs) derived from monoterpene (MT) and sesquiterpene (SQT) oxidation. Organonitrates derived from SQTs account for most of the HOM signal. Combined with the diel profiles and back trajectory analysis, these results suggest that NO3 radical chemistry is active at this site. SQT oxidation products likely contribute to particle growth at the SGP site. The positive ions consist of bases including alkyl pyridines and amines and a series of high-mass species. Nearly all the positive ions contained only one nitrogen atom and in general support ammonia and amines as being the dominant bases that could participate in new particle formation. Overall, this work demonstrates how APi-ToF measurements combined with binPMF analysis can provide insight into the temporal evolution of compounds important for new particle formation and growth.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

Position-specific kinetic isotope effects for nitrous oxide: a new expansion of the Rayleigh model

Nitrous oxide (N 2 O) is a potent greenhouse gas and the most significant anthropogenic ozone-depleting substance currently being emitted. A major source of anthropogenic N 2 O emissions is the microbial conversion of fixed nitrogen species from fertilizers in agricultural soils. Thus, understanding the enzymatic mechanisms by which microbes produce N 2 O has environmental significance. Measurement of the 15 N/ 14 N isotope ratios of N 2 O produced by purified enzymes or axenic microbial cultures is a promising technique for studying N 2 O biosynthesis. Typically, N 2 O-producing enzymes combine nitrogen atoms from two identical substrate molecules (NO or NH 2 OH). Position-specific isotope analysis of the central (N α ) and outer (N β ) nitrogen atoms in N 2 O enables the determination of the individual kinetic isotope effects (KIEs) for N α and N β , providing mechanistic insight into the incorporation of each nitrogen atom. Previously, position-specific KIEs (and fractionation factors) were quantified using the Rayleigh distillation equation, i.e., via linear regression of δ 15 N α or δ 15 N β against [–f In f / (1 – f)], where f is the fraction of substrate remaining in a closed system. This approach, however, is inaccurate for N α and N β because it does not account for fractionation at N α affecting the isotopic composition of substrate available for incorporation into the β position (and vice versa). Therefore, we developed a new expansion of the Rayleigh model that includes specific terms for fractionation at the individual N 2 O nitrogen atoms. By applying this Expanded Rayleigh model to a variety of simulated N 2 O synthesis reactions with different combinations of normal, inverse, and/or no KIEs at N α and N β , we demonstrate that our new model is both accurate and robust. We also applied this new model to two previously published datasets describing N 2 O production from NH 2 OH oxidation in a methanotroph culture (Methylosinus trichosporium) and N 2 O production from NO by a purified Histoplasma capsulatum (fungal) P450 NOR, demonstrating that the Expanded Rayleigh model is a useful tool in calculating position-specific fractionation for N 2 O synthesis.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1973

Terminal shock position and restart control of a Mach 2.7, two-dimensional, twin duct mixed compression inlet

Experimental results of terminal shock and restart control system tests of a two-dimensional, twin-duct mixed compression inlet are presented. High-response (110-Hz bandwidth) overboard bypass doors were used, both as the variable to control shock position and as the means of disturbing the inlet airflow. An inherent instability in inlet shock position resulted in noisy feedback signals and thus restricted the terminal shock position control performance that was achieved. Proportional-plus-integral type controllers using either throat exit static pressure or shock position sensor feedback gave adequate low-frequency control. The inlet restart control system kept the terminal shock control loop closed throughout the unstart-restart transient. The capability to restart the inlet was non limited by the inlet instability.

Cole, G. L.↗
NASA NTRS1971

Study of precise positioning at L-band using communications satellites

The L-band positioning experiment is reported which encompassed experiment design, experimentation, and data reduction and analysis. In the experiment the ATS-5 synchronous satellite L-band transponder was used in conjunction with the modified ALPHA 2 navigation receivers to demonstrate the technical capability of precision position fixing for oceanographic purposes. The feasibility of using relative ranging techniques implemented by two identical receiving systems, properly calibrated, to determine a line of position accurately on the surface of the earth was shown. The program demonstrated the level of resolution, repeatibility, precision, and accuracy of existing modest-cost effective navigation equipment. The experiment configuration and data reduction techniques were developed in parallel with the hardware modification tasks. Test results verify the ability of a satellite-based system to satisfy the requirements of precision position fixing.

Source record↗
NASA NTRS1974

Method and apparatus for optically monitoring the angular position of a rotating mirror

An optical system monitors the angular position of a rotating scanning mirror to indicate the effective start and end of each scan. At a certain angular position, a ray of energy transmitted to the mirror is reflected a plurality of times between the reflectors associated with the optical system and the line on the mirror parallel to the axis, and then to a detector to sense that angular position. A single optical system may be arranged to sense a plurality of different angular positions for each revolution of the mirror.

Lansing, J. C., Jr.↗
NASA NTRS1974

Analytical expressions for position error in triangulation solution of point in space for several station configurations

Analytical expressions are derived to first order for the rms position error in the triangulation solution of a point object in space for several ideal observation-station configurations. These expressions provide insights into the nature of the dependence of the rms position error on certain of the experimental parameters involved. The station geometries examined are: (1) the configuration of two arbitrarily located stations; (2) the symmetrical circular configuration of two or more stations with equal elevation angles; and (3) the circular configuration of more than two stations with equal elevation angles, when one of the stations is permitted to drift around the circle from its position of symmetry. The expressions for the rms position error are expressed as functions of the rms line-of-sight errors, the total number of stations of interest, and the elevation angles.

Long, S. A. T.↗
NASA NTRS1975

A complementary filtering technique for deriving aircraft velocity and position information

An onboard navigation system which employed complementary filtering was developed to provide velocity and position information. The inputs to the mix filter included both acceleration inputs, which provided high-frequency position and velocity information, and radar position inputs, which provided the low-frequency position and velocity information. Onboard aircraft instrumentation, including attitude reference gyros and body-mounted accelerometers, was used to provide the acceleration information. An in-flight comparison of signal quality and accuracy showed good agreement between the complementary filtering system and an aided inertial navigation system. Furthermore, the complementary filtering system was proven to be satisfactory in control and display system applications for both automatic and pilot-in-the-loop instrument approaches and landings.

Niessen, F. R.↗
NASA NTRS1976

Radio source positions from very-long-baseline interferometry observations

Accurate positions of compact radio sources have been determined from very-long-baseline interferometry (VLBI) observations based on the bandwidth-synthesis technique. The coordinates for 18 extragalactic sources were obtained from sets of observations spread over the period from April 1972 to January 1975; the scatter among the independent determinations of the source coordinates from the separate sets of observations is about 0.05 arcsec, except for the declinations of near-equatorial sources, where the scatter is about 0.15 arcsec. Comparison of these positions with those determined with the Cambridge 5-km radio interferometer shows the rms scatter about the mean difference to be about 0.04 arcsec in each coordinate (no sources of low declination were in common). A similar comparison of the present results with those obtained by the Jet Propulsion Laboratory from separate VLBI observations yields a slightly larger rms scatter, after exlusion of the declinations of the near-equatorial sources. A position is also obtained for the galactic object Beta Persei (Algol), which agrees well with the position given in the FK 4 catalogue.

Clark, T. A.↗
NASA NTRS1978

The effect of landing system coverage and path geometry on lateral position errors at the runway threshold

The results of an analytical study performed to determine the effect of the azimuth coverage of a Microwave Landing System (MLS) on the ability of an airplane, with an initial navigation position estimate error, to navigate to the runway threshold are presented. The test path chosen for this study consists of an initial straight segment leading into a 130 deg turn with a 2286 m radius and ending in a straight-in final approach segment. The test path configuration was varied by changing the MLS azimuth coverage angle and the final approach length. The aircraft was positioned with an inital offset to the left or right of the desired path along the line of intersection with the MLS azimuth coverage. A fast time computer simulation program, using a simplistic point mass model of the airplane, was used for this study. The data from this study indicates that the lateral position errors at the runway are primarily a function of the final approach length. The effect of the azimuth coverage on the lateral position errors was restricted by the turn characteristics of the horizontal steering control laws.

Vicroy, D. D.↗
NASA NTRS1978

Positions of galactic X-ray sources with l/II/ between -20 deg and +6 deg

The precise positions of nine X-ray sources in the vicinity of the galactic center are reported. The data were obtained as part of the comprehensive survey of the galactic plane performed with the rotating modulation collimator detectors on the SAS-3 X-ray observatory. The sources include the binary X-ray source 4U 1700-37 which has a well established optical counterpart that lies 7 sec from the reported position. The other sources GX 349+2, 4U 1702-42, 4U 1705-44, MX 1716-31, A 1742-294, 4U 1755-33, GX 5-1, and 2S 1803-245 lack established counterparts in other wavelengths. The obtained position for GX 5-1 adds confidence to the radio counterpart proposed by Braes et al. (1972). The reported position for 4U 1755-33 excludes the optical counterpart proposed by Jones et al. (1974).

Jernigan, J. G.↗
NASA NTRS1978

Positions of galactic X-ray sources - At longitudes /l-II/ of 55-320 deg

Rotating modulation collimeter detectors on the SAS-3 X-ray observatory were used to supply precise (20-40 sec) positional data on 10 galactic X-ray sources in the l super II region between 55 and 320 deg. It is noted that the position for 2S0114+650 has led to the discovery of an optical counterpart. Attention is given to the temperature dependence of the experiments, and it is found that position measurements made at low temperatures are consistent with those obtained at normal (0 C) temperatures. Positions, error radii, and intensities (2-11 keV) are listed for each of the ten sources.

Dower, R. G.↗
NASA NTRS1979

Limb blood flow - Rest and heavy exercise in sitting and supine positions in man

The objectives of the study were twofold: (1) to determine the effect of body position (hydrostatic pressure) on total blood flow in active and passive limbs at rest and after severe exercise; and (2) to further evaluate the impedance technique for measurement of blood flow. To this end, the effect of body position on the redistribution of total blood flow in active (leg) and passive (forearm) limbs during exercise was determined by measuring total limb impedance (blood flow) in five male and one female subjects in sitting and supine positions with a modified Beckman BR-100 rheograph. The results show that, at rest and after exercise, the supine position induces significantly greater flows in the leg but not in the forearm. With severe exercise, blood flows are increased in both passive and active limbs, so that there is probably no net transfer of blood volume from passive to active muscles. The advantages of the impedance technique over other methods are stressed.

Greenleaf, J. E.↗
NASA NTRS1980

Position surveillance using one active ranging satellite and time-of-arrival of a signal from an independent satellite

Position surveillance using one active ranging/communication satellite and the time-of-arrival of signals from an independent satellite was shown to be feasible and practical. A towboat on the Mississippi River was equipped with a tone-code ranging transponder and a receiver tuned to the timing signals of the GOES satellite. A similar transponder was located at the office of the towing company. Tone-code ranging interrogations were transmitted from the General Electric Earth Station Laboratory through ATS-6 to the towboat and to the ground truth transponder office. Their automatic responses included digital transmissions of time-of-arrival measurements derived from the GOES signals. The Earth Station Laboratory determined ranges from the satellites to the towboat and computed position fixes. The ATS-6 lines-of-position were more precise than 0.1 NMi, 1 sigma, and the GOES lines-of-position were more precise than 1.6 NMi, 1 sigma. High quality voice communications were accomplished with the transponders using a nondirectional antenna on the towboat. The simple and effective surveillance technique merits further evaluation using operational maritime satellites.

Anderson, R. E.↗
NASA NTRS1982

2.3-GHz accurate positions and optical identifications for selected Parkes radio sources

Accurate radio positions of 74 extragalactic radio sources contained in the Parkes 2.7-GHz survey were measured at 2.3 GHz with the Tidbinbilla interferometer, located near Canberra, Australia. The radio sources, most of which lie between declinations -30 deg and -35 deg, were measured to an rms positional accuracy of about 3 arcsec relative to a grid of previously identified radio sources. Optical identifications have been made on the basis of positional coincidence alone, without regard to color or morphology, using the UK Schmidt telescope deep IIIa-J sky survey plates. Identifications are suggested and accurate optical positions have been measured for 62 objects brighter than magnitude 22.5 on the IIIa-J plates.

Jauncey, D. L.↗
NASA NTRS1984

Obtaining accurate comet positions despite some inaccurate catalog stars

From an astrographic negative a grid is determined from measurement of all the reference stars and using their catalog positions, and other grids from selections of reference stars. These grids are determined from many stars, and individual stars will have errors with respect to the grid. There are ways to identify stars X that are not at their cataloged position: (1) determine the focal length of the telescope from the measurements of each pair of stars and look for discordant results; (2) stars X are several arcseconds off the grid, and the other stars fit better when stars X do not help determine the grid; and (3) the grid is stretched or distorted to include the stars X. Fifteen to twenty percent of the stars in the S.A.O. catalog are 1.5 seconds or more off their catalog positions. An interactive session with a computer can find and eliminate these errant stars and result in more accurate comet positions.

Everhart, E.↗
NASA NTRS1985

Theoretical prediction of stationary positions in the rectangular chamber during asymmetric electroosmotic flow

Most microscopic cell electrophoretic work depends on the theortical prediction of stationary positions by Smoluchowski and Komagata. Their theoretical solutions are based on the assumption that the electroosmotic flow in a chamber is symmetric. Because experiences with the rectangular chamber indicate that symmetric flow occurs during less than 8% of the experiments, the existing theory for stationary position determination is expanded to include the more general case of asymmetric flow. Smoluchowski's equation for symmetric electroosmotic flow in a rectangular chamber having a width much smaller than its height or length is examined. Smoluchowski's approach is used to approximate stationary positions in rectangular chambers with height/width ratios greater than 40. Support for the theoretical prediction of stationary positions using is given by three types of experimental evidence.

Source record↗
NASA NTRS1985

Middle-atmosphere positive ion measurements during solar eclipses

Solar effects on middle-atmosphere electrical parameters, as demonstrated by eclipse-associated responses of conductivity, ion mobility, and charge density, are considered for the total solar eclipses at Red Lake, Ontario, Canada on February 26, 1979 and at San Marco range, Kenya, on February 16, 1980. Negative-conductivity measurements for the Canadian eclipse and probe-current measurements for the Kenyan eclipse demonstrate a rapid loss of free electrons below 80 km at totality. During the Kenyan eclipse, positive-ion responses were different for each of two distinct ion mobility groups. Between 45 and 60 km, eclipse-related positive-ion responses are associated with the low-mobility ions. It is shown that these ions are lost at totality and that an excess buildup occurs following totality. Above 70 km, positive-ion loss at totality is associated with the more mobile ions and only low-mobility positive ions are measured in this region. The buildup in total ion density following totality is thought to result from a reduction in ion loss associated with weak-electron recovery in the region.

Mitchell, J. D.↗
NASA NTRS1986

Non-dynamic decimeter tracking of earth satellites using the Global Positioning System

A technique is described for employing the Global Positioning System (GPS) to determine the position of a low earth orbiter with decimeter accuracy without the need for user dynamic models. A differential observing strategy is used requiring a GPS receiver on the user vehicle and a network of six ground receivers. The technique uses the continuous record of position change obtained from GPS carrier phase to smooth position measurements made with pseudo-range. The result is a computationally efficient technique that can deliver decimeter accuracy down to the lowest altitude orbits.

Yunck, T. P.↗