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NASA NTRS2018

Fluid Inclusions in Astromaterials: Direct Samples of Early Solar System Aqueous Fluids

We have become increasingly aware of the fundamental importance of water, and aqueous alteration, on primitive solar-system bodies. All classes of astromaterials studied show some degree of interaction with aqueous fluids. We have direct observations of cryovolcanism of several small solar system bodies (e.g. Saturnian and Jovian moons), and indirect evidence for this process on the moons Europa, Titan, Ganymede, and Miranda, and the Kuiper Belt object Charon, and so are certain of the continuing and widespread importance of aqueous processes across the solar system. Nevertheless, we are still lacking fundamental information such as the location and timing of the aqueous alteration and the detailed nature of the aqueous fluid itself.

Zolensky, Michael↗

NASA NTRS2012

Organic Synthesis via Irradiation and Warming of Ice Grains in the Solar Nebula

Complex organic compounds, including many important to life on Earth, are commonly found in meteoritic and cometary samples, though their origins remain a mystery. We examined whether such molecules could be produced within the solar nebula by tracking the dynamical evolution of ice grains in the nebula and recording the environments they were exposed to. We found that icy grains originating in the outer disk, where temperatures were less than 30 K, experienced UV irradiation exposures and thermal warming similar to that which has been shown to produce complex organics in laboratory experiments. These results imply that organic compounds are natural byproducts of protoplanetary disk evolution and should be important ingredients in the formation of all planetary systems, including our own.

Ciesla, Fred J.↗

NASA NTRS1988

Stable isotopic studies of H,C,N,O and S in samples of Martian origin

The present day geochemical cycles of volatile elements through the various reservoirs on Earth are largely understood within the context of the planet's standing as a geologically and biologically evolved body. In terrestrial studies stable isotope measurements of light elements (H, C, N, O and S) can be utilized to obtain insight into the conditions prevailing during formation of rocks of various types. Perhaps the most important problem which could be addressed by light element studies of the sorts of specimen likely to be available from remote automatic sampling, would be the role of volatiles during evolution. Of fundamental importance here is the question of whether Mars was volatile rich or volatile poor. The only way to fully comprehend the effects of volatile cycling through the mantle crust and regolith atmosphere polar cap system of Mars, is by analyses of appropriate returned samples. In order to interpret the record of geological activity in Martian samples it will be necessary to understand how the past, or present, surface environment may have acted to disturb the primary characteristics of the rocks.

Wright, I. P.↗

NASA NTRS1989

VUV-visible measurements on different samples of amorphous carbon

Among various candidate materials for interstellar dust, amorphous carbon (AC) is playing an increasingly important role (Greenstein, 1981; Hecht et al., 1984; Jura, 1983, 1986). Furthermore, recent in situ measurements have clearly shown the presence of carbonaceous grains in the coma of comet Halley (Kissel et al., 1986). Laboratory investigations on AC grains may be very useful to better interpret observations and to support theoretical elaborations. Recently, the authors started an international research program which also includes UV extinction analyses on AC samples, by using synchrotron light. Preliminary results obtained in a first shift of measurements, last June, are given. At the present stage of the data analysis, the authors can only draw some preliminary considerations. A wide band falling at around 240 nm is detected in all the analyzed samples. It intensity seems to decrease with increasing the dust collecting distance. A peak at 150 nm decreases in intensity with increasing the collecting distance. The band seems absent in the samples characterized by a larger amount of dust. A feature at about 200 nm is detected in some samples. At the moment the authors tend to attribute it to the transmission properties of the LiF substrates at the wavelength and/or to some problems in the experimental setup. It is unclear if a hump at 120 nm is real or due to instrumental effects. The profile of the spectra does not show substantial changes when the samples are cooled down to about 100 K. The present results appear to be in general agreement with previous findings, but their analysis is in progress and the interpretation is still on the way.

Blanco, A.↗

NASA NTRS1988

Present imaging limitations to providing a geological assessment of potential sample return sites on Mars

A Mars sample return mission will provide a huge increase in knowledge about the region explored by the roving vehicle. However, presently there are some important limitations on the extent to which the geology of a potential site can be understood prior to landing the sample return vehicle on Mars. These limitations could affect not only the potential science return of the mission but also the safety of the vehicle. These limitations are examined.

Zimbelman, James R.↗

NASA NTRS1988

Application of imaging spectrometer data to the Kings-Kaweah ophiolite melange

The Kings-Kaweah ophiolite melange in east-central California is thought to be an obducted oceanic fracture zone and provides the rare opportunity to examine in detail the complex nature of this type of terrain. It is anticipated that the distribution and abundance of components in the melange can be used to determine the relative importance of geologic processes responsible for the formation of fracture zone crust. Laboratory reflectance spectra of field samples indicate that the melange components have distinct, diagnostic absorptions at visible to near-infrared wavelengths. The spatial and spectral resolution of AVIRIS is ideally suited for addressing important scientific questions concerning the Kings-Kaweah ophiolite melange and fracture zones in general.

Mustard, John F.↗

NASA NTRS1998

High-Temperature Deformation of Dry Diabase with Application to Tectonics on Venus

We have performed an experimental study to quantify the high-temperature creep behavior of natural diabase rocks under dry deformation conditions. Samples of both Maryland diabase and Columbia diabase were investigated to measure the effects of temperature, oxygen fugacity, and plagioclase-to-pyroxene ratio on creep strength. Flow laws determined for creep of these diabases were characterized by an activation energy of Q = 485 +/- 30 kJ/mol and a stress exponent of n = 4.7 +/- 0.6, indicative of deformation dominated by dislocation creep processes. Although n and Q are the same for the two rocks within experimental error, the Maryland diabase, which has the lower plagioclase content, is significantly stronger than the Columbia diabase. Thus the modal abundance of the various minerals plays an important role in defining rock strength. Within the s ample-to-sample variation, no clear influence of oxygen fugacity on creep strength could be discerned for either rock. The dry creep strengths of both rocks are significantly greater than values previously measured on diabase under "as-received" or wet conditions. Application of these results to the present conditions in the lithosphere on Venus predicts a high viscosity crust with strong dynamic coupling between mantle convection and crustal deformation, consistent with measurements of topography and gravity for that planet.

Mackwell, S. J.↗

NASA NTRS1997

The Remote Sensing of Mineral Aerosols and their Impact on Phytoplankton Productivity

The overall objective of this experiment was to test the iron hypothesis does the addition of iron to nutrient rich surface waters enhance productivity? Our specific objectives in this experiment included sampling and studying the marine aerosol size and type (which are related to chemical reactivity) during the PlumEx cruise to determine the importance of local (Galapagos Islands) versus long-range sources of atmospheric material. Detailed results of single particle analysis of our samples are being prepared for publication in two papers. We collect aerosol samples and they have been analyzed for trace metals and other elements. We are mapped aerosol distribution and the desert source areas around the Arabian Sea region. We did record a clear relationship between the aerosol radiance and synoptic weather patterns with distinct signals over the ocean northwest and southwest of Australia. While the interpretation was limited an aerosol climatology pattern was presented.

Tindale, Neil W.↗

NASA NTRSDate not supplied

Exploring the Jezero Crater Floor: Overview of Results from the Mars 2020 Perseverance Rover’s First Science Campaign

The Perseverance rover embarked on its first science campaign after landing in Jezero crater on February 18, 2021 and completing ~90 days of commissioning and Ingenuity helicopter activities. During this first campaign, Perseverance explored a large swath of Jezero’s crater floor, investigating and sampling several of the topographically lowest, and potentially oldest, rocks within the crater. Crater floor units: Perseverance explored the Máaz and Séítah formations (previously mapped as the Crater Floor Fractured Rough; Cf-fr and Crater Floor Fractured 1; Cf-f-1 units[1]). These are both widespread units in the crater that potentially correlate with units outside Jezero [2-4]. The Máaz fm. was distinguished from orbit by its mafic composition and densely cratered surface, and has various hypothesized origins, including lava flows[2] and volcaniclastic airfall [3]. The Máaz fm. is important for providing age/stratigraphic constraints on the Jezero western delta. If igneous, returned Máaz fm. samples may aid in calibrating the Mars crater chronology [2,5]and understanding Mars paleomagnetism and early igneous processes(see [6]). The Séítah fm. is olivine-bearing and has been interpreted to be related to a regional unit exposed along the inner rim of Jezero crater walls and occurs more broadly in the Nili Planum and Nili Fossae region. The olivine-bearing unit and its possible correlatives has a wide range of hypothesized origins including volcaniclastic airfall, impact melt, or aeolian and fluvial deposits [2-4,7,8]. The Séítahfm.is likely the oldest unit accessible to Perseverance and represents an important part of Jezero’s pre-delta-lacustrine history. As in the Máaz fm., the lithochemistry of the samples will help studies of early Mars igneous processes. The olivine-and carbonate-bearing components of this unit may also signify habitable conditions early in Jezero’s history, samples of which would be of high geochemical and astrobiological significance, as well as for understanding the martian carbon cycle(see [9]).

Mars 2020↗

NASA NTRS2011

ALH84001: The Key to Unlocking Secrets About Mars-15 Years and Counting

From the December 27, 1984 discovery of ALH84001, and its subsequent identification as a sample of Mars in 1993, mystery and debate has surrounded the meteorite. With the realization that the ALH84001 sample was a orthopyroxenite and one of the oldest SNC meteorites (~4.09 Ga) available to study, important and critical information about the Martian hydrosphere and atmosphere along with the early history and evolution of the planet could be obtained by studying the unique carbonate globules (~3.9 Ga) in the sample. The initial work showed the carbonate globules were deposited within fractures and cracks in the host-orthopyroxene by low-temperature aqueous fluids. Ideas that the carbonates were formed at temperatures approaching 800oC were ruled out by later experiments. The 1996 announcement by McKay et al. that ALH84001 contained features which could be interpreted as having a biogenic origin generated considerable excitement and criticism. The NASA Administrator Dan Golden said the 1996 ALH84001 announcement saved NASA s Mars planetary exploration program and injected $6 billion dollars over five years into the scientific research and analysis efforts. All of the original four lines of evidence for possible biogenic features within ALH84001 offered by McKay et al. have withstood the test of time. Criticism has been directed at the interpretation of the 1996 analytical data. Research has expanded to other SNC meteorites. Despite the numerous attacks on the ideas, the debate continues after 15 years. The 2009 paper by Thomas-Keprta et al. on the origins of a suite of magnetites within the ALH84001 has offered strong arguments that some of the magnetites can only be formed by biogenic processes and not from thermal decomposition or shock events which happened to the meteorite. NASA s Astrobiology Institute was formed from the foundation laid by the ALH84001 hypothesis of finding life beyond the Earth. The strong astrobiology outreach programs have expanded because of the work done on the Martian meteorites. Despite the criticism on the biogenic-like features in ALH84001, the meteorite has opened a window into the early history of Mars. Clearly low-temperature fluids have left their signatures within the ALH84001 meteorite and subsequent cratering events on Mars have been recorded on observable features within the meteorite. The 15 years of detailed study on ALH84001 and its unique carbonate globules have clearly shown formational and secondary processes at work on Mars. The evidence for biogenic processes operating on early Mars along with ground water activity within the last 15% of the life of Mars offers clear evidence that another niche for life may be possible within our solar system. Now we need a well-documented Mars sample return mission.

Gibson, Everett K.↗

NASA NTRS1985

Atmospheric concentrations and behavior of halocarbons and methane

The atmospheric concentrations of halocarbons and methane in the troposphere and stratosphere were precisely measured by grab-sampling followed by gas-chromatographic analysis in the laboratory. Chlorofluorocarbons such as CCl2F2 and CCl3F have received a great deal of attention due to their probable impact on the stratospheric ozone: the chlorofluorocarbons accumulated in the troposphere are eventually decomposed by photolysis in the stratosphere releasing Cl radicals which in turn participate in the ClO sub x-catalytic chain destroying the ozone, especially in the upper stratosphere. Methane reacts with Cl in the stratosphere reducing the ozone depletion, while its source and future trend of concentration in the troposphere are uncertain. The study of their distribution and behavior in the atmosphere are therefore very important. After the extensive survey of the locations for collection of atmospheriic samples representing the midlatitudes Northern Hemisphere (N.H.) without local contamination, we have measured the concentrations of CCl2F2, CCl3F, CH3CCl3, CC1, CHCl=CCl2 and CCl2=CCl2 with plus or minus 1 pptv precision in samples collected in Hokkaido and west coast Tohoku area (the northern part of Japan, 40 deg to 45 deg N) every summer and winter since 1979. The observed concentrations of CCl2F2 and CCl3F are now above 360 and 200 pptv, respectively, and have been steadily increasing by approx. 15 and approx. 8 pptv/year during the last several years.

Makide, Y.↗

NASA NTRS2012

Crystallization of Yamato 980459 at 0.5 GPA: Are Residual Liquids Like QUE 94201?

The Martian basaltic meteorites Y980459 and QUE94201 (henceforth referred to as Y98 and QUE respectively) are thought to represent magmatic liquid compositions, rather than being products of protracted crystallization and accumulation like the majority of other martian meteorites. Both meteorite compositions have been experimentally crystallized at 1 bar, and liquidus phases were found to match corresponding mineral core compositions in the meteorites, consistent with the notion that these meteorites represent bona fide melts. They also represent the most primitive and most evolved basaltic martian samples, respectively. Y98 has Mg# (molar Mg/Mg+Fe) approximates 65, and lacks plagioclase; whereas QUE has Mg# approximates 40, and lacks olivine. However they share important geochemical characteristics (e.g. superchondritic CaO/Al2O3, very high epsilon(sub Nd) and low Sr-87/Sr-87) that suggest they sample a similar highly depleted mantle reservoir. As such, they represent likely endmembers of martian magmatic liquid compositions, and it is natural to seek petrogenetic linkages between the two. We make no claim that the actual meteorites themselves share a genetic link (the respective ages rule that out); we are exploring only in general whether primitive martian liquids like Y98 could evolve to liquids resembling QUE. Both experimental and computational efforts have been made to determine if there is indeed such a link. Recent petrological models at 1 bar generated using MELTS suggest that a QUE-like melt can be derived from a parental melt with a Y98 composition. However, experimental studies at 1 bar have been less successful at replicating this progression. Previous experimental crystallization studies of Y98 by our group at 0.5 GPa have produced melt compositions approaching that of QUE, although these results were complicated by the presence of small, variable amounts of H2O in some of the runs owing to the use of talc/pyrex experimental assemblies. Therefore we have repeated the four experiments, augmented with additional runs, all using BaCO3 cell assemblies, which are devoid of water, and these new experiments supersede those reported earlier. Here we report results of experiments simulating equilibrium crystallization; fractional crystallization experiments are currently underway.

Rapp, J. F.↗

NASA NTRS2024

Volatiles in melt inclusions from lunar mare basalts: Bridging the gap in the H 2 O/Ce ratio between melt Inclusions in lunar pyroclastic sample 74220 and other mare samples

The H2O concentration and H 2 O/Ce ratio in olivine-hosted melt inclusions are high in lunar pyroclastic sample 74220 (H 2 O up to 1410 ppmw; H 2 O/Ce up to 77) but lower (H2O 10 to 430 ppmw; H 2 O/Ce 0.3 to 9.4) in all other lunar samples studied before this work. The difference in H 2 O concentration and in H 2 O/Ce ratio is absent for other volatile elements (F, S, and Cl) in melt inclusions in 74220 and other lunar samples. Because H 2 O (or H) is a critical volatile component with significant ramifications on the origin and evolution of the Moon, it is important to understand what causes such a large gap in H 2 O/Ce ratio between 74220 and other lunar samples. Two explanations have been advanced. One is that volcanic product in sample 74220 has the highest cooling rate and thus best preserved H 2 O in melt inclusions compared to melt inclusions in other samples. The other explanation is that sample 74220 comes from a localized heterogeneity enriched in some volatiles. To distinguish these two possibilities, here we present new data from two rapidly cooled lunar samples with glassy melt inclusions: olivine-hosted melt inclusions (OHMIs) in 79135 regolith breccia (unknown cooling rate but with glassy MIs similar in texture with those in 74220), and pyroxene-hosted melt inclusions (PHMIs) in 15597 pigeonite basalts (known high cooling rate, second only to 74220 and 15421). In addition, we also investigated new OHMIs in sample 74220. If the gap is due to the difference in cooling rates, samples with cooling rates between those of 74220 and other studied lunar samples should have preserved intermediate H2O concentrations and H 2 O/Ce ratios. Our results show that melt inclusions in 79135 and 15597 contain high H 2 O concentrations (up to 969 ppmw in 79135 and up to 793 ppmw in 15597) and high H 2 O/Ce ratios (up to 21 in 79135 and up to 13 in 15997), bridging the big gap in H 2 O/Ce ratio among 74220 and other lunar samples. Combined with literature data, we confirm that H 2 O/Ce ratios of different lunar samples are positively correlated to the cooling rates and independent of the type of mare basalts. We hence reinforce the interpretation that the lunar sample with the highest cooling rate best represents pre-eruptive volatiles in lunar basalts due to the least degassing. Based on Ce concentration in the primitive lunar mantle, we estimate that H 2 O concentration in the primitive lunar mantle (meaning bulk silicate Moon) is 121 ± 15 ppmw. Our new data also further constrain F/P, S/Dy and Cl/Ba ratios in lunar basalts and the lunar mantle. Estimated F, P, and S concentrations in the lunar primitive mantle are 4.4 ± 1.1 ppmw, 22 ± 8 ppmw, and 67 +67 −33 ppmw, respectively.

Xue Su↗

NASA NTRS2016

Spatial Sampling of Weather Data for Regional Crop Yield Simulations

Field-scale crop models are increasingly applied at spatio-temporal scales that range from regions to the globe and from decades up to 100 years. Sufficiently detailed data to capture the prevailing spatio-temporal heterogeneity in weather, soil, and management conditions as needed by crop models are rarely available. Effective sampling may overcome the problem of missing data but has rarely been investigated. In this study the effect of sampling weather data has been evaluated for simulating yields of winter wheat in a region in Germany over a 30-year period (1982-2011) using 12 process-based crop models. A stratified sampling was applied to compare the effect of different sizes of spatially sampled weather data (10, 30, 50, 100, 500, 1000 and full coverage of 34,078 sampling points) on simulated wheat yields. Stratified sampling was further compared with random sampling. Possible interactions between sample size and crop model were evaluated. The results showed differences in simulated yields among crop models but all models reproduced well the pattern of the stratification. Importantly, the regional mean of simulated yields based on full coverage could already be reproduced by a small sample of 10 points. This was also true for reproducing the temporal variability in simulated yields but more sampling points (about 100) were required to accurately reproduce spatial yield variability. The number of sampling points can be smaller when a stratified sampling is applied as compared to a random sampling. However, differences between crop models were observed including some interaction between the effect of sampling on simulated yields and the model used. We concluded that stratified sampling can considerably reduce the number of required simulations. But, differences between crop models must be considered as the choice for a specific model can have larger effects on simulated yields than the sampling strategy. Assessing the impact of sampling soil and crop management data for regional simulations of crop yields is still needed.

upscaling↗

NASA NTRS1978

Sampling analysis for the Earth Radiation Budget Satellite System mission based on orbital coverage and cloud variability

It is pointed out that accurate computation of the earth's radiation budget from satellite measurements requires spatial and temporal sampling which accounts for variations in cloud and surface conditions. It is in this connection important that cloud radiative properties and areal cloud cover be accurately determined for the desired time period. The reported investigation represents an extension of a study by Harrison et al. (1976). The time and space coverage capabilities of various sampling schemes are analyzed for the proposed Earth Radiation Budget Satellite System. The effects of cloud cover variability on the measured monthly mean reflected shortwave (0.2-5.0 micrometers) irradiance are also analyzed for several spatial scales.

Harrison, E. F.↗

NASA NTRS2014

X-Ray Micro-Computed Tomography of Apollo Samples as a Curation Technique Enabling Better Research

X-ray micro-computed tomography (micro-CT) is a technique that has been used to research meteorites for some time and many others], and recently it is becoming a more common tool for the curation of meteorites and Apollo samples. Micro-CT is ideally suited to the characterization of astromaterials in the curation process as it can provide textural and compositional information at a small spatial resolution rapidly, nondestructively, and without compromising the cleanliness of the samples (e.g., samples can be scanned sealed in Teflon bags). This data can then inform scientists and curators when making and processing future sample requests for meteorites and Apollo samples. Here we present some preliminary results on micro-CT scans of four Apollo regolith breccias. Methods: Portions of four Apollo samples were used in this study: 14321, 15205, 15405, and 60639. All samples were 8-10 cm in their longest dimension and approximately equant. These samples were micro-CT scanned on the Nikon HMXST 225 System at the Natural History Museum in London. Scans were made at 205-220 kV, 135-160 microamps beam current, with an effective voxel size of 21-44 microns. Results: Initial examination of the data identify a variety of mineral clasts (including sub-voxel FeNi metal grains) and lithic clasts within the regolith breccias. Textural information within some of the lithic clasts was also discernable. Of particular interest was a large basalt clast (approx.1.3 cc) found within sample 60639, which appears to have a sub-ophitic texture. Additionally, internal void space, e.g., fractures and voids, is readily identifiable. Discussion: It is clear from the preliminary data that micro-CT analyses are able to identify important "new" clasts within the Apollo breccias, and better characterize previously described clasts or igneous samples. For example, the 60639 basalt clast was previously believed to be quite small based on its approx.0.5 sq cm exposure on the surface of the main mass. These scans show the clast to be approx.4.5 g, however (assuming a density of approx.3.5 g/cc). This is large enough for detailed studies including multiple geo-chronometers. This basalt clast is of particular interest as it is the largest Apollo 16 basalt, and it is the only mid-TiO2 basalt in the Apollo sample suite. By identifying the location of interesting clasts or grains within a sample, we will be able to make more informed decisions about where to cut a sample in order to best expose clasts of interest for future study. Moreover, knowing the location of internal defects (e.g., fractures) will allow more precise chipping and extraction of clasts or grains. By combining micro-CT scans with compositional techniques like micro x-ray fluorescence (particularly on sawn slabs), we will be able to provide even more comprehensive information to scientists trying to best select samples that fit their scientific needs.

Ziegler, R. A.↗

NASA NTRS1980

An assessment of Landsat data acquisition history on identification and area estimation of corn and soybeans

During the past decade, numerous studies have demonstrated the potential of satellite remote sensing for providing accurate and timely crop area information. This study assessed the impact of Landsat data acquisition history on classification and area estimation accuracy of corn and soybeans. Multitemporally registered Landsat MSS data from four acquisitions during the 1978 growing season were used in classification of eight sample segments in the U.S. Corn Belt. The results illustrate the importance of selecting Landsat acquisitions based on spectral differences in crops at certain growth stages.

Hixson, M. M.↗

NASA NTRS1984

Rotation and surface brightness in elliptical galaxies

Correlations between the mean surface brightness and level of rotational support are presented and discussed for the sample of elliptical galaxies presented by Davies et al. (1983). The importance of these distance-independent correlations lies in the ability to isolate the effects of projection, and hence to define an intrinsic, edge-on correlation. Thus the position of an elliptical galaxy in this plane contains information about its true shape. In addition, the slope of the 'edge-on' correlation can be compared cleanly with theoretical predictions. The correlation is interpreted as a manifestation of varying amounts of dissipation during the formation epoch of a galaxy, with higher surface brightness, rotating ellipticals having dissipated more binding energy.

Wyse, R. F. G.↗