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At least 487 records · Page 27

Hard X-ray imaging with sub-10 nm resolution by scanning bonded 2D multilayer Laue lenses

Multilayer Laue lenses (MLLs) offer significant advantages over traditional diffractive focusing optics, such as zone plates (ZPs), in terms of efficiency and durability when focusing hard X-rays to 10 nm and below. Typically, a pair of 1D MLLs is aligned independently to achieve point focusing. This approach only permits scanning microscopy by moving the sample stage, which presents a limitation when it comes to scanning large or bulky objects at high speed. In this study, we present an experimental demonstration of scanning monolithically bonded 2D MLLs while keeping the sample stationary, effectively addressing the limitation of the sample’s size and weight. We characterized the system’s positional and angular stabilities during scanning, which are critical parameters to the nanofocusing performance of MLLs. In addition, we provided the X-ray measurement results and corresponding image resolution analysis.

36 MATERIALS SCIENCE↗

A real-time electronic imaging system for solar X-ray observations from sounding rockets

A real-time imaging system for displaying the solar coronal soft X-ray emission, focussed by a grazing incidence telescope, is described. The design parameters of the system, which is to be used primarily as part of a real-time control system for a sounding rocket experiment, are identified. Their achievement with a system consisting of a microchannel plate, for the conversion of X-rays into visible light, and a slow-scan vidicon, for recording and transmission of the integrated images, is described in detail. The system has a quantum efficiency better than 8 deg above 8 A, a dynamic range of 1000 coupled with a sensitivity to single photoelectrons, and provides a spatial resolution of 15 arc seconds over a field of view of 40 x 40 square arc minutes. The incident radiation is filtered to eliminate wavelengths longer than 100 A. Each image contains 3.93 x 10 to the 5th bits of information and is transmitted to the ground where it is processed by a mini-computer and displayed in real-time on a standard TV monitor.

Davis, J. M.↗

Plasma temperature measurement with a silicon photomultiplier (SiPM)

The temperature of a nonneutral plasma confined in a Penning–Malmberg trap can be determined by slowly lowering one side of the trap’s electrostatic axial confinement barrier; the temperature is inferred from the rate at which particles escape the trap as a function of the barrier height. In many experiments, the escaping particles are directed toward a microchannel plate, and the resulting amplified charge is collected on a phosphor screen. The screen is used for imaging the plasma but can also be used as a Faraday cup (FC) for a temperature measurement. The sensitivity limit is then set by microphonic noise enhanced by the screen’s high-voltage bias. Alternately, a silicon photomultiplier (SiPM) can be employed to measure the charge via the light emitted from the phosphor screen. This decouples the signal from the microphonic noise and allows the temperature of colder and smaller plasmas to be measured than could be measured previously; this paper focuses on the advantages of a SiPM over a FC.

Hunter, E. D. (ORCID:0000000236242840)↗

Enhancement of the jets in NGC 1097

Plates of NGC 1097 taken in four spectral bands have been digitized and processed at JPL's Image Processing Laboratory. The processing has revealed that (1) there is a fourth jet, R4, counter to the L-shaped jet, R1; (2) the area density of point sources in the jets is no different from that found on the sky; (3) two of the jets, R1 and R2, are bluer than the night sky, while one of the jets, R3, is redder than the night sky; (4) the nonstellar objects situated on the jets are noticeably bluer than the night sky; and (5) color-enhanced images of the spiral structure illustrate the distribution of both gaseous and spiral-arm stellar population disrupted from symmetry by an apparent companion elliptical.

Lorre, J. J.↗

Compact Imaging Spectrometer

Imaging spectrometer for use in crop and mineral resource-mapping experiments is scaled-down version. Compact imaging spectrometer uses Schmidt/Littrow optics with single spherical primary mirror. Radiation from scene strikes reflecting Schmidt corrector plate located near center of curvature of primary spherical mirror.

Wellman, J. B.↗

OTS 1809+314 and the gamma-ray burst GB 790325b

Deep CCD images of the field containing the recurring Optical Transient Source (OTS) 1809+314 recently discovered on archival plates of the Sonneberg Observatory are presented. At the position of OTS 1809+314 no optical counterpart brighter than V = 24.0-24.5, r(Gunn) = 22.0-22.5, and I = 22.0-22.5 is found. In the zero proper motion limit our observations place severe constraints on possible quiescent counterparts. There is no compelling evidence to suggest an association between the historical optical transient source and the gamma-ray burst GB 790325b located about 5 arcmin to the east of OTS 1809+314.

Hartmann, Dieter↗

Multilayer and grazing incidence X-ray/EUV optics; Proceedings of the Meeting, San Diego, CA, July 22-24, 1991

The present conference discusses the Advanced X-ray Astrophysics Facility (AXAF) calibration by means of synchrotron radiation and its X-ray reflectivity, X-ray scattering measurements from thin-foil X-ray mirrors, lobster-eye X-ray optics using microchannel plates, space-based interferometry at EUV and soft X-ray wavelengths, a water-window imaging X-ray telescope, a graded d-spacing multilayer telescope for high energy X-ray astronomy, photographic films for the multispectral solar telescope array, a soft X-ray ion chamber, and the development of hard X-ray optics. Also discussed are X-ray spectroscopy with multilayered optics, a slit aperture for monitoring X-ray experiments, an objective double-crystal spectrometer, a Ly-alpha coronagraph/polarimeter, tungsten/boron nitride multilayers for XUV optical applications, the evaluation of reflectors for soft X-ray optics, the manufacture of elastically bent crystals and multilayer mirrors, and selective photodevices for the VUV.

Hoover, Richard B.↗

Transport and Chemical Effects on Concurrent and Opposed-Flow Flame Spread at Microgravity

With support from a previous NASA grant, NAG3-161 1, the PI studied the effects of diluent type, the addition of sub-flammability-limit concentrations of combustible gases, and the effects of concurrent buoyant flow on flame spread processes. The results of these studies are reported and directions for the current grant outlined. Most experiments were conducted in a 20 liter combustion chamber. Exactly the same apparatus was used for 1 g and microgravity tests. The effect of inert gases He, Ar, N2, CO2 and SF6 on flame spread were tested since they provide a variety of radiative properties and oxygen Lewis numbers. CO and CH4 were used for the gaseous fuels in partially-premixed atmosphere tests, plus H2, C3H8 and NH3 for 1 g tests only. In most experiments 5 cm wide Kimwipe samples 15 cm long were used and were held by aluminum quenching plates. The samples were ignited by an electrically-heated Kanthal wire. The flame spread process was imaged via three video cameras and a laser shearing interferometer.

Honda, L. K.↗

Leonid's Particle Analyses from Stratospheric Balloon Collection on Xerogel Surfaces

Recovered from a stratospheric balloon above 20 km on 17-18 November 1998, at least eight candidate microparticles were collected and analyzed from low-density silica xerogel collection plates. Capture time at Leonids' storm peak was validated locally along the balloon trajectory by direct video imaging of meteor fluence up to 24/hr above 98% of the Earth's atmosphere. At least one 30 micron particle agrees morphologically to a smooth, unmelted spherule and compares most closely in non-volatile elemental ratios (Mg/Si, Al/Si, and Fe/Si) to compositional data in surface/ocean meteorite collections. A Euclidean tree diagram based on composition makes a most probable identification as a non-porous stratospherically collected particle and a least probable identification as terrestrial matter or an ordinary chondrite. If of extraterrestrial origin, the mineralogical class would be consistent with a stony (S) type of silicate, olivine [(Mg,Fe)2SiO4] and pyroxene [(Mg, Fe)Si!O3)--or oxides, herecynite [(Fe,Mg) Al2O4].

Noever, David↗

High-Speed PLIF Imaging of Hypersonic Transition over Discrete Cylindrical Roughness

In two separate test entries, advanced laser-based instrumentation has been developed and applied to visualize the hypersonic flow over cylindrical protrusions on a flat plate. Upstream of these trips, trace quantities of nitric oxide (NO) were seeded into the boundary layer. The protuberances were sized to force laminar-to-turbulent boundary layer transition. In the first test, a 10-Hz nitric oxide planar laser-induced fluorescence (NO PLIF) flow visualization system was used to provide wide-field-of-view, high-resolution images of the flowfield. The images had sub-microsecond time resolution. However these images, obtained with a time separation of 0.1 sec, were uncorrelated with each other. Fluorescent oil-flow visualizations were also obtained during this test. In the second experiment, a laser and camera system capable of acquiring NO PLIF measurements at 1 million frames per second (1 MHz) was used. This system had lower spatial resolution, and a smaller field of view, but the images were time correlated so that the development of the flow structures could be observed in time.

Danehy, P. M.↗

An Experimental Investigation of the Flow Structure of Supersonic Impinging Jets

An experimental investigation into the jet structure associated with sound production by a supersonic impinging jet is presented. Large plate impinging tones are investigated for a nozzle pressure ratio (NPR) of 4 and nozzle-to-plate spacings between 1 and 5 nozzle exit diameters, where NPR is equal to the ratio of the stagnation pressure to the pressure at the nozzle lip. Results from phase-locked shadowgraph and phase-averaged digital particle image velocimetry (DPIV) studies indicate that, during the oscillation cycle, the Mach disk oscillates axially, a well defined recirculation zone is created in the subsonic impingement region and moves toward the plate, and the compression and expansion regions in the outer supersonic flow move downstream, Sound appears to be generated in the wall jet at approximately 2.6R from the jet axis, where R is the nozzle exit radius. The oscillatory motion in the wall jet is the result of the periodic fluid motion in the near wall region.

Henderson, Brenda↗

Probing the Role of Multi-scale Heterogeneity in Graphite Electrodes for Extreme Fast Charging

Electrode-scale heterogeneity can combine with complex electrochemical interactions to impede lithium-ion battery performance, particularly during fast charging. This research investigates the influence of electrode heterogeneity at different scales on the lithium-ion battery electrochemical performance under operational extremes. We employ image-based mesoscale simulation in conjunction with a three-dimensional electrochemical model to predict performance variability in 14 graphite electrode X-ray computed tomography data sets. Our analysis reveals that the tortuous anisotropy stemming from the variable particle morphology has a dominating influence on the overall cell performance. Cells with platelet morphology achieve lower capacity, higher heat generation rates, and severe plating under extreme fast charge conditions. On the contrary, the heterogeneity due to the active material clustering alone has minimal impact. Our work suggests that manufacturing electrodes with more homogeneous and isotropic particle morphology will improve electrochemical performance and improve safety, enabling electromobility.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Laser Image Contrast Enhancement System

An optical image enhancement system provides improved image contrast in imaging of a target in high temperature surroundings such as a furnace. The optical system includes a source of vertically polarized light such as laser and a beam splitter for receiving the light and directing the light toward the target. A retardation plate is affixed to a target-facing surface of the beam splitter and a vertical polarizer is disposed along a common optical path with the beam splitter between the retardation plate and the target. A horizontal polarizer disposed in the common optical path, receives light passing through a surface of the beam splitter opposed to the target-facing surface. An image detector is disposed at one end of the optical path. A band pass filter having a band pass filter characteristic matching the frequency of the vertically polarized light source is disposed in the path between the horizontal polarizer and the image detector. The use of circular polarization, together with cross polarizers, enables the reflected light to be passed to the detector while blocking thermal radiation.

Robert L Kurtz↗

Angular scattering of protons through ultrathin graphene foils: Application for time-of-flight instrumentation

Space plasma instruments often rely on ultrathin carbon foils for incident ion detection, time-of-flight (TOF) mass spectrometry, and ionization of energetic neutral atoms. Angular scattering and energy loss of ions or neutral atoms in the foil can degrade instrument performance, including sensitivity and mass resolution; thus, there is an ongoing effort to manufacture thinner foils. Using new 3-layer graphene foils manufactured at the Los Alamos National Laboratory, we demonstrate that these are the thinnest foils reported to date and discuss future testing required for application in space instrumentation. We characterize the angular scattering distribution for 3–30 keV protons through the foils, which is used as a proxy for the foil thickness. We show that these foils are ~2.5–4.5 times thinner than the state-of-the-art carbon foils and ~1.6 times thinner than other graphene foils described in the literature. We find that the inverse relationship between angular scattering and energy no longer holds, reaffirming that this may indicate a new domain of beam–foil interactions for ultrathin (few-layer) graphene foils.

47 OTHER INSTRUMENTATION↗

In situ Visible Light and Thermal Imaging Data from a Laser Powder Bed Fusion Additive Manufacturing Process Co-Registered to X-ray Computed Tomography and Fatigue Data

This dataset is comprised of in situ sensing data collected during a laser-based powder bed fusion additive manufacturing process, as well as rasterized scan path information, post-build X-ray computed tomography (XCT), and fatigue test results. A total of 64 cylinders, approximately 15 mm in diameter and 102 mm tall, were printed out of stainless steel 316H on a Colibrium Additive Concept Laser M2 Series 5 machine. Parameters known to produce dense material were used to construct 56 of these cylinders, while the remaining 8 cylinders were printed with relatively high energy density parameters prone to producing keyhole pores. In addition, two spatter generation blocks were constructed upstream of the 64 cylinders such that ejecta produced during the melting of the spatter generators were stochastically seeded onto the 64 cylinders. Based on previous experiments, these spatter particles were theorized to produce stochastic lack-of-fusion pores. During the construction of the build, high-resolution images of reflected light in the visible spectrum were captured both before and after recoating for each print layer. Additionally, temporally integrated thermal imaging in the near infrared spectrum produced integrated sum and max images on a layerwise basis. The multimodal in situ data has been co-registered to the build plate coordinate system, allowing for identification of process anomalies (e.g., spatter particles) apparent in the two sensors. Following construction of the build, the cylinders were subjected to XCT to identify internal flaws, and the resulting data have also been registered to the build plate coordinate system. Finally, 60 of the 64 cylinders were machined into fatigue coupons conforming to ASTM E466 and subsequently subjected to either high- or -low-cycle fatigue testing. The results of the fatigue tests have also been included in the dataset, and the XCT data corresponded to the approximate location of the gauge sections of the machine fatigue specimen geometry.

42 ENGINEERING↗

Ionized interstellar froth in irregular galaxies

The warm interstellar medium of galaxies is a complicated place. It is often full of holes, neutral and ionized loops and shells, and diffuse ionized gas. Deep H alpha images of Magellanic-type irregular galaxies also reveal complex spatial structures consisting of loops and filaments in the interstellar gas outside of the boundaries of traditional HII regions. Researchers refer to these ionized structures as froth. Such structures could mark paths over which newly produced heavy elements are dispersed in irregular galaxies, and they could be the signatures of a feedback process related to star formation. In order to investigate the physical nature of the froth, researchers obtained narrow-band images and high and low dispersion spectra from Kitt Peak National Observatory (KPNO) and deep blue-passband plates from the Canada-France-Hawaii Observatory (CFHO).

Hunter, Deidre A.↗

Low-Current, Xenon Orificed Hollow Cathode Performance for In-Space Applications

An experimental investigation of the operating characteristics of 3.2-mm diameter orificed hollow cathodes was conducted to examine low current and low flow rate operation. Cathode power was minimized with an orifice aspect ratio of approximately one and the use of an enclosed keeper. Cathode flow rate requirements were proportional to orifice diameter and the inverse of the orifice length. The minimum power consumption in diode mode was 10-W, and the minimum mass flow rate required for spot-mode emission was approximately 0.08-mg/s. Cathode temperature profiles were obtained using an imaging radiometer and conduction was found to be the dominant heat transfer mechanism from the cathode tube. Orifice plate temperatures were found to be weakly dependent upon the flow rate and strongly dependent upon the current.

Domonkos, Matthew T.↗

Cytoskeletal filament assembly and the control of cell spreading and function by extracellular matrix

This study was undertaken to analyze how cell binding to extracellular matrix produces changes in cell shape. We focused on the initial process of cell spreading that follows cell attachment to matrix and, thus, cell 'shape' changes are defined here in terms of alterations in projected cell areas, as determined by computerized image analysis. Cell spreading kinetics and changes in microtubule and actin microfilament mass were simultaneously quantitated in hepatocytes plated on different extracellular matrix substrata. The initial rate of cell spreading was highly dependent on the matrix coating density and decreased from 740 microns 2/h to 50 microns 2/h as the coating density was lowered from 1000 to 1 ng/cm2. At approximately 4 to 6 hours after plating, this initial rapid spreading rate slowed and became independent of the matrix density regardless of whether laminin, fibronectin, type I collagen or type IV collagen was used for cell attachment. Analysis of F-actin mass revealed that cell adhesion to extracellular matrix resulted in a 20-fold increase in polymerized actin within 30 minutes after plating, before any significant change in cell shape was observed. This was followed by a phase of actin microfilament disassembly which correlated with the most rapid phase of cell extension and ended at about 6 hours; F-actin mass remained relatively constant during the slow matrix-independent spreading phase. Microtubule mass increased more slowly in spreading cells, peaking at 4 hours, the time at which the transition between rapid and slow spreading rates was observed. However, inhibition of this early rise in microtubule mass using either nocodazole or cycloheximide did not prevent this transition. Use of cytochalasin D revealed that microfilament integrity was absolutely required for hepatocyte spreading whereas interference with microtubule assembly (using nocodazole or taxol) or protein synthesis (using cycloheximide) only partially suppressed cell extension. In contrast, cell spreading could be completely inhibited by combining suboptimal doses of cytochalasin D and nocodazole, suggesting that intact microtubules can stabilize cell form when the microfilament lattice is partially compromised. The physiological relevance of the cytoskeleton and cell shape in hepatocyte physiology was highlighted by the finding that a short exposure (6 hour) of cells to nocodazole resulted in production of smaller cells 42 hours later that exhibited enhanced production of a liver-specific product (albumin). These data demonstrate that spreading and flattening of the entire cell body is not driven directly by net polymerization of either microfilaments or microtubules.(ABSTRACT TRUNCATED AT 400 WORDS).

NASA Discipline Cell Biology↗