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DOE OSTI2025

Mapping Rare Earths and Toxics in E-Waste via Hyperspectral Imaging and Machine Learning

Electronic waste (e-waste) presents a mounting challenge to environmental sustainability due to its complex composition, which includes high-value rare earth elements, hazardous organic compounds, and non-recyclable plastics. Accurate and scalable material classification is essential for enabling efficient resource recovery and safe recycling practices. This study introduces a confidence-aware classification pipeline that combines mid-infrared hyperspectral imaging (HSI), spectral angle mapping (SAM), and iterative machine learning to perform pixel-level material identification across e-waste devices. A curated spectral library encompassing artificial materials (e.g., plastic iron oxide, galvanized metals), minerals (e.g., allanite, hematite), and organic compounds (e.g., benzanthracene, toluene) was used to generate pseudo-labels, each assigned a confidence score based on SAM-derived spectral similarity. High-confidence samples from seven consumer electronics—digital cameras, keyboards, laptop fans, modems, motherboards, TV remotes, and speakers—were iteratively expanded and classified using models such as Support Vector Machine (SVM), Random Forest, Gradient Boosting Classifier, Partial Least Squares Discriminant Analysis (PLSDA) and Logistic Regression. The best-performing classifiers achieved macro F1 scores approaching 1.0. Results revealed widespread plastic content (dominated by plastic iron oxide), the presence of rare earth-bearing minerals like cerium-containing allanite, and pervasive detection of hazardous organics such as benzanthracene. Principal Component Analysis (PCA) visualizations and confusion matrices confirmed high separability and robust classification performance. This methodology enables precise, non-destructive, and scalable classification of heterogeneous e-waste streams. It supports automated, hazard-aware sorting in recycling workflows, facilitating selective recovery of critical materials and compliance with circular economy goals. The confidence-aware framework provides a foundation for real-time deployment in industrial settings, offering significant implications for smart e-recycling infrastructure and policy-driven material stewardship.

Circular economy↗

DOE OSTI2025

Measurements of the temperature and $E$-mode polarization of the cosmic microwave background from the full 500-square-degree SPTpol dataset

Using the full four-year SPTpol 500 deg 2 dataset in both the 95 and 150 GHz frequency bands, we present measurements of the temperature and E-mode polarization of the cosmic microwave background (CMB), as well as the E-mode polarization autopower spectrum (EE) and temperature-E-mode cross-power spectrum (TE) in the angular multipole range 50 < ℓ < 8000. We find the SPTpol dataset to be self-consistent, passing several internal consistency tests based on maps, frequency bands, bandpowers, and cosmological parameters. The full SPTpol dataset is well-fit by the ΛCDM model, for which we find H 0 = 70.48 ± 2.16 km s -1 Mpc -1 and Ω m = 0.271 ± 0.026, when using only the SPTpol data and a Planck-based prior on the optical depth to reionization. The ΛCDM parameter constraints are consistent across the 95 GHz-only, 150 GHz-only, TE-only, and EE-only data splits. Between the ℓ < 1000 and ℓ > 1000 data splits, the ΛCDM parameter constraints are borderline consistent at the ∼2σ level. This consistency improves when including a parameter A L , the degree of lensing of the CMB inferred from the smearing of acoustic peaks. When marginalized over A L , the ΛCDM parameter constraints from SPTpol are consistent with those from Planck. In conclusion, the power spectra presented here are the most sensitive measurements of the lensed CMB damping tail to date for roughly ℓ > 1700 in TE and ℓ > 2000 in EE.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2023

Search for e → τ charged lepton flavor violation at the EIC with the ECCE detector

The recently approved Electron-Ion Collider (EIC) will provide a unique new opportunity for searches of charged lepton flavor violation (CLFV) and other new physics scenarios. In contrast to the e ↔ μ CLFV transition for which very stringent limits exist, there is still a relatively large discovery space for the e → τ CLFV transition, potentially to be explored by the EIC. Here, with the latest detector design of ECCE (EIC Comprehensive Chromodynamics Experiment) and projected integral luminosity of the EIC, we find the τ-leptons created in the DIS process ep → τX are expected to be identified with high efficiency. A first ECCE simulation study, restricted to the 3-prong τ-decay mode and with limited statistics for the Standard Model backgrounds, estimates that the EIC will be able to improve the current exclusion limit on e → τ CLFV by an order of magnitude. As a result, the very high vertex resolution of the ECCE detector configuration plays a critical role in τ identification.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2021

Electropolymerized-molecularly imprinted polymers (E-MIPS) as sensing elements for the detection of dengue infection

Here, a straightforward in situ detection method for dengue infection was demonstrated through the molecular imprinting of a dengue nonstructural protein 1 (NS1) epitope into an electropolymerized molecularly imprinted polyterthiophene (E-MIP) film sensor. The key enabling step in the sensor fabrication is based on an epitope imprinting strategy, in which short peptide sequences derived from the original target molecules were employed as the main template for detection and analysis. The formation of the E-MIP sensor films was facilitated using cyclic voltammetry (CV) and monitored in situ by electrochemical quartz crystal microbalance (EC-QCM). Surface properties were analyzed using different techniques including atomic force microscopy (AFM), X-ray photoelectron spectroscopy (XPS), and polarization modulation-infrared reflection-adsorption (PM-IRRAS). The standard calibration curve (R = 0.9830) was generated for the detection of the epitope, Ac-VHTWTEQYKFQ-NH 2 , with a linear range of 0.2 to 30 μg/mL and detection limit of 0.073 μg/mL. A separate calibration curve (R = 0.9786) was obtained using spiked buffered solutions of dengue NS1 protein, which resulted in a linear range of 0.2 to 10 μg/mL and a detection limit of 0.056 μg/mL. The fabricated E-MIP sensor exhibited long-term stability, high sensitivity, and good selectivity towards the targeted molecules. These results indicated that the formation of the exact and stable cavity imprints in terms of size, shape, and functionalities was successful. In our future work, we aim to use our E-MIP sensors for NS1 detection in real-life samples such as serum and blood.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2021

Response of thermal and fast-ion transport to beam ion population, rotation and T e / T i in the DIII-D steady state hybrid scenario

The thermal and fast-ion transport properties of DIII-D steady-state hybrid discharges with normalized beta β N ≳ 3 are studied at low injected torque and an increased electron to ion temperature ratio T e / T i . Linear stability analysis performed with the TGLF turbulent code indicates that a high-k mode is usually dominant at smaller radii, whereas a low-k mode is usually dominant at larger radii in these plasmas. A reduction in the net injected torque from 8.6 to 4.3 N-m leads to reduced E × B shear and hence, an enhanced turbulence that was observed on the Doppler backscattering diagnostic and was also computed with TGLF. As T e / T i in the core was increased from 0.57 to 0.66 by adding electron cyclotron current drive (ECCD) to these plasmas, higher levels of transport are observed with increased high-k modes indicated by TGLF. The fast-ion transport level varied over an order of magnitude in these discharges depending on whether Alfvén eigenmodes, fishbones, or no instabilities were observed. Hybrid plasmas with fishbones have decreased fast-ion transport, compared to plasmas with Alfvén eigenmodes, since they are resonant with a smaller portion of phase space and their resonance is farther from the wall. This reduction in fast-ion transport with ECCD mitigates the increase in turbulent transport, resulting in higher performance than expected during strong electron heating. Similarly, the lowest fast-ion transport was observed in the low torque plasma, which also led to better than expected performance at this torque value. Finally, the thermal and fast-ion transport changes observed as the torque/rotation and T e / T i are varied indicate possible methods for transferring this scenario to a reactor.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2021

First evidence of dominant influence of E × B drifts on plasma cooling in an advanced slot divertor for tokamak power exhaust

Addressing power exhaust in tokamaks is presently recognized as one of the major remaining open issues for the development of fusion reactors. At the forefront of this endeavor is the effort to develop an advanced divertor by maximizing dissipation of plasma power and momentum inside the divertor. Here, we demonstrate, for the first time, that the electromagnetic (E × B) drifts exert a key influence on plasma and gas dynamics in a new advanced slot divertor in the DIII-D tokamak, named the small angle slot (SAS). SAS leverages the effect of drifts to achieve a highly dissipative divertor with electron temperature T e ≲ 10 eV over a wide range of plasma densities, for ion B × ∇B away from the divertor, as used for advanced tokamak operation on DIII-D. Modeling with the SOLPS-ITER code shows that for this drift direction, the E × B flow carries particles toward the outer common flux region (CFR) via the private flux region (PFR), reinforcing neutral recycling and enhancing divertor dissipation. In contrast, for the opposite field direction, the E × B flow carries particles away from the outer CFR into the PFR, offsetting the anticipated SAS geometric effects. Furthermore, this finding is an important step in the understanding of the behavior of advanced divertors for achieving a power exhaust solution for fusion reactors.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2022

E × B flow driven electron temperature bifurcation in a closed slot divertor with ion B × ∇ B away from the X-point in the DIII-D tokamak

An electron temperature bifurcation is observed in the small angle slot divertor, which has been developed to enhance neutral cooling across the divertor target by coupling a closed slot structure with appropriate target shaping. Experiments in the DIII-D tokamak and associated SOLPS-ITER modeling with full drifts find a strong interplay between drifts and divertor geometry on divertor dissipation. The coupling of divertor geometry and drift flows can strongly affect the path towards divertor detachment onset as the plasma density is raised. With the strike point on the inner slanted surface and ion B × ∇B away from the magnetic X-point, bifurcative transitions were observed with sharp decrease of T e towards detachment onset both experimentally and computationally. This differs from the situation for the open divertor where the T e cliff was only observed for ion B × ∇B towards the X-point. SOLPS-ITER modeling with full drifts demonstrates that the magnitude of the E × B drift flow is comparable with the main plasma flow. The reversal of both the poloidal and radial E × B flows near the strike point leads to rapid density accumulation right near the separatrix, which results in bifurcative step transition of divertor conditions with cold plasma across the entire divertor target plate. Furthermore, these results indicate that the interplay between geometry and drifts should be fully taken into account in future fusion reactor divertor designs.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2023

Measurement of the $\textit{B}(\textit{E}2 ↑)$ strengths of 36 Ca and 38 Ca

In this work, the $B(E2, 0^+_1 → 2^+_1)$ strengths of 36 Ca and 38 Ca are measured to be 131(20) $e^2\text{fm}^4$ and 101(11) $e^2\text{fm}^4$, respectively. The $\textit{B}(\textit{E}2)$ value for 36 Ca required a measurement of the p/γ branching ratio because the 2 + state is proton unbound. This branching ratio is $B_p$=0.087(8). These $\textit{B}(\textit{E}2)$ and branching-ratio values can be reproduced in the shell-model with the ZMB2 interaction, an interaction that predicts the $\textit{Z} = 20 \textit{sd}$-shell closure is incomplete with large proton pf-shell occupancies in the ground state. These occupancies are at odds with other shell-model and energy-density-functional calculations of 36 Ca. New data are used to provide an update on constraints of the density dependence of the symmetry energy through mirror charge-radii differences as well as to help reduce uncertainties of the astrophysical important 35 K(p,γ) reaction.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2023

Measurement of the helicity asymmetry $${\mathbb {E}}$$ for the $$\vec {\gamma }\vec {p} \rightarrow p \pi ^0$$ reaction in the resonance region: The CLAS Collaboration

Abstract The double-spin-polarization observable $${\mathbb {E}}$$ E for $$\vec {\gamma }\vec {p}\rightarrow p\pi ^0$$ γ → p → → p π 0 has been measured with the CEBAF Large Acceptance Spectrometer (CLAS) at photon beam energies $$E_\gamma $$ E γ from 0.367 to $$2.173~\textrm{GeV}$$ 2.173 GeV (corresponding to center-of-mass energies from 1.240 to $$2.200~\textrm{GeV}$$ 2.200 GeV ) for pion center-of-mass angles, $$\cos \theta _{\pi ^0}^{c.m.}$$ cos θ π 0 c . m . , between $$-$$ - 0.86 and 0.82. These new CLAS measurements cover a broader energy range and have smaller uncertainties compared to previous CBELSA data and provide an important independent check on systematics. These measurements are compared to predictions as well as new global fits from The George Washington University, Mainz, and Bonn-Gatchina groups. Their inclusion in multipole analyses will allow us to refine our understanding of the single-pion production contribution to the Gerasimov-Drell-Hearn sum rule and improve the determination of resonance properties, which will be presented in a future publication.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2023

Mobility Energy Productivity and Equity: E-Bike Impacts for Low-Income Essential Workers in Denver

New mobility technologies such as electrified and shared mobility, combined with polices and incentive programs, are emerging to help address sustainability and equity issues in transportation planning. However, it can be difficult to understand the impacts of novel mobility trends and emerging modes on energy-efficient access. This is owing to a lack of (1) open-source tools enabling rapid data collection, and (2) open-source metrics that consider multimodal, multiactivity access and mobility within the contexts of sustainability and equity. Here, this paper addresses the topic of improving evaluation of transportation modes and incentive programs by integrating an open-source platform for tracking human travel data—the Open Platform for Agile Trip Heuristics (OpenPATH)—with a mobility metric that quantifies the efficiency of a region’s transportation system: Mobility Energy Productivity (MEP). Integration is demonstrated in the context of pilot programs in Colorado, where low-income essential workers were provided with electric bikes (e-bikes). OpenPATH-informed MEP calculations showed that several locations in downtown Denver provided comparable time-, cost-, and energy-efficient access to opportunities using e-bikes compared with driving. Additionally, providing e-bikes to low-income essential workers was found to be meaningful, as they utilized e-bikes the most to commute, despite driving still being their most utilized mode and the mode with highest MEP scores in Denver. We show how data collected from open-source tools coupled with robust metrics such as MEP can help evaluate the impacts of emerging mobility options. This could support developing policies to incentivize novel modes to achieve greater levels of sustainable, equitable, and efficient access.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

NASA NTRS1978

E region coupling effects on the Perkins spread F instability

The Perkins instability theory for mid-latitude spread F is generalized to include the effects of the E region on growth rates. A three-layer model, representing the E region, the F region, and a resistive layer of low Pedersen conductivity which separates them, is developed. The E region Pedersen current has a stabilizing effect on the perturbed F region, thereby reducing the growth rate of the instability. For spread F onset on September 17, 1974, the maximum growth rate is found to be only one third of the Perkins growth rate. The resistive layer reduces the electric field perturbation in the E region for short wavelengths but has little effect for long wavelengths.

Klevans, E. H.↗

NASA NTRS1978

Temperate zone sporadic-E maps /f/0/E/s/ greater than 7 MHz/

Three maps are presented of f(0) sporadic-E greater than 7 MHz for temperate zones. During map preparation it was assumed that: (1) the geographical area would be between plus and minus 60 deg geomagnetic latitude, excluding the equatorial zone, (2) the maps would be for f(0) sporadic-E greater than 7 MHz, (3) sunspot cycle variation would be ignored, (4) one map would represent the peak sporadic-E period with a discontinuity at the geographic equator, (5) one map would represent non-peak periods with a discontinuity at the geographic equator, (6) one map would represent all twelve months with no equatorial discontinuity, and (7) previously determined coefficients for median and upper decile f(0) sporadic-E would be extrapolated to 7 MHz.

Smith, E. K.↗

NASA NTRS1986

The laboratory millimeter-wave spectrum of methyl formate in its ground torsional E state

Over 250 rotational transitions of the internal rotor methyl formate (HCOOCH3) in its ground v(t) = 0 degenerate (E) torsional substate have been measured in the millimeter-wave spectral region. These data and a number of E-state lines identified by several other workers have been analyzed using an extension of the classical principal-axis method in the high barrier limit. The resulting rotational constants allow accurate prediction of the v(t) = 0 E substate methyl formate spectrum below 300 GHz between states with angular momentum J not greater than 30 and rotational energy of not more than 350/cm. The calculated transition frequencies for the E state, when combined with the results of the previous analysis of the ground-symmetric, nondegenerate state, account for over 200 of the emission lines observed toward Orion in a recent survey of the 215-265 GHz band.

Plummer, G. M.↗

NASA NTRS1995

Global equatorial ionospheric vertical plasma drifts measured by the AE-E satellite

Ion drift meter observations from the Atmosphere Explorer E (AE-E) satellite during the period of January 1977 to December 1979 are used to study the dependence of equatorial (dip latitudes less than or equal to 7.5 deg) F region vertical plasma drifts (east-west electric fields) on solar activity, season, and longitude. The satellite-observed ion drifts show large day-to-day and seasonal variations. Solar cycle effects are most pronounced near the dusk sector with a large increase of the prereversal velocity enhancement from solar minimum to maximum. The diuurnal, seasonal, and solar cycle dependence of the logitudinally averaged drifts are consistent with results from the Jicamarca radar except near the June solstice when the AE-E nighttime downward velocities are significantly smaller than those observed by the radar. Pronounced presunrise downward drift enhancements are often observed over a large longituudinal range but not in the Peruvian equatorial region. The satellite data indicate that longitudinal variations are largest near the June solstice, particularly near dawn and dusk but are virtually absent during equinox. The longitudinal dependence of the AE-E vertical drifts is consistent with results from ionosonde data. These measurements were also used to develop a description of equatorial F region vertical drifts in four longitudinal sectors.

Fejer, B. G.↗

NASA NTRS2005

What is the Water (OH) Content of the E Asteroids?

Attempts to match the E asteroids with enstatite-rich meteorites universally conclude that the aubrites or enstatite chondrites are natural candidates, and accordingly conclude that E asteroids as a class are very water-poor. Accordingly, the highly reduced nature of typical enstatite-rich meteorites suggests that aqueous alteration was an improbable process on any E asteroid. However, there are spectroscopic observations of several E-class asteroids that suggest the presence there of hydrated phases. Examination of the Kaidun meteorite reveals the true situation.

Zolensky, M. E.↗

NASA NTRS2005

Sporadic E Morphology from GPS-CHAMP Radio Occultation

The scintillations of phase and amplitude in terms of signal-to-noise ratio (SNR) of the GPS radio occultation signal are caused by thin ionization layers. These thin irregular electron density layers in the E region ionosphere are often called sporadic E (Es). For a monthly retrieval of Es morphology we use the variances of the phase and SNR fluctuations of worldwide ~6000 GPS/CHAMP occultations in the E region. The Es climatology is studied globally with the SNR and phase variances in terms of monthly zonal means, seasonal maps, and diurnal and long-term variations. The zonal mean variances reveal strong, extended Es activities at summertime midlatitudes but weak, confined activities in wintertime high latitudes, peaking at ~105 km. Global maps at 105-km altitude show clear dependence of Es activities on the geomagnetic dip angle, where the summertime midlatitude Es occurs mostly at dip angles of 30 deg. - 60 deg. and the wintertime high-latitude enhancement occurs mostly at dip angles greater than 80 deg. The midlatitude Es variances exhibit a strong semidiurnal variation with peak hours near 0800 1000 and 2000 local solar time, respectively. The peak hours are delayed slightly with decreasing height, suggesting influences from the semidiurnal tide. To provide more insights on the observed SNR and phase variances, we model radio wave propagation for the CHAMP observing geometry under several perturbed cases in the E region ionosphere. The model simulations indicate that the SNR variance has the maximum response to Es perturbations at vertical wavelengths of 1.2 km, whereas the phase response maximizes at ~2 km (for the 1-s variance analysis). The characteristic scale depends little on the truncation time used in the SNR variance analysis, but it increases with the truncation time for the phase variances. Initial studies show that reasonable global Es morphology can be produced on a monthly and seasonal basis with the CHAMP one-antenna occultations. Better results from other existing and upcoming GPS occultation missions are anticipated in future studies, and they will significantly improve our understanding of this important phenomenon.

signal to noise ration (SNR)↗

NASA NTRS2011

Subsurface Emission Effects in AMSR-E Measurements: Implications for Land Surface Microwave Emissivity Retrieval

An analysis of land surface microwave emission time series shows that the characteristic diurnal signature associated with subsurface emission in sandy deserts carry over to arid and semi-arid region worldwide. Prior work found that diurnal variation of Special Sensor Microwave/Imager (SSM/I) brightness temperatures in deserts was small relative to International Satellite Cloud Climatology Project land surface temperature (LST) variation and that the difference varied with surface type and was largest in sand sea regions. Here we find more widespread subsurface emission effects in Advanced Microwave Scanning Radiometer-EOS (AMSR-E) measurements. The AMSR-E orbit has equator crossing times near 01:30 and 13 :30 local time, resulting in sampling when near-surface temperature gradients are likely to be large and amplifying the influence of emission depth on effective emitting temperature relative to other factors. AMSR-E measurements are also temporally coincident with Moderate Resolution Imaging Spectroradiometer (MODIS) LST measurements, eliminating time lag as a source of LST uncertainty and reducing LST errors due to undetected clouds. This paper presents monthly global emissivity and emission depth index retrievals for 2003 at 11, 19, 37, and 89 GHz from AMSR-E, MODIS, and SSM/I time series data. Retrieval model fit error, stability, self-consistency, and land surface modeling results provide evidence for the validity of the subsurface emission hypothesis and the retrieval approach. An analysis of emission depth index, emissivity, precipitation, and vegetation index seasonal trends in northern and southern Africa suggests that changes in the emission depth index may be tied to changes in land surface moisture and vegetation conditions

Galantowicz, John F.↗

NASA NTRS2016

A New Operational Snow Retrieval Algorithm Applied to Historical AMSR-E Brightness Temperatures

Snow is a key element of the water and energy cycles and the knowledge of spatio-temporal distribution of snow depth and snow water equivalent (SWE) is fundamental for hydrological and climatological applications. SWE and snow depth estimates can be obtained from spaceborne microwave brightness temperatures at global scale and high temporal resolution (daily). In this regard, the data recorded by the Advanced Microwave Scanning Radiometer-Earth Orbiting System (EOS) (AMSR-E) onboard the National Aeronautics and Space Administration's (NASA) AQUA spacecraft have been used to generate operational estimates of SWE and snow depth, complementing estimates generated with other microwave sensors flying on other platforms. In this study, we report the results concerning the development and assessment of a new operational algorithm applied to historical AMSR-E data. The new algorithm here proposed makes use of climatological data, electromagnetic modeling and artificial neural networks for estimating snow depth as well as a spatio-temporal dynamic density scheme to convert snow depth to SWE. The outputs of the new algorithm are compared with those of the current AMSR-E operational algorithm as well as in-situ measurements and other operational snow products, specifically the Canadian Meteorological Center (CMC) and GlobSnow datasets. Our results show that the AMSR-E algorithm here proposed generally performs better than the operational one and addresses some major issues identified in the spatial distribution of snow depth fields associated with the evolution of effective grain size.

passive microwave↗