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At least 487 records · Page 27

Experimental Observations of Damage States in Unnotched and Notched 3D Orthogonal Woven Coupons Loaded in Tension

This paper describes a series of unnotched and notched tensile tests on two 3D orthogonal woven architectures loaded in the warp direction. Dogbone specimens were used for the unnotched tests, and open-hole specimens were used for the notched tests. For each architecture and test type, two specimens were loaded under monotonic displacement control to failure, and two specimens were incrementally loaded to failure in five steps. X-ray computed tomography (CT) was used to characterize the woven architecture and defects on each specimen prior to testing. Digital image correlation (DIC) images were obtained from both sides of the specimen throughout the loading and unloading. For the incremental tests, X-ray CT was used to document the damage progression after each load increment. The results for both architectures and test specimens followed a similar pattern where matrix cracks formed perpendicular to the load direction and were primarily located between the stacks of warp tows. Two-piece failure path always occurred perpendicular to the loading direction, along the through-thickness segments of the Z-tows. The combination of stress concentrations due to the specimen geometry, weave geometry, and cut tows created stress concentrations that appear to initiate failure.

Woven materials↗

Effects of Cooling Holes on SiC/SiC Strength and Durability

Ceramic Matrix Composites (CMCs) such as SiC/SiC are currently operating in select high temperature components of turbine engines. When these materials are implemented in components at higher operating temperatures, film cooling may be necessary. Film cooling requires holes to be fabricated at appropriate locations within these components. This study examines the effect of cooling holes on SiC/SiC composite strength and durability. Mechanical test data on specimens with multiple holes is reported for isothermal conditions at room and elevated temperatures. Tools such as Digital Image Correlation (DIC) and Acoustic Emission (AE) are used to monitor strain and cracking upon loading.

Ceramic matrix composite↗

High-Temperature Mechanical Tensile Testing of Unidirectional Sic/Sic Composites Using A Versatile Lamp Furnace

Silicon carbide (SiC) based ceramic matrix composites (CMCs) are of interest for high-temperature structural applications, including use in turbine engine components. To understand damage mechanisms and predict durability of these systems, in-depth knowledge of their behavior at ambient and high temperatures is necessary. A method for high temperature testing of SiC/SiC minicomposite specimens up to 1500oC in both tensile fast fracture and creep conditions to investigate their thermomechanical behavior will be presented. This method utilizes a novel radiation heat furnace, equipped with infrared lamps with ellipsoidal reflectors, to heat the specimen at the furnace center in user-defined atmospheres. The housing structure of the lamps allows for observation of the specimen during testing using optical methods and for conducting other experimental studies. The goal is to employ nondestructive health monitoring techniques in-situ, including acoustic emission (AE), electrical resistance (ER), and digital image correlation (DIC) to evaluate damage initiation and evolution in the minicomposite specimens during tensile testing. Results from mechanical testing and nondestructive techniques will be presented. Electron microscopy and X-ray micro-computed tomography were used to further characterize specimen damage after testing.

Aeronautics↗

High-Cycle Fatigue Behavior of SiC-based Ceramic Matrix Composites (CMCs) at High Temperatures

High-cycle fatigue (HCF) behavior of a melt-infiltrated, pre-preg SiC/SiC ceramic matrix composite (CMC) was investigated using dogbone tensile specimens without and with simulated cooling holes at 1500 and 2400 °F. The CMC material used for this study was fabricated by GE Aviation and had a ply configuration of [0/90/0]3. HCF tests were conducted with an R-ratio of 0.6 and a cyclic frequency of 30 Hz. Runout in HCF was defined as 30 million cycles. Monotonic tensile tests were conducted at room temperature (RT) on as-received CMC specimens and on runout HCF specimens to determine residual tensile strengths. Digital image correlation (DIC) and acoustic emission (AE) techniques were used to monitor the initiation and progression of damage in RT tensile tests on specimens with and without holes. Microscopy was performed on the polished edge of specimens without cooling holes and on the polished face of specimens with cooling holes that were tested in HCF and achieved runout. Comparisons were made with baseline specimens. Fractography was performed to examine the fracture surfaces of samples that failed under different loading conditions.

Ceramic Matrix Composites↗

Advances in Integrally Formed Metallic Structures

NASA Langley Research Center (LaRC) is applying flow forming technology to aerospace aluminum alloys for the manufacture of integrally stiffened cylinders that meet aircraft fuselage or launch vehicle specifications. High-strength 2xxx series alloys, in various temper/product form conditions, are being compared with medium-strength, very formable AA 6061 as the benchmark. Screening of candidate materials traditionally relies on empirical forming trials, but more recently on metrics derived from constant nominal strain rate tensile testing. In this work, the established hierarchy of formability metrics is adopted as the baseline; tensile area reduction, work hardening exponent, and modulus of resilience. The suite of metrics can be expanded based on phenomenological and mechanistic considerations of plastic flow instabilities to incorporate anisotropy ratio, rate of work hardening, and dynamic strain aging effects. Separate research thrusts at LaRC are aimed at formulating a protocol for scalable production of fully formed, defect-free components: 1) quantifying the extended set of formability metrics from constant and jump strain rate tensile tests with digital image correlation (DIC); 2) using statistically designed experiments on a vertical spin/flow forming facility (WF VUD-600®) to isolate the effect of convenient process variables, such as axial feed rate and thickness reduction; and 3) predicting the effect of feed ratio (roller translation relative to mandrel rotation speeds) on material response via process modeling using the DEFORM® simulation software. Current results will be discussed in terms of correlating intrinsic material properties with the bulk workability characteristics to successfully fabricate cylinders with complex cross-sections.

Aluminum↗

Applications and Development Work for Digital Image Correlation Using High Speed Cameras

NASA, Army, and industry partners are working to advance optical measurement techniques used in highly dynamic rocket engine and missile test environments. This allows for direct component data collection during test and flight environments, significantly reduced analysis time, and associated cost savings. Digital Image Correlation (DIC) uses calibrated stereo cameras to collect three-dimensional (3-D) displacements, strains, and acceleration data by referencing a stochastic speckle pattern applied to the test object. These optical measurement techniques provide significantly improved data resulting in better performance predictions, model validation, and information about components during hot-fire tests and test flights.

Rachel Paden↗

Simulating High Energy Dynamic Impact of IM7/PEKK Continuous Fiber Laminated Thermoplastic Composite using Open Hole Coupon Experiments

The use of advanced thermoplastic composites (TPC) for structural applications in the aerospace and automotive industries has grown increasingly popular due to their high performance, high manufactured part output, and sustainability. Enhancing verification simulations of the progressive failure in TPCs at the coupon scale is needed to better validate advanced composite material models at larger length scales, such as element level panels. MAT_213, a tabulated composite material model, has been applied to simulate high velocity dynamic impact (HEDI) and is integrated in the LS-DYNA explicit finite element (FE) software. Previous efforts using MAT_213 have calibrated HEDI simulated failures with experimental data. Traditionally simulations have relied on a structured mesh to represent quasi-isotropic panels. For this study, a continuous fiber unidirectional tape, IM7/PEKK, was analyzed through a series of verification studies of notched laminate coupons, then validation analyses of quasi-isotropic panels under HEDI were compared with experimental data. Experiments using unidirectional TPC were performed to obtain tabulated stress vs strain curves using Digital Image Correlation (DIC) for input into MAT_213. Next, notched coupon experiments were used as an intermediate step to calibrate the damage and failure behavior in MAT_213. Lastly, investigations into differences between HEDI simulations using a fiber aligned mesh were compared with experimental failure patterns and damage sizes. The use of experimentally generated material behavior along with selective mesh layout improved HEDI predictions with minimal material parameter calibration.

Polymer matrix composites↗

An Overview of Nuclear Thermal Rocket Element Environmental Simulator (NTREES) Capabilities, Upgrades, and Overlaps in Advanced Material Testing Areas

The Nuclear Thermal Rocket Element Environmental Simulator (NTREES) was designed to perform non-nuclear testing of nuclear thermal rocket (NTR) fuel elements and materials. NTREES can simulate the thermal hydraulic environment within the reactor of an NTR and has been leveraged to provide data on the thermochemical, thermomechanical and thermohydraulic performance of components and materials. Active upgrades to the NTREES facility include installing a DC power supply for DC powered joule heating, a supply gas chiller for a cryogenically cool gas supply, gas pre-heaters with sample holders for testing samples too small to be inductively heated by bathing them in hot gas, and a high temperature digital image correlation (DIC) capability for measuring high temperature strains real time. In addition to NTR testing, given the commonality of high enthalpy flow environments between the reactor of an NTP engine and the aerothermal heating of high-speed flight, the unique capabilities of NTREES to provide high temperature gas flows at high pressure without combustion or electrode spallation byproducts may lend itself to additional usage of the facility beyond the original intent.

Michael P Schoenfeld↗

Forensic Determination of Residual Stresses from Fracture Surfaces

Forensic engineering - the scientific examination and analysis of failed structures and parts relating to their failure or cause of damage. Real advances in experimental mechanics require innovative theoretical and analytical thinking to go with innovative capabilities. For example, taking full field data (e.g., DIC) and treating it like discrete data (strain gauge) misses a wonderful opportunity.

36 MATERIALS SCIENCE↗

Rapid Field Measurement of Dissolved Inorganic Carbon Based on CO{sub 2} Analysis

Dissolved inorganic carbon (DIC) is commonly measured in water and is an important parameter for understanding carbonate equilibrium, carbon cycling, and water-rock interaction. While accurate measurements can be made in the analytical laboratory, we have developed a rapid, portable technique that can be used to obtain accurate and precise data in the field as well.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

MECHANICAL PROPERTIES AND MICROSTRUCTURAL CHARACTERIZATION OF A MULTILAYERED MULTIPASS FRICTION STIR WELD IN STEEL

Multilayered multipass friction stir welding (MM-FSW) makes it possible to use FSW to fabricate thick-section structures. In this work, MM-FSW was demonstrated on a high strength low alloy steel; ASTM A572 Grade 50. Three steel plates with thicknesses of 0.18", 0.18", 0.24" respectively were stacked and friction stir welded together to form a 0.6" thick welded structure. The welded plate was sectioned into rectangular bars transverse to the weld direction for tensile testing to evaluate mechanical properties. Digital image correlation (DIC) was employed to map the local strain fields during tensile testing. The initial failure was found to occur simultaneously at the bottom and middle layers away from the weld zone. The top layer failed last in the base metal. The failure locations were consistent among different samples tested. Also, Charpy V-notch impact tests were conducted for weld metal, heat affected zone, and the base metal at each layer as a function of temperature. The weld microstructures were characterized using optical and electron microscopy and micro-hardness mapping.

Lim, Yong Chae↗

Rehabilitation of notch damaged steel beam using a carbon fiber reinforced multiphase-matrix composite

The retrofit of notch damaged steel beams is investigated via the experimental testing of nine wide-flange steel beam specimens and finite element simulation. Three notch configurations representing various damage levels were identified, and the beam specimens were retrofitted using CFRP laminates and a recently developed polymeric matrix composite - CarbonFlex - that exhibits superior energy dissipation and ductility properties, where the peak-load deflections were between 49.4% and 65.2% higher using the CarbonFlex-retrofitted beams. The results are attributed to the substantially higher damage tolerance capability of CarbonFlex than conventional CFRP. Finite element models were developed to investigate the damage processes and strain/ stress distributions near the notch tips. The numerical results match closely with the experimentally determined load-deflection curves and the strain fields obtained by the digital imaging correlations (DIC) system. Both experimental and numerical results clearly indicate the effectiveness of CarbonFlex, as a candidate retrofitting material, to retrofit damaged steel structures. Lastly, the micro-mechanisms by which CarbonFlex could sufficiently sustain a significant amount of the peak strength at large displacement ductility values are discussed with the aid of scanning electron microscopy (SEM) pictures.

Zhou, HongYu↗

Controlling the distribution of microbially induced calcite precipitation in the subsurface

Microbially induced calcite precipitation (MICP) has gained interest as an environmentally friendly method for a number of subsurface applications, including consolidation of granular materials, modification of permeability, metal and radionuclide immobilization, self-healing of concrete, etc. MICP relies on microorganisms that when provided with appropriate nutrients create chemical conditions conducive to calcite precipitation. A major challenge is controlling and predicting spatial distribution of precipitates, whether the target be uniform or nonuniform (e.g., in specific strata or locations) deposition. The spatial distribution depends on calcite precipitation kinetics, the kinetics of the biological and chemical reactions that generate the required Ca2+ and carbonate, locations and phase association of the microbial catalyst, and timing of the arrival of amendments introduced into the medium; the latter depends on hydraulic boundary conditions and medium properties (porosity, permeability). We present results from a field experiment where we sought to induce uniform precipitation relying only on indigenous microorganisms and calcium within an approximately 3 meter thick saturated zone between two wells located 4 meters apart. We employed a continuous recirculation design; water extracted from the downgradient well was amended with urea and molasses and re-injected into the upgradient well for 12 days and the aqueous chemistry and microbiology was monitored for 419 days. Measurements of substrates and products, and isotopic data for DIC all indicated desired reactions were stimulated within the zone and downstream, during active recirculation and afterward. The results could be reasonably simulated by postulating that the recirculation resulted in homogeneous aqueous geochemistry within the entire zone, that a metabolic lag time persisted during the recirculation period, and that native ureolytic microorganisms were all attached.While alternative scenarios cannot be ruled out, the data and model support that spatial distribution of urolytic calcite precipitation can be manipulated by engineering design, although still constrained by site hydrogeology.

58 GEOSCIENCES↗

A Novel Decentralized PWM Interleaving Technique for Ripple Minimization in Series-Stacked DC-DC Converters: Preprint

Cascaded dc-dc converters are commonly used in applications where distributed energy sources or loads are connected to elevated voltage levels for power transfer. In such systems, it is advantageous to minimize the ripple on the bus current and voltage by proper phase shifting of the pulse-width modulation (PWM) pulses among the converters via a method known as interleaving. Existing approaches use either a centralized controller or separate communication lines among the stacked converters to control their relative PWM switch transitions. The key drawbacks are that these methods entail significant wiring, the central controller acts as a single point of failure, and implementation on very large numbers of units is impractical. In this paper, we introduce a decentralized interleaving control (DIC) strategy that acts on local current measurements at every converter and achieves communication-free PWM interleaving among the series-stacked converters. The proposed controller is simple in structure and is shown to converge asymptotically to the interleaved state irrespective of clock drifts among the digital signal processors. Experimental results are provided for a system of five series-connected converters showing a 10 times reduction in the current ripple compared to normal operation.

41 EE - Solar Energy Technologies Office (EE-4S)↗

Baseline Graphite Characterization

Presentation will include baseline graphite characterization information, such as purpose and results, baseline property measurements, baseline graphite characterization method, baseline progress, split disc tensile strength: ASTM Tensile Strength Alternative, Identification of proper split disk fracture, baseline graphite ASTM D8289, horizontal orientation, digital image correlation, and DIC Analyzation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Bare Fiber Bragg Gratings embedded into concrete buffer Supercontainer concept for nuclear waste storage [ANIMMA--2015-IO-337]

Nuclear power plants have been generating electricity for more than 50 years. In Belgium, 55% of the current energy supply comes from nuclear power. Providing for the safe storage of nuclear waste, including spent fuel (SF) and vitrified high level radioactive waste (HLW), remains an important challenge in the life cycle of nuclear fuel. In this context, the Belgian Agency for Radioactive Waste and Enriched Fissile Materials (ONDRAF/NIRAS) is investigating a reference conceptual design called the Supercontainer (SC) for the packaging of SF and HLW. This conceptual design is based on a multiple-barrier system consisting of a hermetically-sealed carbon steel overpack and a surrounding highly-alkaline concrete buffer. The first one is developed to retain the radionuclides. The two main functions of the buffer are (a) to create a high pH environment around the carbon steel overpack in order to passivate the metal surface and so to slow down the corrosion propagation during the thermal phase and (b) to provide a radiological shielding during the construction and the handling of the Supercontainer. A recent test has been performed to investigate the feasibility to construct the SC. This test incorporated several kinds of sensors including Digital Image Correlation (DIC), Acoustic Emission (AE), corrosion sensing techniques and optical fibers with and without fiber Bragg gratings (FBGs). In particular, several single-mode optical fibers with 4 mm long FBGs with different Bragg wavelengths and distributed along the optical fibers were used. For casting and curing condition monitoring, a number of gratings were incorporated inside the concrete buffer during the first stage of construction. Then other sensors were embedded near a heat source installed in the second stage to simulate the effects of heat generated by radioactive waste. The FBGs were designed to measure both temperature and strain effects in the concrete. To discriminate between these effects special packaging was used for some sensors that were installed very close to the unpackaged ones. Sensors placed in plastic tubes have reduced sensitivity to strain, while the ones inserted in metal tubes are only temperature sensitive and their readings can be directly compared with those obtained from thermocouples located nearby. In addition to monitoring temperature and strain behaviour, embedding also had as objective to determine the impact of the high alkaline environment on the silica fibers over a very long time. This article presents the preliminary results obtained with the different FBGs and provides recommendations for future improvement. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Secondary creep behavior of Zr-4 claddings under LOCA conditions

The thermo-mechanical behavior of Zircaloy-4 fuel rods under Loss-Of-Coolant Accident (LOCA) conditions in water cooled reactors is investigated. A custom experimental setup is dedicated to the high-temperature creep ballooning study of 90 mm long cladding samples. Creep tests were performed under an inert environment (argon), for temperatures from 750 to 850 C. degrees and internal pressures ranging from 1 to 5 MPa. During its operating life, Zr-4 cladding is submitted to oxidation and hydriding. These parameters strongly influence the creep behavior of Zirconium alloys at high temperatures. A first campaign on as-received Zr-4 was performed. Creep-rates are computed using 2-Dimensional Digital Image Correlation (2D-DIC) and are correlated to local temperatures measured using Near Infra-Red thermography. As-received Zr-4 behavior laws are determined using Finite Element Model Updating (FEMU). Norton exponents and activation energies are determined for thermal-mechanical conditions of the performed tests. The results show that the effect of applied stress on the Norton exponent is evidenced in the study for both α-phase and (α + β)-phase domains. The determined stress exponent magnitudes are very consistent with literature data depending on the thermomechanical test conditions. The activation energy parameter is very sensitive to the thermo-mechanical conditions and remains valid within a limited temperature and stress ranges to the authors' knowledge. The beginning of the (α + β)-phase domain is clearly identified with the activation energy increase. Finally, steady-state creep is accurately modeled depending on ballooning thermo-mechanical conditions.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

The PROMETRA program: plane strain tests on fresh and highly irradiated zircaloy-4, ZIRLO and M5 fuel claddings

In the framework of the PROMETRA program, clad hardening constitutive laws (stress-strain curves) have been already implemented in the SCANAIR code. These laws were derived from uniaxial hoop tensile tests performed on narrow machined ring samples. However, they do not reproduce the conditions of strain multi-axiality acting on cladding during a RIA (Reactivity-Initiated Accident) in a PWR. As a consequence, a new specimen called Plane Strain Tensile (PST) similar to the annular sample developed by Pennsylvania State University has been developed at CEA on a wider notched ring. It aims to accurately predict the cladding failure in more prototypical conditions, close to plane strain hoop tension in the middle of the gage section. This paper details the PST tests implementation and results in the framework of the PROMETRA program on fresh and irradiated claddings. The development of this test has led also to the development of a technique to measure local deformations in the gage section of the PST specimen using 2-D Digital Image Correlation (DIC). Tests performed on fresh Zircaloy-4 and on irradiated Zircaloy-4, M5 and ZIRLO specimens are analyzed relying of post-test examinations and finite element simulations. In the case of tests performed on irradiated Zry-4 and ZIRLO at 280 and 350 Celsius degrees, the presence of a hydride rim favors the crack nucleation on the outer surface. In this case, rupture nucleation occurs preferentially in the vicinity of notches. Such tests are not representative of the rupture of a cladding subjected to plane strain loading. Nevertheless, they give a good representation of the initiation of rupture observed during RIA on irradiated cladding, resulting in a hydride damage. Zry-4 specimens tested at 480 Celsius degrees and M5TM at 280 and 350 C. degrees result in a ductile fracture nucleation in the center of the specimen. This rupture is prototypical of a ductile rupture of an irradiated specimen subjected to a plane strain loading. However, the nucleation on inner surface by shear at the mandrel contact is not prototypical of a clad rupture during the PCMI (Pellet Clad Mechanical Interaction) phase of a RIA (membrane stresses in the clad thickness in RIA). An important lesson learned from this experimental approach is that the PST test is a particularly complex test, both in its implementation and interpretation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗