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DOE OSTI2022

The High-Frequency Signature of Slow and Fast Laboratory Earthquakes

Tectonic faults fail through a spectrum of slip modes, ranging from slow aseismic creep to rapid slip during earthquakes. Understanding the seismic radiation emitted during these slip modes is key for advancing earthquake science and earthquake hazard assessment. In this work, we use laboratory friction experiments instrumented with ultrasonic sensors to document the seismic radiation properties of slow and fast laboratory earthquakes. Stick-slip experiments were conducted at a constant loading rate of 8 μm/s and the normal stress was systematically increased from 7 to 15 MPa. We produced a full spectrum of slip modes by modulating the loading stiffness in tandem with the fault zone normal stress. Acoustic emission data were recorded continuously at 5 MHz. We demonstrate that the full continuum of slip modes radiate measurable high-frequency energy between 100 and 500 kHz, including the slowest events that have peak fault slip rates <100 μm/s. The peak amplitude of the high-frequency time-domain signals scales systematically with fault slip velocity. Stable sliding experiments further support the connection between fault slip rate and high-frequency radiation. Experiments demonstrate that the origin of the high-frequency energy is fundamentally linked to changes in fault slip rate, shear strain, and breaking of contact junctions within the fault gouge. Our results suggest that having measurements close to the fault zone may be key for documenting seismic radiation properties and fully understanding the connection between different slip modes.

58 GEOSCIENCES↗

DOE OSTI2021

Ordering effects on deformation substructures and strain hardening behavior of a CrCoNi based medium entropy alloy

Here, a CrCoNi based medium entropy alloy with small additions of Ti, Al and Nb (denoted as (CrCoNi) 93 Al 4 Ti 2 Nb) in the as-quenched condition, exhibits tensile properties comparable to those of the equiatomic CrCoNi alloy at room temperature. Dark field transmission electron microscopy (TEM), atomic resolution high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM) together with atom probe tomography (APT) show that spatially-localized long range ordering (LRO) L1 2 domains exist in this alloy. The evolution of deformation substructure with plastic deformation in this alloy was characterized using electron backscatter diffraction (EBSD), electron channeling contrast imaging (ECCI) and STEM based techniques including the recently developed weak beam dark field STEM imaging. Plastic deformation occurs by the slip of a/2<110>dislocations, which are narrowly dissociated into Shockley partial dislocations on {111} slip planes. Their dissociation distances in the (CrCoNi) 93 Al 4 Ti 2 Nb alloy are much smaller than the widths of the corresponding partials in the equiatomic CrCoNi alloy due to one or more of the minor alloying elements (Al, Ti, Nb). Dislocation slip in this alloy has a pronounced planar character. The leading dislocations in slip bands glide as pairs due to the existence of LRO domains. Multipoles were formed through the slip of dislocations with opposite signs on adjacent {111} slip planes. Those multipoles serve as building blocks for the formation of subgrain structures consisting of fine slip bands. The distances between slip bands were continuously refined during plastic deformation and dynamic refinement of slip bands plays a crucial role in strain hardening. The effects of LRO domains on planar dislocation slip, the deactivation of deformation twinning and strain hardening of this alloy are discussed.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Designing Ti-6Al-4V microstructure for strain delocalization using neural networks

Abstract The deformation behavior of Ti-6Al-4V titanium alloy is significantly influenced by slip localized within crystallographic slip bands. Experimental observations reveal that intense slip bands in Ti-6Al-4V form at strains well below the macroscopic yield strain and may serially propagate across grain boundaries, resulting in long-range localization that percolates through the microstructure. These connected, localized slip bands serve as potential sites for crack initiation. Although slip localization in Ti-6Al-4V is known to be influenced by various factors, an investigation of optimal microstructures that limit localization remains lacking. In this work, we develop a novel strategy that integrates an explicit slip band crystal plasticity technique, graph networks, and neural network models to identify Ti-6Al-4V microstructures that reduce the propensity for strain localization. Simulations are conducted on a dataset of 3D polycrystals, each represented as a graph to account for grain neighborhood and connectivity. The results are then used to train neural network surrogate models that accurately predict localization-based properties of a polycrystal, given its microstructure. These properties include the ratio of slip accumulated in the band to that in the matrix, fraction of total applied strain accommodated by slip bands, and spatial connectivity of slip bands throughout the microstructure. The initial dataset is enriched by synthetic data generated by the surrogate models, and a grid search optimization is subsequently performed to find optimal microstructures. Describing a 3D polycrystal with only a few features and a combination of graph and neural network models offer robustness compared to the alternative approaches without compromising accuracy. We show that while each material property is optimized through a unique microstructure solution, elongated grain shape emerges as a recurring feature among all optimal microstructures. This finding suggests that designing microstructures with elongated grains could potentially mitigate strain localization without compromising strength.

Ahmadikia, Behnam↗

NASA NTRS1987

The characteristics of gamma-prime dislocation pairs in a nickel-base superalloy

The gamma-prime dislocation pairs of a single crystal nickel-base superalloy, PWA 1480, after tensile and fatigue loading at 650 C are analyzed. The existence and extent of cube cross slip in octahedral slip, and the nature of gamma-prime dislocation pairs in primary cube slip are investigated. It is observed that the PWA 1480 specimens oriented near (001) and (-3 6 10) line directions deform by octahedral slip and specimens oriented near (-1 1 1) and (-2 3 4) lines deform by primary cube slip. It is determined that the overall dislocation distributions are more homogeneous in low cycle fatigue (LCF) loading than in monotonic tensile loading; however, the gamma-prime dislocation pair characteristics are similar for tensile and LCF test specimens. The data reveal that the gamma-prime dislocation pairs of octahedral slip specimens are near-screw and on the cube cross slip plane and for the cube slip specimens, the dislocation pairs are of various characters and on the primary cube slip plane.

Gabb, T. P.↗

NASA NTRS2005

Quantifying Exact Motions Along Lineaments on Europa

Evaluating the precise motions along lineaments on the surface of Jupiter's icy moon, Europa, is a valuable tool for interpreting the development and history of lineaments of various morphologies. Such morphologies include strike-slip faults, dilational bands, ridges, and convergence zones. However, the exact mode of origin and kinematic behavior of these various lineaments are not obvious based on morphology alone. In fact, the apparent motions implied by displaced crosscut features can provide misleading indications of true motions along lineaments. Identifying the precise motions (combinations of sliding and opening/closing) is critical to the accurate characterization and interpretation of each of these lineament types. Lineaments of interest (i.e., those having displaced relatively older features in some manner) are identified on Galileo spacecraft images and measurements are made of the total offset, the separation, and relative orientations of crosscut features with respect to the lineament of interest. Specifically, by using these measured quantities and a series of trigonometric equations, the precise motions (i.e., dilation, convergence, strike-slip, or a combination of strike-slip and dilation or convergence) can be determined. These measurements are, however, limited by the resolution of the available images. This study focuses on motion analysis techniques for Europan lineaments and the precise characterization of fault-orthogonal and/or strike-slip motion along lineaments of varying morphologies. We highlight potential pitfalls of cursory analyses of motion indicators. For example, lineaments with obvious lateral offsets have typically been identified simply as strike-slip faults. This assumption may actually be incorrect, as fault-orthogonal motions may contribute to apparent lateral displacements (offsets or separations). Also, variability in the amount of fault motion along the trace length should theoretically be identifiable using the outlined technique. Strike-slip faults on Europa have conventionally been presumed to have a constant slip magnitude along their lengths; however, we posit that variable distributions of slip may be common, as is typical along terrestrial strike-slip faults.

Vetter, J. C.↗

NASA NTRS1974

High-purity silica reflecting heat shield development

A high-purity, fused-silica reflecting heat shield for the thermal protection of outer-planet probes was developed. Factors that strongly influence the performance of a silica heat shield were studied. Silica-bonded silica configurations, each prepared by a different technique, were investigated and rated according to its relative merits. Slip-casting was selected as the preferred fabrication method because it produced good reflectivity and good strength, and is relatively easy to scale up for a full-size outer-planet probe. The slips were cast using a variety of different particle sizes: continuous particle-size slips; monodisperse particle-size slips; and blends of monodisperse particle-size slips were studied. In general, smaller particles gave the highest reflectance. The monodisperse slips as well as the blend slips gave a higher reflectance than the continuous particle-size slips. An upgraded and fused natural quartz was used to study the effects of microstructure on reflectance and as the baseline to ascertain the increase in reflectance obtained from using a higher-purity synthetic material.

Congdon, W. M.↗

NASA NTRS1985

Constitutive modeling for single crystal superalloys

A crystallographic approach to constitutive modeling of single crystal superalloys is discussed. The approach is based on identifying the active slip planes and slip directions. The shear stresses are computed on each of the slip planes from applied stress components. The slip rate is then computed on each slip system and the microscopic inelastic strain rates are the sum of the slip in the individual slip systems. The constitutive model was implemented in a finite element code using twenty noted isoparametric solid elements. Constants were determined for octahedral and cube slip systems. These constants were then used to predict tension-compression asymmetry and fatigue loops. Other data was used to model the tensile and creep response.

Stouffer, Donald C.↗

DOE OSTI2020

Crystallographic Orientation Dependence of Mechanical Responses of FeCrAl Micropillars

Iron-chromium-aluminum (FeCrAl) alloys are used in automobile exhaust gas purifying systems and nuclear reactors due to its superior high-temperature oxidation and excellent corrosion resistance. Single-phase FeCrAl alloys with a body centered cubic structure plastically deform through dislocation slips at room temperature. Here, we investigated the orientation dependence of mechanical responses of FeCrAl alloy through testing single-crystal and bi-crystal micropillars in a scanning electron microscopy at room temperature. Single-crystal micropillars were fabricated with specific orientations which favor the activity of single slip system or two slip systems or multiple slip systems. The strain hardening rate and flow strength increase with increasing the number of activated slip system in micropillars. Bi-crystal micropillars with respect to the continuity of slip systems across grain boundary were fabricated to study the effect of grain boundary on slip transmission. The high geometrical compatibility factor corresponds to a high flow strength and strain hardening rate. Experimental results provide insight into understanding mechanical response of FeCrAl alloy and developing the mechanisms-based constitutive laws for FeCrAl polycrystalline aggregates.

36 MATERIALS SCIENCE↗

NASA NTRS1984

Low cycle fatigue of MAR-M 200 single crystals at 760 and 870 deg C

Fully reversed low cycle fatigue tests were conducted on single crystals of the nickel-base superalloys Mar-M 200 at 760 C and 870 C. At 760 C, planar slip (octahedral) lead to orientation-dependent strain hardening and cyclic lives. Multiple slip crystals strain hardened the most, resulting in relatively high stress ranges and low lives. Single slip crystals strain hardened the least, resulting in relatively low stress ranges and higher lives. A preferential crack initiation site which was related to slip plane geometry was observed in single slip orientated crystals. At 870 C, the trends were quite different, and the slip character was much more homogeneous. As the tensile axis orientation deviated from 001 , the stress ranges increased and the cyclic lives decreased. Two possible mechanisms were proposed to explain the behavior: one is based on Takeuchi and Kuramoto's cube cross-slip model, and the other is based on orientation-dependent creep rates.

Milligan, W. W.↗

NASA NTRS1988

Resolved shear stress intensity coefficient and fatigue crack growth in large crystals

Fatigue crack growth in large grain Al alloy was studied. Fatigue crack growth is caused primarily by shear decohesion due to dislocation motion in the crack tip region. The crack paths in the large crystals are very irregular and zigzag. The crack planes are often inclined to the loading axis both in the inplane direction and the thickness direction. The stress intensity factors of such inclined cracks are approximated from the two dimensional finite element calculations. The plastic deformation in a large crystal is highly anisotropic, and dislocation motion in such crystals are driven by the resolved shear stress. The resolved shear stress intensity coefficient in a crack solid, RSSIC, is defined, and the coefficients for the slip systems at a crack tip are evaluated from the calculated stress intensity factors. The orientations of the crack planes are closely related to the slip planes with the high RSSIC values. If a single slip system has a much higher RSSIC than all the others, the crack will follow the slip plane, and the slip plane becomes the crack plane. If two or more slip systems have a high RSSIC, the crack plane is the result of the decohesion processes on these active slip planes.

Chen, QI↗

NASA NTRS1989

Deformation modeling and constitutive modeling for anisotropic superalloys

A study of deformation mechanisms in the single crystal superalloy PWA 1480 was conducted. Monotonic and cyclic tests were conducted from 20 to 1093 C. Both (001) and near-(123) crystals were tested, at strain rates of 0.5 and 50 percent/minute. The deformation behavior could be grouped into two temperature regimes: low temperatures, below 760 C; and high temperatures, above 820 to 950 C depending on the strain rate. At low temperatures, the mechanical behavior was very anisotropic. An orientation dependent CRSS, a tension-compression asymmetry, and anisotropic strain hardening were all observed. The material was deformed by planar octahedral slip. The anisotropic properties were correlated with the ease of cube cross-slip, as well as the number of active slip systems. At high temperatures, the material was isotropic, and deformed by homogeneous gamma by-pass. It was found that the temperature dependence of the formation of superlattice-intrinsic stacking faults was responsible for the local minimum in the CRSS of this alloy at 400 C. It was proposed that the cube cross-slip process must be reversible. This was used to explain the reversible tension-compression asymmetry, and was used to study models of cross-slip. As a result, the cross-slip model proposed by Paidar, Pope and Vitek was found to be consistent with the proposed slip reversibility. The results were related to anisotropic viscoplastic constitutive models. The model proposed by Walter and Jordan was found to be capable of modeling all aspects of the material anisotropy. Temperature and strain rate boundaries for the model were proposed, and guidelines for numerical experiments were proposed.

Milligan, Walter W.↗

NASA NTRS1988

Resolved shear stress intensity coefficient and fatigue crack growth in large crystals

Fatigue crack growth tests were carried out on large-grain Al 7029 aluminum alloy and the finite element method was used to calculate the stress field near the tip of a zigzag crack. The resolved shear stresses on all 12 slip systems were computed, and the resolved shear stress intensity coefficient (RSSIC) was defined. The RSSIC was used to analyze the irregular crack path and was correlated with the rate of single-slip-plane shear crack growth. Fatigue crack growth was found to be caused primarily by shear decohesion at a crack tip. When the RSSIC on a single-slip system was much larger than all the others, the crack followed a single-slip plane. When the RSSICs on two conjugate slip systems were comparable, a crack grew in a zigzag manner on these planes and the macrocrack-plane bisected the two active slip planes. The maximum RSSIC on the most active slip system is proposed as a parameter to correlate with the shear fatigue crack growth rate in large crystals.

Chen, Q.↗

NASA NTRS1991

Creep behavior of copper at intermediate temperatures. II - Surface microstructural observations. III - A comparison with theory

Three different types of microstructural slip features are noted to occur during the creep of Cu at 0.46-0.72 of absolute melting point. While single slip is associated with higher temperatures and lower stresses, complex wavy slip features are observed at higher temperatures and higher stresses as well as with increasing strains: suggesting the importance of cross-slip mechanisms. At lower temperatures and higher stresses the multiple-slip morphologies observed indicate that cross-slip mechanisms may control the creep of polycrystalline Cu only over a limited stress and temperature range. A phenomenological model is proposed which assumes that (1) cell boundaries within subgrains act as both sources of, and obstacles to, gliding dislocations, and (2) dislocation annihilation occurs at the cell boundaries by climb and cross-slip.

Raj, S. V.↗

NASA NTRS1992

Improving the low temperature ductility of NiAl

The intermetallic NiAl exhibits excellent potential as a structural material for application in air-breathing and single-stage-to-orbit engines. Unfortunately NiAl is brittle at ambient temperature, which is partly attributed to the lack of five independent slip systems as required by von Mises criterion for uniform, volume conserving deformation since the operative group of zone axes (100) slip offers only three independent slip systems. Isostructural FeAl, however, deforms by group of zone axes (111) slip at room temperature which provides five independent slip systems. Thus, it was decided to macroalloy NiAl with Fe to promote group of zone axes (111) slip thereby possibly improving the ductility. For Ni - 30 at. (percent) Al - 20 at. (percent) Fe having essentially bcc microstructure indicated up to 6 percent tensile elongation combined with high yield strength (about 800 MPa). The results compare favorably with those of stoichiometric Ni - 50 at. (percent) Al which, however, deforms by group of zone axes (100) slip at room temperature. The multi-phase alloy approach has proven even more successful for Ni - 20 at. (percent) Al - 30 at. (percent) Fe. The high temperature ductility of the multi-phase alloy was attributed to deformation transfer across interphase boundaries and the crack stopping action of the constituent gamma/gamma' phase. While the constituent phase became increasingly brittle, the beta' phase became more ductile at elevated temperatures. Thus the multi-phase alloy did not exhibit any elevated temperature embrittlement. Similarly, while the beta' phase became weak at high temperatures, the gamma/gamma' phase exhibited better strength retention leading to the improved elevated temperature strength of the multi-phase alloy. Thus, the multi-phase alloy benefits from both its constituent phases, with each phase alleviating the disadvantages associated with the other phase over any temperature range. The multi-phase alloy approach is suggested as a possible approach to designing intermetallic-based alloys.

Guha, Sumit↗

NASA NTRS1996

Cross-Effects in Microgravity Flows

Film growth by chemical/physical vapor deposition is a process of considerable interest in microgravity experiments. The absence of natural convection should allow better control of film growth processes but, in highly non-isothermal ampoules, thermal slip (creep) can become a matter of significant concern. The reported research is a theoretical and experimental investigation of the flow of gas/vapor mixtures under non-continuum conditions. The Boltzmann equation has been solved for a monatomic gas under non-condensing conditions and the various phenomenological coefficients have been computed. Computations for realistic potentials as well as for velocity and creep slip have been completed and the creep slip has been found to be dependent on the type of gas confirming the accuracy of previous variational results. The variational technique has been extended and planar flows calculated via the Burnett solutions. Velocity, diffusion and creep slips have been computed for gas mixtures and previously unknown dependencies of the creep slip on the mixture properties have been observed. Also for gas mixtures, an integral representation of the linearized Boltzmann operator has been developed for use in numerical and variational calculations for all intermolecular force laws. Two, two-bulb capillary systems have been designed, built and tested for the measurements of cross-flows; one of glass for isothermal measurements and one of stainless steel for non-isothermal measurements. Extensive data have been collected for Ar-He and N2-He mixtures at a variety of pressures and mole ratios. Viscosity, velocity slip coefficients and tangential momentum accommodation coefficients have been obtained from measurements with a spinning rotor gauge via a new theory that has been formulated for the spinning rotor gauge in the slip regime. The FIDAP fluid dynamics code has been applied to condensing flows in ampoules in the continuum regime and agreement obtained with the earlier work of Duval.

Loyalka, Sudarshan K.↗

NASA NTRS1995

Alaska Crustal Deformation: Finite Element Modeling Constrained by Geologic and Very Long Baseline Interferometry Data

We compute crustal motions in Alaska by calculating the finite element solution for an elastic spherical shell problem. The method we use allows the finite element mesh to include faults and very long baseline interferometry (VLBI) baseline rates of change. Boundary conditions include Pacific-North American (PA-NA) plate motions. The solution is constrained by the oblique orientation of the Fairweather-Queen Charlotte strike-slip faults relative to the PA-NA relative motion direction and the oblique orientation from normal convergence of the eastern Aleutian trench fault systems, as well as strike-shp motion along the Denali and Totschunda fault systems. We explore the effects that a range of fault slip constraints and weighting of VLBI rates of change has on the solution. This allows us to test the motion on faults, such as the Denali fault, where there are conflicting reports on its present-day slip rate. We find a pattern of displacements which produce fault motions generally consistent with geologic observations. The motion of the continuum has the general pattern of radial movement of crust to the NE away from the Fairweather-Queen Charlotte fault systems in SE Alaska and Canada. This pattern of crustal motion is absorbed across the Mackenzie Mountains in NW Canada, with strike-slip motion constrained along the Denali and Tintina fault systems. In south central Alaska and the Alaska forearc oblique convergence at the eastern Aleutian trench and the strike-shp motion of the Denali fault system produce a counterclockwise pattern of motion which is partially absorbed along the Contact and related fault systems in southern Alaska and is partially extruded into the Bering Sea and into the forearc parallel the Aleutian trench from the Alaska Peninsula westward. Rates of motion and fault slip are small in western and northern Alaska, but the motions we compute are consistent with the senses of strike-slip motion inferred geologically along the Kaltag, Kobuk Trench, and Thompson Creek faults and with the normal faulting observed in NW Alaska near Nome. The nonrigid behavior of our finite element solution produces patterns of motion that would not have been expected from rigid block models: strike-slip faults can exist in a continuum that has motion mostly perpendicular to their strikes, and faults can exhibit along-strike differences in magnitudes and directions.

Lundgren, Paul↗

NASA NTRS1998

The Surface Displacement Field of the November 8, 1997, Mw7.6 Manyi (Tibet) Earthquake Observed with ERS InSAR Data

ERS2 radar data acquired before and after the Mw7.6, Manyi (Tibet) earthquake of November 8, 1997, provide geodetic information about the surface displacement produced by the earthquake in two ways. (1) The sub-pixel geometric adjustment of the before and after images provides a two dimensional offset field with a resolution of approx, 1m in both the range (radar line of sight) and azimuth (satellite track) directions. Comparison of offsets in azimuth and range indicates that the displacement along the fault is essentially strike-slip and in a left-lateral sense. The offset map reveals a relatively smooth and straight, N78E surface rupture that exceeds 150 km in length, consistent with the EW plane of the Harvard CMT solution. The rupture follows the trace of a quaternary fault visible on satellite imagery (Tapponnier and Molnar, 1978; Wan Der Woerd, pers. comm.). (2) Interferometric processing of the SAR data provides a range displacement map with a precision of a few millimeters. The slip distribution along the rupture reconstructed from the range change map is a bell-shaped curve in the 100-km long central section of the fault with smaller, local maxima near both ends. The curve shows that the fault slip exceeds 2.2 m in range, or 6.2 in strike-slip, along a 30-km long section of the fault and remains above 1 m in range, approx. 3 m strike-slip, along most of its length. Preliminary forward modeling of the central section of the rupture, assuming a uniform slip distribution with depth, indicates that the slip occur-red essentially between 0 and the depth of 10 km, consistent with a relatively shallow event (Velasco et al., 1998).

Peltzer, G.↗

NASA NTRS1978

Report of the Seasat Failure Review Board

The Seasat spacecraft failed on October 9, 1978, after satisfactory operation in orbit for 105 days, as a result of a loss of electrical power in the Agena bus that was used as a part of the spacecraft. This loss of power was caused by a massive and progressive short in one of the slip ring assemblies that was used to connect the rotating solar arrays into the power subsystem. The most likely cause of this short was the initiation of an arc between adjacent slip ring brush assemblies. The triggering mechanism of this arc could have been either a wire-to-brush assembly contact, a brush-to-brush contact, or a momentary short caused by a contaminant that bridged internal components of opposite electrical polarity. The slip ring assembly, as used in the Seasat spacecraft, was connected into the power subsystem in such a way that most of the adjacent brush assemblies were of opposite electrical polarity. This wiring arrangement, together with the congested nature of the design itself, made the Seasat slip ring assembly a unique, first-of-a-kind component that was particularly prone to shorting. The possibility of slip ring failures resulting from placing opposite electrical polarities on adjacent brush assemblies was known at least as early-as the summer of 1977 to other projects within the contractor's organization. Furthermore, failures of slip ring assemblies due to shorting between brushes had been experienced by the prime contractor on slip ring assemblies used by other programs. That the Seasat organization was not fully aware of these potential failure modes was due to a breakdown in communication within the contractor's organization.

Lundin, Bruce T.↗