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At least 469 records · Page 26
All sourcesNASA NTRSDOE OSTI
NASA NTRS2012

Bump Bonding Using Metal-Coated Carbon Nanotubes

Bump bonding hybridization techniques use arrays of indium bumps to electrically and mechanically join two chips together. Surface-tension issues limit bump sizes to roughly as wide as they are high. Pitches are limited to 50 microns with bumps only 8-14 microns high on each wafer. A new process uses oriented carbon nanotubes (CNTs) with a metal (indium) in a wicking process using capillary actions to increase the aspect ratio and pitch density of the connections for bump bonding hybridizations. It merges the properties of the CNTs and the metal bumps, providing enhanced material performance parameters. By merging the bumps with narrow and long CNTs oriented in the vertical direction, higher aspect ratios can be obtained if the metal can be made to wick. Possible aspect ratios increase from 1:1 to 20:1 for most applications, and to 100:1 for some applications. Possible pitch density increases of a factor of 10 are possible. Standard capillary theory would not normally allow indium or most other metals to be drawn into the oriented CNTs, because they are non-wetting. However, capillary action can be induced through the ability to fabricate oriented CNT bundles to desired spacings, and the use of deposition techniques and temperature to control the size and mobility of the liquid metal streams and associated reservoirs. This hybridization of two technologies (indium bumps and CNTs) may also provide for some additional benefits such as improved thermal management and possible current density increases.

Lamb, James L.↗
NASA NTRS2012

ORIGIN: Metal Creation and Evolution from the Cosmic Dawn

ORIGIN is a proposal for the M3 mission call of ESA aimed at the study of metal creation from the epoch of cosmic dawn. Using high-spectral resolution in the soft X-ray band, ORIGIN will be able to identify the physical conditions of all abundant elements between C and Ni to red-shifts of z=10, and beyond. The mission will answer questions such as: When were the first metals created? How does the cosmic metal content evolve? Where do most of the metals reside in the Universe? What is the role of metals in structure formation and evolution? To reach out to the early Universe ORIGIN will use Gamma-Ray Bursts (GRBs) to study their local environments in their host galaxies. This requires the capability to slew the satellite in less than a minute to the GRB location. By studying the chemical composition and properties of clusters of galaxies we can extend the range of exploration to lower redshifts (z approx. 0.2). For this task we need a high-resolution spectral imaging instrument with a large field of view. Using the same instrument, we can also study the so far only partially detected baryons in the Warm-Hot Intergalactic Medium (WHIM). The less dense part of the WHIM will be studied using absorption lines at low redshift in the spectra for GRBs. The ORIGIN mission includes a Transient Event Detector (coded mask with a sensitivity of 0.4 photon/sq cm/s in 10 s in the 5-150 keV band) to identify and localize 2000 GRBs over a five year mission, of which approx.65 GRBs have a redshift >7. The Cryogenic Imaging Spectrometer, with a spectral resolution of 2.5 eV, a field of view of 30 arcmin and large effective area below 1 keV has the sensitivity to study clusters up to a significant fraction of the virial radius and to map the denser parts of the WHIM (factor 30 higher than achievable with current instruments). The payload is complemented by a Burst InfraRed Telescope to enable onboard red-shift determination of GRBs (hence securing proper follow up of high-z bursts) and also probes the mildly ionized state of the gas. Fast repointing is achieved by a dedicated Controlled Momentum Gyro and a low background is achieved by the selected low Earth orbit.

Kouveliotou, C.↗
NASA NTRS2013

Castable Amorphous Metal Mirrors and Mirror Assemblies

A revolutionary way to produce a mirror and mirror assembly is to cast the entire part at once from a metal alloy that combines all of the desired features into the final part: optical smoothness, curvature, flexures, tabs, isogrids, low CTE, and toughness. In this work, it has been demonstrated that castable mirrors are possible using bulk metallic glasses (BMGs, also called amorphous metals) and BMG matrix composites (BMGMCs). These novel alloys have all of the desired mechanical and thermal properties to fabricate an entire mirror assembly without machining, bonding, brazing, welding, or epoxy. BMGs are multi-component metal alloys that have been cooled in such a manner as to avoid crystallization leading to an amorphous (non-crystalline) microstructure. This lack of crystal structure and the fact that these alloys are glasses, leads to a wide assortment of mechanical and thermal properties that are unlike those observed in crystalline metals. Among these are high yield strength, carbide-like hardness, low melting temperatures (making them castable like aluminum), a thermoplastic processing region (for improving smoothness), low stiffness, high strength-to-weight ratios, relatively low CTE, density similar to titanium alloys, high elasticity and ultra-smooth cast parts (as low as 0.2-nm surface roughness has been demonstrated in cast BMGs). BMGMCs are composite alloys that consist of a BMG matrix with crystalline dendrites embedded throughout. BMGMCs are used to overcome the typically brittle failure observed in monolithic BMGs by adding a soft phase that arrests the formation of cracks in the BMG matrix. In some cases, BMGMCs offer superior castability, toughness, and fatigue resistance, if not as good a surface finish as BMGs. This work has demonstrated that BMGs and BMGMCs can be cast into prototype mirrors and mirror assemblies without difficulty.

Hofmann, Douglas C.↗
NASA NTRS2013

Low Masses and High Redshifts: The Evolution of the Mass-Metallicity Relation

We present the first robust measurement of the high redshift mass-metallicity (MZ) relation at 10(exp 8) < M/Stellar Mass < or approx. 10(exp 10), obtained by stacking spectra of 83 emission-line galaxies with secure redshifts between 1.3 < or approx. z < or approx. 2.3. For these redshifts, infrared grism spectroscopy with the Hubble Space Telescope Wide Field Camera 3 is sensitive to the R23 metallicity diagnostic: ([O II] (lambda)(lambda)3726, 3729 + [OIII] (lambda)(lambda)4959, 5007)/H(beta). Using spectra stacked in four mass quartiles, we find a MZ relation that declines significantly with decreasing mass, extending from 12+log(O/H) = 8.8 at M = 10(exp 9.8) Stellar Mass to 12+log(O/H)= 8.2 at M = 10(exp 8.2) Stellar Mass. After correcting for systematic offsets between metallicity indicators, we compare our MZ relation to measurements from the stacked spectra of galaxies with M > or approx. 10(exp 9.5) Stellar Mass and z approx. 2.3. Within the statistical uncertainties, our MZ relation agrees with the z approx. 2.3 result, particularly since our somewhat higher metallicities (by around 0.1 dex) are qualitatively consistent with the lower mean redshift (z = 1.76) of our sample. For the masses probed by our data, the MZ relation shows a steep slope which is suggestive of feedback from energy-driven winds, and a cosmological downsizing evolution where high mass galaxies reach the local MZ relation at earlier times. In addition, we show that our sample falls on an extrapolation of the star-forming main sequence (the SFR-M∗ relation) at this redshift. This result indicates that grism emission-line selected samples do not have preferentially high star formation rates (SFRs). Finally, we report no evidence for evolution of the mass-metallicity-SFR plane; our stack-averaged measurements show excellent agreement with the local relation.

Hgih Redshifts↗
NASA NTRS2015

Additively Manufactured Metals in Oxygen Systems Project

Metals produced by additive manufacturing methods, such as Powder Bed Fusion Technology, are now mature enough to be considered for qualification in human spaceflight oxygen systems. The mechanical properties of metals produced through AM processes are being systematically studied. However, it is unknown whether AM metals in oxygen applications may present an increased risk of flammability or ignition as compared to wrought metals of the same metallurgical composition due to increased porosity. Per NASA-STD-6001B materials to be used in oxygen system applications shall be based on flammability and combustion test data, followed by a flammability assessment. Without systematic flammability and ignition testing in oxygen there is no credible method for NASA to accurately evaluate the risk of using AM metals in oxygen systems.

Tylka, Jonathan↗
NASA NTRS2016

The Carnegie Chicago Hubble Program: The Mid-Infrared Colours of Cepheids and the Effect of Metallicity on the CO Band-Head at 4.6 Micron

We compare mid-infrared (IR) 3.6 and 4.5 micron Warm Spitzer observations for Cepheids in the Milky Way and the Large and Small Magellanic Clouds. Using models, we explore in detail the effect of the CO rotation-vibration band-head at 4.6 micron on the mid-IR photometry. We confirm the temperature sensitivity of the CO band-head at 4.6 micron and find no evidence for an effect at 3.6 micron. We compare the ([3.6]-[4.5]) period-colour relations in the MW, LMC and SMC. The slopes of the period-colour relations for the three galaxies are in good agreement, but there is a trend in zero-point with metallicity, with the lowest metallicity Cepheids having redder mid-IR colours. Finally, we present a colour-[Fe/H] relation based on published spectroscopic metallicities. This empirical relation, calibrated to the metallicity system of Genovali et al., demonstrates that the ([3.6]-[4.5]) colour provides a reliable metallicity indicator for Cepheids, with a precision comparable to current spectroscopic determinations.

Scowcroft, Victoria↗
NASA NTRS2018

Lifetimes of Multiply Alkylated Cyclopentane Oil in Contact with Various Metals, Evaluated with Vacuum Spiral Orbit Tribometer

The dependence of the lifetimes of small quantities of a Multiply Alkylated Cyclopentane (MAC) lubricant oil, Pennzane (Registered Trademark) 2001A (Nye Lubricants, Inc.), in rolling and sliding contact with different metals was evaluated with a vacuum spiral orbit tribometer. The metals were the bearing alloys 52100 steel, 440C steel, 17-4 PH steel and Nitinol 60 and the elements chromium, vanadium and titanium. The lifetimes of the lubricant oil on different metals fell into distinct groups with 52100 greater than 440C approx. Nitinol 60 greater than 17-4 PH for the order of the lifetimes of the steels and chromium greater than vanadium greater than titanium for the order of the lifetimes for the elements. The limited life of the small quantities of oil is assumed to be due to its consumption by the tribochemical reaction of the oil with the different metal bearing materials. The lifetimes are then inversely related to the reaction rates of the oil molecules with the various metals: the longest life of 52100 steel having the lowest reaction rate and the shortest life of titanium having the highest reaction rate. Mechanisms for the tribochemical reactions are discussed.

lubrication↗
NASA NTRS2019

Electrochemical, Polarization, and Crevice Corrosion Testing of Inconel X750: A Supplement to the Environmental Control and Life Support System Sustaining Metal Materials Compatibility Study

In previous studies, electrochemical test results were experimentally acquired and then presented for several noble alloys in two specific solutions representative of waste liquids generated or present within the Environmental Control and Life Support System (ECLSS) aboard the International Space Station (ISS). Subsequently, another metal candidate, Inconel X750, has been submitted and was subjected to the same test routines in the same solutions and evaluated with the same statistical/analytical methodologies as those utilized in the earlier studies. Previous studies included three titanium grades, (Commercially Pure, 6Al-4V alloy, and 6Al-4V Low Interstitial alloy), two nickel-chromium alloys (Inconel® 625 and Hastelloy® C276), one high tier stainless steel (Cronidur® 30), and a nickel-titanium alloy (Nitinol 60). Thus far, all candidate alloys have exhibited excellent corrosion protection and galvanic compatibility attributes and have been deemed qualified materials for application within the ECLSS facility. Inconel X750 now joins that group. The titanium alloys gave the best results of all the metal candidates by demonstrating superior nobility and galvanic protection properties. It is worth noting that the corrosion performance properties for the three titanium alloys were essentially indistinguishable. As such and for expediency, this study and all future evaluations will refer only to the comparative properties already documented for Titanium 6Al-4V as this alloy is representative of all three alloys and considered to be more mainstream. Now the measured corrosion properties for Inconel X750 were very similar to those determined previously for Inconel 625 and Hastelloy C276 which were also determined to be very high performers. For the current effort, the results have clearly shown that Inconel X750 possesses exceptional anti-corrosion attributes comparable to metals in the highest tier of the galvanic series. Overall, one can conclude that Inconel X750 is quite noble, highly corrosion resistant and galvanically compatible with the other metal groups from both an electrochemical perspective and a long-term exposure scenario. This was clearly demonstrated after utilizing the same techniques as those applied in previous studies which included linear, Tafel and cyclic polarization, galvanic coupling with each of the other metal candidates, and pitting/crevicing assessments after one full year of immersion in the subject test solutions. Attributes defining the nobility and anti-corrosion capabilities for X750 appear to be on par with all the other candidates thus far and this alloy can now be classified as ‘excellent’ exhibiting very high resistance toward general, localized, and galvanic corrosion in the subject test media.

Lee, R. E.↗
NASA NTRSDate not supplied

Metal Fused Filament Fabrication of Titanium Alloy for In Space Manufacturing

NASA is developing materials and processes for the in-space manufacturing of many items for the International Space Station (ISS) and future exploration platforms. These new manufacturing processes will require the further development of current 3D printing processes to achieve high-performance metal parts within the power and space constraints of the ISS. Manufacturing Ti-6Al-4V alloy parts with 3D printing using a metal fused filament fabrication (MF3) process is an alternative process to the Direct Metal Laser Sintering (DMLS) of the metal powders additive manufacturing process. Our initial work fabricating Ti-6Al-4V parts from Ti-6Al-4V powder-binder feedstock and processed with the MF3 process has resulted in 95-97% sintered densities. The current development work of optimized sintered properties investigates the effects of variation in sintering time, temperature, and vacuum on the sintered properties of Ti-6Al-4V MF3 printed tensile bars. Sintered properties such as density, hardness, and tensile properties were characterized followed by microstructural and chemical (O/C/N) analysis to understand the role of sintering process on the ensuing material properties. Future development of the MF3 process will also involve investigation of the effects of micro-milling the Ti-64Al-4V powder to nanometer particle sizes and the investigation of laser sintering of the 3D printed devices. This new micro-milling technique will have broad application to other areas that require particle size reduction of hard metallic materials, such as Nuclear Thermal Propulsion and other NASA technologies. Laser sintering in lieu of high temperature thermal sintering should allow for significant power reduction and improved processing speeds.

sintering, alloys, 3D printing↗
NASA NTRS2020

Sierra Gorda 009: A New Member of the Metal-Rich G Chondrites Grouplet

We investigated the metal-rich chondrite Sierra Gorda (SG) 009, a member of the new G chondrite grouplet (also including NWA 5492, GRO 95551). G chondrites contain 23% metal, very reduced silicates, and rare oxidized mineral phases (Mg-chromite, FeO-rich pyroxene). G chondrites are not related to CH-CB chondrites, based on bulk O, C and N isotopic compositions, mineralogy and geochemistry. G chondrites have no fine-grained matrix or matrix lumps enclosing hydrated material typical for CH-CB chondrites. G chondrites’ average metal compositions are similar to H chondrites. Siderophile and lithophile geochemistry indicate sulfidization and fractionation of the SG 009 metal and silicates, unlike NWA 5492 and GRO 05551. The G chondrites have average O isotopic compositions DELTA 17O >0 ‰ ranging between bulk enstatite (E) and ordinary (O) chondrites. An Al-rich chondrule from SG 009 has DELTA 17O <0 ‰ indicating some heterogeneity in oxygen isotopic composition of G chondrite components. SG 009’s bulk carbon and nitrogen isotopic compositions correspond to E and O chondrites. Neon isotopic composition reflects a mixture of cosmogenic and solar components, and cosmic ray exposure age of SG 009 is typical for O, E, and R chondrites. G chondrites are closely related to O, E, and R chondrites and may represent a unique metal-rich parent asteroid containing primitive and fractionated material from the inner Solar System. Oxidizing and reducing conditions during SG 009 formation may be connected with a chemical micro-environment and possibly could indicate that G chondrites may have formed by a planetesimal collision resulting in the lack of matrix.

chondrite↗
NASA NTRSDate not supplied

Novel Ceramic Dispersion Strengthened Refractory Metals for Improved Printability and Properties

Refractory metals and alloys are of major interest for nuclear fusion systems, space nuclear power and propulsion, and hypersonic applications due to their desirable properties at elevated temperatures (>1500°C). Limitations of refractory materials include their low ductility, poor oxidation resistance, and high manufacture cost using traditional techniques. Additive manufacturing (AM) can reduce material waste associated with manufacture, but AM fabrication is impacted by the brittleness of these refractory metals, resulting in excessive cracking during printing. Cracking reduces the effectiveness of hot isostatic pressing (HIP) which is commonly used to improve density and mechanical properties of AM components. The goal of this work is to improve refractory metal printability without majorly affecting the material properties which are the main reason these materials are used. Ceramic nanoparticles have been shown to help improve material properties after heat treatment. Results will be shown that demonstrate the effectiveness of adding nanoparticles to refractory metals. Additionally, there will be discussion regarding how these nanoparticles change the effect of heat treatments such as HIP compared with the AM pure metal samples.

Carly J. Romnes↗
NASA NTRSDate not supplied

Qualification of a Pulsed, Millinewton Class Metal Plasma Thruster for Broad Mission Applications

In the field of low power (<100W) electric propulsion, all thruster options demand significant trade-offs between operating parameters, reliability and scalable cost. With many systems on the market there are concerns with reliability, the need for extra considerations such as electron neutralizers for pure ion plumes, and the cost or craft compatibility of propellants. The Metal Plasma Thruster (MPT) is a new type of electric propulsion technology intended for low power applications. The system imparts momentum using inert, solid metal pucks as a propellant by using pulsed power to convert the metal into high velocity (~17km/s for Mo) jets of quasi-neutral plasma. The MPT technology does not require gas or liquid propellants, neutralizers, standby heaters, high voltage electronics, high electric or magnetic fields to operate. This comparatively simple pulsed operation is amenable to closed loop control, which provides for fine thrust control and S/C directed impulse on demand. Furthermore, the technology can use any metal as propellant, opening up unique opportunities for In-Situ Resource Utilization (ISRU) as well as customizability of performance for meeting specific mission needs. This paper describes implementation and direct measurement of this closed loop control mode as well as impulse measurement of multiple metals consistent with the aim of ISRU at NASA Glenn Research Center (GRC).

Electric Propulsion↗
NASA NTRSDate not supplied

Qualification of a Pulsed, Millinewton Class Metal Plasma Thruster for Broad Mission Applications

In the field of low power (<100W) electric propulsion, all thruster options demand significant trade-offs between operating parameters, reliability and scalable cost. With many systems on the market there are concerns with reliability, the need for extra considerations such as electron neutralizers for pure ion plumes, and the cost or craft compatibility of propellants. The Metal Plasma Thruster (MPT) is a new type of electric propulsion technology intended for low power applications. The system imparts momentum using inert, solid metal pucks as a propellant by using pulsed power to convert the metal into high velocity (~17km/s for Mo) jets of quasi-neutral plasma. The MPT technology does not require gas or liquid propellants, neutralizers, standby heaters, high voltage electronics, high electric or magnetic fields to operate. This comparatively simple pulsed operation is amenable to closed loop control, which provides for fine thrust control and S/C directed impulse on demand. Furthermore, the technology can use any metal as propellant, opening up unique opportunities for In-Situ Resource Utilization (ISRU) as well as customizability of performance for meeting specific mission needs. This paper describes implementation and direct measurement of this closed loop control mode as well as impulse measurement of multiple metals consistent with the aim of ISRU at NASA Glenn Research Center (GRC).

Electric Propulsion↗
NASA NTRS1994

(abstract) Studies on AB(sub 5) Metal Hydride Alloys with Sn Additives

The use of metal hydrides as negative electrodes in alkaline rechargeable cells is becoming increasingly popular, due to several advantages offered by the metal hydrides over conventional anode materials (such as Zn, Cd) in terms of specific energy environmental cycle life and compatibility. Besides, the similarities in the cell voltage pressure characteristics, and charge control methods of the Ni-MH cells to the commonly used Ni-Cd point to a projected take over of 25% of the Ni-Cd market for consumer electronics by the Ni-MH cells in the next couple of years. Two classes of metal hydrides alloys based on rare earth metals (AB(sub 5)) and titanium (AB(sub 2)) are being currently developed at various laboratories. AB(sub 2) alloys exhibit higher specific energy than the AB(sub 5) alloys but the state of the art commercial Ni-MH cells are predominately manufactured using AB(sub 5) alloys.

earth metals↗
NASA NTRS2013

Is There a Metallicity Ceiling to Form Carbon Stars? - A Novel Technique Reveals a Scarcity of C-Stars in the Inner M31 Disk

We use medium-band near-infrared (NIR) Hubble Space Telescope WFC3 photometry with model NIR spectra of Asymptotic Giant Branch (AGB) stars to develop a new tool for efficiently distinguish- ing carbon-rich (C-type) AGB stars from oxygen-rich (M-type) AGB stars in galaxies at the edge of and outside the Local Group. We present the results of a test of this method on a region of the inner disk of M31, where we nd a surprising lack of C stars, contrary to the ndings of previous C star searches in other regions of M31. We nd only 1 candidate C star (plus up to 6 additional, less certain C stars candidates), resulting in an extremely low ratio of C to M stars (C=M = (3.3(sup +20)(sub - 0.1) x 10(sup -4)) that is 1-2 orders of magnitude lower than other C/M estimates in M31. The low C/M ratio is likely due to the high metallicity in this region which impedes stars from achieving C/O > 1 in their atmospheres. These observations provide stringent constraints to evolutionary models of metal-rich AGB stars and suggest that there is a metallicity threshold above which M stars are unable to make the transition to C stars, dramatically affecting AGB mass loss and dust production and, consequently, the observed global properties of metal-rich galaxies.

Metallicity↗
NASA NTRS2013

The Metallicity Evolution of Low Mass Galaxies: New Contraints at Intermediate Redshift

We present abundance measurements from 26 emission-line-selected galaxies at z approx. 0.6-0.7. By reaching stellar masses as low as 10(exp 8) M stellar mass, these observations provide the first measurement of the intermediate-redshift mass-metallicity (MZ) relation below 10(exp 9)M stellar mass. For the portion of our sample above M is greater than 10(exp 9)M (8/26 galaxies), we find good agreement with previous measurements of the intermediate-redshift MZ relation. Compared to the local relation, we measure an evolution that corresponds to a 0.12 dex decrease in oxygen abundances at intermediate redshifts. This result confirms the trend that metallicity evolution becomes more significant toward lower stellar masses, in keeping with a downsizing scenario where low-mass galaxies evolve onto the local MZ relation at later cosmic times. We show that these galaxies follow the local fundamental metallicity relation, where objects with higher specific (mass-normalized) star formation rates (SFRs) have lower metallicities. Furthermore, we show that the galaxies in our sample lie on an extrapolation of the SFR-M∗ relation (the star-forming main sequence). Leveraging the MZ relation and star-forming main sequence (and combining our data with higher-mass measurements from the literature), we test models that assume an equilibrium between mass inflow, outflow, and star formation.We find that outflows are required to describe the data. By comparing different outflow prescriptions, we show that momentum, driven winds can describe the MZ relation; however, this model underpredicts the amount of star formation in low-mass galaxies. This disagreement may indicate that preventive feedback from gas heating has been overestimated, or it may signify a more fundamental deviation from the equilibrium assumption.

Low Mass↗
NASA NTRS2016

Metallic Hydrogen: A Game Changing Rocket Propellant

The objective of this research is to produce metallic hydrogen in the laboratory using an innovative approach, and to study its metastability properties. Current theoretical and experimental considerations expect that extremely high pressures of order 4-6 megabar are required to transform molecular hydrogen to the metallic phase. When metallic hydrogen is produced in the laboratory it will be extremely important to determine if it is metastable at modest temperatures, i.e. remains metallic when the pressure is released. Then it could be used as the most powerful chemical rocket fuel that exists and revolutionize rocketry, allowing single-stage rockets to enter orbit and chemically fueled rockets to explore our solar system.

Metallic↗
NASA NTRSDate not supplied

Adaptation of Metal Additive Manufacturing Processes for the International Space Station

The In-Space Manufacturing (ISM) project at NASA Marshall Space Flight Center, in a partnership with the company, Made in Space, has previously investigated 3D printing of polymer materials on-orbit. In recent years, the project has begun exploring the potential for metal additive manufacturing (AM) on future space missions to reduce logistics and enable point-of-use manufacturing for sparing and repair. This paper provides an overview of constraints for demonstrating a manufacturing process on the International Space Station (ISS) as well as information on previous trades of available metal AM processes and their potential for in-space use. There are currently two processes in development as payloads for an ISS technology demonstration: wire+arc additive manufacturing (the Vulcan payload from Made in Space, Inc.) and bound metal additive manufacturing (the Fabrication Laboratory from Techshot, Inc). An update on both of these systems, key results to date, and future development efforts will be presented. Relevant modeling work, performed by NASA Ames Research Center, to evaluate operation of certain aspects of the bound metal AM process in a microgravity environment will also be summarized.

in-space manufacturing↗