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At least 469 records · Page 26

Electron bunch position determination using a high frequency button beam position monitor in the AWAKE facility

The AWAKE facility uses novel proton beam-driven plasma wakefields to accelerate electron bunches over 10m of Rubidium plasma. Precise monitoring of 2 diverse beam types necessitates an electron beam position monitor (BPM) working in a frequency regime of tens of GHz. A high frequency conical button-style BPM with a working regime of up to 40 GHz has been investigated as a way to discriminate the electromagnetic fields of 19 MeV, 4 ps electron bunches propagating spatially and temporally together with a 400 GeV, 170 ps proton bunch in the AWAKE common beamline. The sensitivity of the HF BPM to the electron beam position is determined under various beam conditions, with both electrons and protons, and integration with a TRIUMF front-end is discussed.

43 PARTICLE ACCELERATORS↗

Analysis of DWPF Sludge Batch 6 (Macrobatch 7): Pour Stream Glass Samples

The Defense Waste Processing Facility (DWPF) began processing Sludge Batch 6 (SB6), also referred to as Macrobatch 7 (MB7), in June 2010. SB6 is a blend of the heel of Tank 40 from Sludge Batch 5 (SB5), H-Canyon Np transfers and SB6 that was transferred to Tank 40 from Tank 51.1 SB6 was processed using Frit 418. Sludge is received into the DWPF Chemical Processing Cell (CPC) and is processed through the Sludge Receipt and Adjustment Tank (SRAT) and Slurry Mix Evaporator Tank (SME). The treated sludge slurry is then transferred to the Melter Feed Tank (MFT) and fed to the melter. During processing of each sludge batch, the DWPF is required to take at least one glass sample to meet the objectives of the Glass Product Control Program (GPCP) and to complete the necessary Production Records so that the final glass product may be disposed of at a Federal Repository. The DWPF requested various analyses of radioactive glass samples obtained from the melter pour stream during processing of SB6 as well as reduction/oxidation (REDOX) analysis of MFT samples to determine the impact of Argon bubbling. Sample analysis followed the Task Technical and Quality Assurance Plan (TTQAP) and an Analytical Study Plan (ASP). Four Pour Stream (PS) glass samples and two MFT slurry samples were delivered to the Savannah River National Laboratory (SRNL) from the DWPF. Table 1-1 lists the sample information for each pour stream glass sample. SB6 PS3 (S03472) was selected as the official pour stream sample for SB6 and full analysis was requested. This report details the visual observations of the as-received SB6 PS No.3 glass sample as well as results for the chemical composition, Product Consistency Test (PCT), radionuclide content, noble metals, and glass density. REDOX results will be provided for all four pour stream samples and vitrified samples of MFT-558 and MFT-568A. Where appropriate, data from other pour stream samples will be provided.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Performance of Scintillation Detectors Based on Quantum Dots in a Semiconductor Matrix (Final Technical Report)

InAs Quantum Dots (QDs) embedded into GaAs semiconductor waveguide have unique scintillation properties, valuable for nuclear security, medical imaging, and high energy physics. In this work, we developed thick (~25um) epitaxial heterostructres with high luminescence efficiency composed of self-assembled nano-engineered InAs QDs grown by molecular beam epitaxy. In this type of detector, the GaAs matrix acts as a stopping material for charged particles or photons generating electrons captured by the QDs acting as luminescence centers. The QD medium is designed to provide fast capture of electrons into QDs (few ps), high QD luminescence efficiency at room temperature (>50%), and strong red-shift of photoluminescence (PL) from the GaAs absorption edge (>250nm). Typical devices consist of a 10-25um thick GaAs layer with embedded sheets of modulation p-type doped InAs QDs and an InGaAs photodetector tuned to the QD emission wavelength. The thick GaAs layer acts also as a waveguide when layer-transferred onto a low-index substrate. Waveguiding and self-absorption (~1cm -1 ) were studied using photoluminescence with scanning laser excitation and modeled with ray optics approximation and geometrical coupling of high-index waveguide to a collection fiber. Scintillating signals from α-particles were analyzed with both an external photodiode (PD) and an integrated PD which provided an improved optical coupling. In the former case, the external InGaAs PD was air-coupled to the scintillator and had the light collection efficiency of about 1% corresponding to limited light extraction through a planar interface with air due to total internal reflection. The mean charge collected by the integrated PD was in the range of (3÷5)×10 4 photoelectrons per 1 MeV of deposited energy, or ~13-20% of the theoretically achievable light yield. Timing of the integrated device was measured by wire-bonding it to the input of an 8 GHz IC. The scintillation response shows an extremely fast 0.3-0.6 ns decay constant and about 40-70 ps time resolution, limited by the system noise. The combined light yield and decay time makes the InAs/GaAs QD heterostructures the fastest high yield scintillation material reported making it valuable for high energy physics and medical imaging applications.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

Plasma Photonics: Manipulating Light Using Plasmas (Full Technical Final Report)

In this LDRD, we made significant advances on multiple fronts on the investigation and design of plasma-based optical structures to manipulate light at extreme intensities. We have unveiled new fundamental properties of laser-plasma interaction that were leveraged to introduce transformative applications. We first investigated new ways to generate high-amplitude plasma-based optical structures, based on the auto-resonance mechanism in order to produce refractive structures in plasmas. New insights into the interaction of such plasma structures with light waves allowed us to propose new methods for polarization manipulation and control for high-intensity lasers in the nonlinear regime, i.e. allowing the manipulation of an intense laser via its interaction with a less intense “control” laser beam in plasmas. Another application that we demonstrated experimentally is the capability to manipulate the velocity of light waves in plasmas by tailoring its refractive index; we reported the first demonstration of “slow light” and supra-luminal light propagation in plasmas. We also developed a new technological concept that would allow the probing of the type of plasma structures investigated in such applications, using high-bandwidth laser probing [Ludwig Phys. Plasmas 2019]. Finally, first steps were taken towards the demonstration of a plasma-based amplifier and compressor for the National Ignition Facility, in order to achieve powers equal of greater than those delivered by the Advanced Radiographic Capability (ARC). This technique uses a plasma-based grating acting like a compressor and amplifier, which could potentially compress and amplify an 88 ps, 56 J beam from the National Ignition Facility to <10 ps and hundreds of J.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Time-Lapse Vertical Seismic Profiling (VSP) for CO 2 Storage in a Depleted Oil Field in Northern Michigan

The Midwest Regional Carbon Sequestration Partnership (MRCSP) was founded in 2003 as part of the U.S. Department of Energy’s (DOE’s) Regional Carbon Sequestration Partnership initiative. Since its founding, MRCSP has made significant strides toward making CCUS a viable option for states in the region. The public/private consortium, funded through the DOE Regional Carbon Sequestration Initiative, brings together nearly 40 industry partners and 10 states. Battelle, as the project lead, oversees research, development and operations and coordinates activities among the partners. The incremental, phased approach has built a valuable knowledge base for the industry and paved the way for commercial-scale adoption of CCUS technologies. From 2008 to 2020, MRCSP Phase III focused on the development of large-scale injection projects. This report is part of a series of reports prepared under the Midwestern Regional Carbon Sequestration Partnership (MRCSP) Phase III (Development Phase). These reports summarize and detail the findings of the work conducted under the Phase III project. This report describes the Dover 33 VSP study to test the effectiveness of time-lapse Vertical Seismic Profile (VSP) for detecting and delineating a plume of more than 271,000 tonnes of CO2 injected into the Brown Niagaran and A-1 Carbonate formations within the Dover 33 reef between March 2013 and September 2016. Five 2D walkaway VSP (WVSP) source lines were acquired by SIGMA3 in September 2016 to investigate the possible time-lapse response in both P-wave and PS-wave seismic data. The data was compared to the same survey geometry acquired in March 2013 by SR2020. The seismic energy was recorded into an 80-level, three-component geophone array deployed into the Dover 1-33 well and placed just above the reef. P-wave and PS-wave reflection images were produced for each of the three source lines from both the 2013 baseline and 2016 monitor surveys. The images were then compared to look for changes in the reflectivity at and around the injection location that might indicate how the CO 2 has moved over this time period. This technique revealed several localized areas with sizable impedance differences inside the reef where CO 2 would be expected; however, a large number of similar impedance “hotspots” were also detected outside the reef in areas where injected CO 2 would not be expected. Therefore, a second analysis that involved calculating P-wave and S-wave travel time differences between the 2013 and 2016 VSPs was conducted to look for a change that could be caused by the CO 2 plume.

01 COAL, LIGNITE, AND PEAT↗

Atomic Force Microscope Active Optical Probe for Single-Molecule Imaging and Time-Resolved Optical Spectroscopy (DOE SBIR Phase II/IIA Final Report)

Actoprobe LLC reports on the results of its DOE SBIR Phase II/IIA project on the development of Atomic Force Microscope Active Optical Probe for Single-Molecule Imaging and Time-Resolved Optical Spectroscopy. While chemistry science and technology greatly benefit from Atomic Force Microscopy in surface characterization, time-resolved chemical imaging on the single-molecule level lags far behind. Current scanning probe microscopy only obtains information about mechanical but not optical/chemical properties. To address this problem, the Actoprobe LLC research team has proposed a novel class of Atomic Force Microscopy probes, Ultra-Fast Pulsed Active Atomic Force Microscopy Optical Probes (UFP AAOPs), that will allow ultrafast time-resolved optical and chemical imaging at the nanoscale. As envisioned, these unique optical probes will perform the functions of conventional Atomic Force Microscopy probes and, in addition, will simultaneously provide chemical information about molecular scale interactions. This innovation is accomplished by integrating an ultrafast pulsed Quantum Dot laser source into an Atomic Force Microscopy probe. This report describes our progress with the fabrication of an ultrafast micrometer-size semiconductor laser, based on “artificial atoms” - Quantum Dots, integrated with an Atomic Force Microscopy probe. In this Phase II/IIA project, we have demonstrated the feasibility of the UFP AAOP concept by fabricating a first prototype of the UFP AAOP. The excellent performance of the probe has been proven in terms of AFM and optical spatial resolution through rigorous tests. The UFP AAOP provides pulses with less than 4 ps duration and higher than 11 GHz repetition rate, and spatial resolution better than 300 nm at 1240 nm wavelength. Technically, it is possible to reduce the pulse width to less than 1 ps and to improve lateral resolution to ~ 0.5 nm, which implies the potential capability for the probe to characterize chemical compounds with single-molecule resolution. The UFP AAOP fabrication procedure has been developed for wafer-scale production of multiple devices, with the yield of the process estimated to be lower than 1% with the limited fabrication capabilities and equipment available for use in the research project. However, using high-volume production tools and special GaAs processing equipment, the yield can be significantly improved, theoretically to ~ 50%. Finally, economic feasibility and scale-up manufacturing potential were analyzed for UFP AAOP and found to be very promising. In summary, the Actoprobe team has successfully demonstrated the feasibility of the UFP AAOP concept.

36 MATERIALS SCIENCE↗

Use of Electronic Laboratory Notebooks (ELN) in a Laboratory Information Management System (LIMS) [Slides]

The Actinide Analytical Chemistry (CAAC) group at Los Alamos National Laboratory (LANL) uses the LabWare LIMS (LabWare 7) system to manage our samples and material at risk. The LIMS system also provides other functionality which the Plasma Spectroscopy (PS) team has developed along with our LIMS team to provide streamlining and automation of all sample related actions required by PS.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

A Functional Reference Architecture and Assessment Thereof for the National Ignition Facility Industrial Controls Systems

The Industrial Control System (ICS) at the National Ignition Facility (NIF) has an effective, well-established architecture based off a conventional cyclical software paradigm focused on maintainability and the identification of issues. This architecture exhibits scalability in ensuring expansions of the system conform to the existing architecture, modularity enough to allow relatively easy integrations of such expansions and works as a successful tool to introduce control system engineers new to the NIF ICS to the structure of the system at each layer. This architecture, like most software architectures, is object-oriented, lending itself to ease of understanding by control systems engineers and software engineers familiar with an object-oriented perspective. There are occasions, however, where engineers of other disciplines require insight into the functionality and structure of the ICS for the purposes of understanding fundamentally how their own system is or will be governed by the ICS, without the need for the details of operation of the ICS or the object-oriented view. For this reason, a functional architecture of the ICS could be a potent tool for communicating this insight. Even more powerful, a generalization of this proposed functional ICS architecture in the form of a National Ignition Facility and Photon Science (NIF & PS) Industrial Controls Reference Architecture could communicate this insight not just to systems governed by the ICS in the NIF proper, but across entirety of the NIF & PS Principal Associate Directorate (PAD), anywhere an instance of the ICS architecture is present, such as the approximately 40 “small labs” distributed across the directorate. Such a tool will provide an alternative means of understanding the implementation of these control systems, conducive to a larger variety of engineering and scientific disciplines.

42 ENGINEERING↗

Automation and Quality Control for CMS Outer Tracker Module Assembly at Fermilab’s SiDet

Automation and quality control techniques for 2S and PS sensor modules for the CMS Outer Tracker for the HL-LHC era have been developed at the Silicon Detector facility at Fermilab. Examples include a laser scanning procedure to check manufacturing specifications for the 2S sensor modules, and an automated gluing process to accurately assemble PS sensor modules. Processes were verified and documented for the production stage of the Outer Tracker.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Analysis of the Sludge Batch 9 (Macrobatch 11) DWPF Pour Stream Glass Sample

A pour stream (PS) sample taken near the end of processing of Sludge Batch 9 (SB9, Macrobatch 11) with the Nitric-Formic Acid Flowsheet was analyzed by the Savannah River National Laboratory to comply with the Defense Waste Processing Facility (DWPF) Glass Product Control Program. The SB9 PS sample was taken on 5/28/2022 during Melter Feed Batch 815 associated with glass canister S04741, and was transferred to SRNL in Primary Container PC0136.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

From ETROC to VTROC

The Endcap Timing ReadOut Chip (ETROC) is designed to process LGAD signals with time resolution down to about 40-50ps per hit, to reach 30-35ps per track with two detector layers. The ETROC2 is the first full size (16x16) prototype design and is fully compatible with the final chip specifications in terms of functionality. The ETROC2 has been extensively tested recently. In this talk, the testing results of the ETROC2 will be presented first, including performance study using charge injection, laser and beam, as well as TID testing and wafer probe testing to study the yield. In addition, future challenges of precision position and timing ASIC design will be discussed, based on what we have learned from the ETROC development, and how the challenges could be addressed in the VTROC, Vertically integrated Timing ReadOut chip (funded as SBIR phase 2) for precision position and timing detector R&D.

Liu, Ted↗

Analysis of the Sludge Batch 9 (Macrobatch 11) DWPF Pour Stream Glass Sample Collected During the Nitric-Glycolic Acid Flowsheet Transition

A pour stream (PS) sample taken near the end of processing of Sludge Batch 9 (SB9, Macrobatch 11) during the transition to the nitric-glycolic acid (NGA) flowsheet was analyzed by the Savannah River National Laboratory (SRNL). The SB9 NGA PS sample was taken on 12/18/2022 during Melter Feed Batch 823 associated with glass canister S04773 and was transferred to SRNL in Primary Container PC0139 in February 2023.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Characterization of ORNL PSD ASIC

The performance of the ORNL ASIC and its readout system was tested with pixelated organic scintillators. We use a pixelated trans-Stilbene scintillator array from Inrad Optics and a pixelated organic glass scintillator array developed at Sandia National Laboratories to characterize the energy and timing resolutions and the pulse-shape discrimination (PSD) figure-of-merit (FoM). The results are compared to previous work in which the same metrics were measured on waveforms digitized at 250 MHz with 14-bit resolution. We found that the PSD FoM at 340 keVee of the ASIC configuration compared to waveform data varied with the scintillator type. We measured a PSD FoM of 1.12 ± 0.14 with the ASIC configuration versus 1.39 ± 0.23 with waveform data using the trans-Stilbene array. We measured a PSD FoM of 0.52 ± 0.18 with the ASIC configuration versus 1.25 ± 0.19 with waveform data using the the organic glass scintillator array. The coincidence timing resolution was measured using two 6x6x6 mm 3 cubes of trans-Stilbene. It was measured to be 805 ± 9 ps with the ASIC configuration versus 300 ps on average with waveform data.

42 ENGINEERING↗

Beam test results for the Endcap Timing ReadOut Chip (ETROC2) for the CMS ETL upgrade

The Endcap Timing ReadOut Chip (ETROC) for the Compact Muon Solenoid (CMS) Minimum ionizing particle Timing Detector (MTD) is designed to process Low Gain Avalanche Diode (LGAD) signals with a time resolution of 40-50ps per hit, with 30-35 ps per charged particle using two layer detector. The ETROC2, is the first full size (16x16 pixels) and full functionally design that has been tested in hadron and electron beams at CERN and DESY (Sep 2023 - June 2024). Precision timing studies at these test beams are done using a self-referential beam telescope composed of up to 4 layers/chips. This talk describes the ETROC2 beam telescope and summarizes the performance of the ETROC2 chips bump-bonded to (16x16) Fondazione Bruno Kessler (FBK) and Hamamatsu Photonics K.K. (HPK) LGAD sensors using results from recent test beams. The experiences and lessons learned during the course of these test beams are also detailed in this talk.

Safdari, Murtaza↗

28nm front end ASIC and 12” LGADs for 3D integration

The 3DIntSenS Collaboration—a joint effort between SLAC, Fermilab, and LLNL—is developing enabling technologies for next-generation radiation imaging detectors that combine ultra-fine spatial resolution (≈10 μm) with precision timing (<20 ps), while maintaining low power <1 W/cm2 and high data throughput. The approach leverages 3D integration between advanced CMOS readout ASICs and finely pixelated LGAD sensors to achieve the performance and scalability required for large-area, high-rate applications. High-granularity, precision-timing detectors are essential for scientific advances in HEP, NP, BES, and FES, but widespread adoption is limited by the cost and complexity of 3D integration. To close this gap, the collaboration is developing LGAD sensors compatible with 12-inch commercial CMOS processes, enabling cost-effective integration with high-performance ASICs under development. We present the design and results from a 28 nm CMOS ASIC prototype, including a low-jitter front end, and in-pixel TDC demonstrating sub-10 ps timing resolution. We also report on the co-design and characterization of reticle-scale LGAD sensors with 50 μm and 100 μm pixels and introduce the next 10k-pixel ASIC designed for full 3D integration. These advances represent a critical step toward scalable, high-resolution radiation imaging systems for future scientific instrumentation.

England, Troy [Fermilab] (ORCID:0000000154405255)↗

Flat TBPS Integration Testing for the CMS Outer Tracker Upgrade

The upcoming High-Luminosity (HL) LHC will significantly increase luminosity, introducing more demanding operating conditions for the CMS detector. To meet these challenges, CMS is undergoing major upgrades, including a complete replacement of its tracking detector. This poster presents recent integration testing efforts conducted at Fermilab on the Flat Tracker Barrel with pixel-strip (PS) modules integration test stand, a subcomponent of the outer tracker located in the central barrel region. In this region, PS modules are mounted on structures that provide mechanical support and cooling, called planks. The testing focuses on validating the integrated system’s thermal and electrical performance. Results from these tests will be discussed, highlighting their importance for ensuring reliable tracker operation in the HL-LHC era.

Salazar Segovia, Itzelli [UC, Davis]↗

Evaluation of Howard A. Hanson Dam Juvenile Fish Passage and Survival Study: Downstream Passage and Survival (Acoustic Telemetry) (Task Final Report)

The Downstream Passage and Survival (Acoustic Telemetry) task was one of several tasks for the Evaluation of Howard A. Hanson Dam (HAHD) Juvenile Fish Passage and Survival study. For this task, a juvenile fish passage and survival study was conducted at HAHD from March 10, 2024 through June 27, 2024 for arrays in the HAHD Reservoir and Green River, and through July 9, 2024 for the arrays in the Duwamish River. Fish releases occurred over four times from March through May. Active tag (acoustic telemetry) technology was used to provide biological baseline information for the passage and survival of juvenile Puget Sound (PS) Chinook salmon (Oncorhynchus tshawytscha). Results will be used by biologists, engineers, resource managers, and regional decision-makers to inform the engineering design of the new fish passage facility (FPF) at HAHD. However, hatchery sub-yearling PS Chinook salmon of the appropriate size for tag implantation during the study period (> 95 mm in fork length, Geist et al. 2018) were unavailable. Therefore, yearling Coho salmon (O. kisutch) were used as a surrogate species for this acoustic telemetry study.

13 HYDRO ENERGY↗

Two 28-nm front-end ASICs for ultra-fine spatial resolution and precision timing to be 3D integrated with 12 LGADs

The 3DIntSenS Collaboration—a joint effort between SLAC, Fermilab, and LLNL—is developing enabling technologies for next-generation radiation imaging detectors that combine ultra-fine spatial resolution (about 10 µm) with precision timing (<20 ps), while maintaining low power <1 W/cm2 and high data throughput. The approach leverages 3D integration between advanced CMOS readout ASICs and finely pixelated LGAD sensors to achieve the performance and scalability required for large-area, high-rate applications. High-granularity, precision-timing detectors are essential for scientific advances in HEP, NP, BES, and FES, but widespread adoption is limited by the cost and complexity of 3D integration. To close this gap, the collaboration is developing LGAD sensors compatible with 12-inch commercial CMOS processes, enabling cost-effective integration with high-performance ASICs under development. We present two 28 nm CMOS ASIC prototypes, including a low-jitter front end, and in-pixel TDC demonstrating sub-10 ps timing resolution. These advances represent a critical step toward scalable, high-resolution radiation imaging systems for future scientific instrumentation.

England, Troy [Fermilab] (ORCID:0000000154405255)↗