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At least 469 records · Page 26

Cluster 1: commercializing additive manufacturing—hurdles in materials characterization and testing

A major challenge in the commercialization of additive manufactured (AM) materials and processes is the ability to achieve acceptance of processes and products. There has been some progress towards acceptance has been made by adapting legacy qualification paradigms to match with the very limited process control and monitoring offered by AM machines. The opportunity for in-situ measurement can provide process monitoring and control perhaps changing the way we qualify parts however it is limited by lack of adequate process measurement methods. New measurement techniques, sensors and correlations to relevant phenomena are needed that enable process control and monitoring for consistently producing high quality articles. Beyond process data we need to characterize uncertainties of performance in all aspects of material, process and final part. These are prerequisites to achieving articles that are indeed worthy of materials characterization efforts that establish a microstructural reference of desirable performance through process-structure-property relations. Only then can industry apply physics based understanding of the material, part and process to probabilistically predict performance of an AM part. Our paper provides a brief overview, discussion of hurdles and key areas where R&D investment is needed.

36 MATERIALS SCIENCE↗

A fiber-optic probe for particle sizing in concentrated suspensions

A fiber-optic probe employing two monomode optical fibers, one for transmitting a Gaussian laser beam to the scattering volume and the second, positioned at some backscatter angle, for receiving the scattered light is described. Performance and suitability of the system for a process control environment is assessed by studying a suspension of polystyrene latex particles over a wide range of sizes and concentrations. The results show that the probe is ideal for a process control environment in industrial and laboratory applications. Particle size is recovered, without any additional corrections for multiple light scattering, in concentrations containing up to 10 percent solids of 39-nm polystyrene latex spheres.

Dhadwal, Harbans S.↗

Regulatory Aspects of the Human Factors Engineering Process in Control Room Modernization

This report describes the basic aspects of control room modernization projects in the U.S. nuclear industry and the need for supplementary guidance on the integration of human factors considerations into the licensing and regulatory aspects of digital upgrades. The report pays specific attention to the integration of principles described in NUREG-0711 (Human Factors Engineering Program Review Model) and how supplementary guidance can help to raise general awareness in the industry regarding the complexities of control room modernization projects created by many interdependent regulations, standards and guidelines. The report also describes how human factors engineering principles and methods provided by various resources and international standards can help in navigating through the process of licensing digital upgrades. In particular, the integration of human factors engineering guidance and requirements into the process of licensing digital upgrades can help reduce uncertainty related to development of technical bases for digital upgrades that will avoid the introduction of new failure modes.

99 GENERAL AND MISCELLANEOUS↗

IMPACT OF URANIUM AND THORIUM ON HIGH TIO2 CONCENTRATION NUCLEAR WASTE GLASSES

This study focused on the potential impacts of the addition of Crystalline Silicotitanate (CST) and Monosodium Titanate (MST) from the Small Column Ion Exchange (SCIX) process on the Defense Waste Processing Facility (DWPF) glass waste form and the applicability of the DWPF process control models. MST from the Salt Waste Processing Facility (SWPF) is also considered in the study. The KT08-series of glasses was designed to evaluate any impacts of the inclusion of uranium and thorium in glasses containing the SCIX components. All but one of the study glasses were found to be amorphous by X-ray diffraction (XRD). One of the slowly cooled glasses contained a small amount of trevorite, which is typically found in DWPF-type glasses and had no practical impact on the durability of the glass. The measured Product Consistency Test (PCT) responses for the study glasses and the viscosities of the glasses were well predicted by the current DWPF models. No unexpected issues were encountered when uranium and thorium were added to the glasses with SCIX components.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Mapping Glacier Basal Sliding Applying Machine Learning

During the RESOLVE project (“High-resolution imaging in subsurface geophysics: development of a multi-instrument platform for interdisciplinary research”), continuous surface displacement and seismic array observations were obtained on Glacier d’Argentière in the French Alps for 35 days in May 2018. The data set is used to perform a detailed study of targeted processes within the highly dynamic cryospheric environment. In particular, the physical processes controlling glacial basal motion are poorly understood and remain challenging to observe directly. Especially in the Alpine region for temperate based glaciers where the ice rapidly responds to changing climatic conditions and thus, processes are strongly intermittent in time and heterogeneous in space. Spatially dense seismic and Global Positioning System (GPS) measurements are analyzed applying machine learning to gain insight into the processes controlling glacial motions of Glacier d’Argentière. Using multiple bandpass-filtered copies of the continuous seismic waveforms, we compute energy-based features, develop a matched field beamforming catalog and include meteorological observations. Features describing the data are analyzed with a gradient boosting decision tree model to directly estimate the GPS displacements from the seismic noise. We posit that features of the seismic noise provide direct access to the dominant parameters that drive displacement on the highly variable and unsteady surface of the glacier. The machine learning model infers daily fluctuations and longer term trends. The results show on-ice displacement rates are strongly modulated by activity at the base of the glacier. The techniques presented provide a new approach to study glacial basal sliding and discover its full complexity.

58 GEOSCIENCES↗

An Automated SVD for Alignment and Control of James Webb Space Telescope Mirrors

The James Webb Space Telescope (JWST) is a three-mirror anastigmatic telescope. The alignment of the segmented primary and secondary mirrors in the wavefront sensing and control process involves a series of actuators to control the six degrees-of-freedom motion on each surface in addition to the radius of curvature. The control matrix developed from the alignment parameters is over-determined and singular value decomposition (SVD) method is used to solve it in the least square sense. An automated SVD scheme has been developed to identify the most contributing modes in a typical alignment process and reduce the impact of error-prone modes from the control process.

Shiri, Sharam↗

Light Water Reactor Sustainability Program: Advanced Instrumentation, Information, and Control Systems Technologies Technical Program Plan for 2013

Reliable instrumentation, information, and control (II&C) systems technologies are essential to ensuring safe and efficient operation of the U.S. light water reactor (LWR) fleet. These technologies affect every aspect of nuclear power plant (NPP) and balance-of-plant operations. In 1997, the National Research Council conducted a study concerning the challenges involved in modernizing existing analog-based instrumentation and controls with digital instrumentation and control systems in NPPs. Their findings identified the need for new II&C technology integration. The objective of these efforts is to develop, demonstrate, and support deployment of new digital II&C technologies for nuclear process control, enhance worker performance, and provide enhanced monitoring capabilities to ensure the continued safe, reliable, and economic operation of the nation’s NPPs. Digital II&C technologies are deployed in a number of power generation settings worldwide. Current instrumentation and human-machine interfaces in the nuclear power sector employ analog technologies. In other power generation sectors, analog technologies have largely been replaced with digital technologies. This is in part due to the manufacturing and product support base transitioning to these newer technologies. It also accompanies the transition of education curricula for I&C engineers to digital technologies. Consequently, product manufacturers refer to analog I&C as having reached the end of its useful service life. Although considered obsolete by other industries, analog I&C continues to function reliably, though spare and replacement parts are becoming increasingly scarce as is the workforce that is familiar with and able to maintain it. Analog I&C was also the predominant means used for process control in an era when human labor was more affordable, and maintaining an I&C technology base through a larger workforce conducting frequent rounds for surveillances, inspections, and tests was accepted in the nuclear power generation business model. Today’s power generation business climate is much different and II&C technologies are needed in the long run that are more highly automated and require less cost to operate and maintain, are as highly reliable as those used today, and will be familiar to a future work force. They should also enable performance gains for the utility so that they are not merely a sunken cost, as this would weigh heavily on the balance sheet at a time of particularly high cost competitiveness in electricity markets.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

A Data-Driven Solution for Performance Improvement

Marketed as the "Software of the Future," Optimal Engineering Systems P.I. EXPERT(TM) technology offers statistical process control and optimization techniques that are critical to businesses looking to restructure or accelerate operations in order to gain a competitive edge. Kennedy Space Center granted Optimal Engineering Systems the funding and aid necessary to develop a prototype of the process monitoring and improvement software. Completion of this prototype demonstrated that it was possible to integrate traditional statistical quality assurance tools with robust optimization techniques in a user- friendly format that is visually compelling. Using an expert system knowledge base, the software allows the user to determine objectives, capture constraints and out-of-control processes, predict results, and compute optimal process settings.

Source record↗

Wide emission-tunable CdTeSe/ZnSe/ZnS core–shell quantum dots and their conjugation with E. coli O-157

Highlights: • QDs with variety morphology were obtained via an injection controlled process. • 3-D PL spectra of core–shell QDs show different excitation wavelength dependence. • The PL intensity of QDs with ZnSe transition layer increases dramatically. • Core–shell QDs were processed into aqueous phase and conjugated with E. coli O-157. - Abstract: Wide emission-tunable and different morphological alloyed CdTeSe quantum dots (QDs), CdTeSe/ZnS and CdTeSe/ZnSe/ZnS core–shell QDs were successfully synthesized via an injection controlled process. The effect of injection procedure and reaction temperature were systematically discussed and the growth mechanism was proposed. Most efficient PL wavelength was correlated with reaction time and temperature. The 3-D PL spectra of spherical bare CdTeSe and core–shell QDs with different passivation showed different excitation wavelength dependency. The PL intensity of CdTeSe/ZnSe/ZnS core–shell QDs increased greatly in comparison with that of CdTeSe and CdTeSe/ZnSe QDs. ZnSe transition layer played an important role in improving the PL intensity by providing a smoothened interface and gradient band offsets. The core–shell QDs were transferred into aqueous phase and successfully conjugated with Escherichia coli O-157. The proposed phase-transfer and bio-labeling strategy may be applicable to various QDs with different compositions.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

External Tank Program - Legacy of Success

The largest single element of Space Shuttle is the External Tank (ET), which serves as the structural backbone of the vehicle during ascent and provides liquid propellants to the Orbiter s three Main Engines. The ET absorbs most of the seven million pounds of thrust exerted by the Solid Rocket Boosters and Main Engines. The design evolved through several block changes, reducing weight each time. Because the tank flies to orbital velocity with the Space Shuttle Orbiter, minimization of weight is mandatory, to maximize payload performance. The initial configuration, the standard weight tank, weighed 76,000 pounds and was an aluminum 2219 structure. The light weight tank weighed 66,000 pounds and flew 86 missions. The super light weight tank weighed 58,500 pounds and was primarily an aluminum-lithium structure. The final configuration and low weight enabled system level performance sufficient for assembly of the International Space Station in a high inclination orbit, vital for international cooperation. Another significant challenge was the minimization of ice formation on the cryogenic tanks. This was essential due to the system configuration and the choice of ceramic thermal protection system materials on the Orbiter. Ice would have been a major debris hazard. Spray on foam insulation materials served multiple functions including thermal insulation, conditioning of cryogenic propellants, and thermal protection for the tank structure during ascent and entry. The tank is large, and unique manufacturing facilities, tooling, and handling, and transportation operations were developed. Weld processes and tooling evolved with the design as it matured through several block changes. Non Destructive Evaluation methods were used to assure integrity of welds and thermal protection system materials. The aluminum-lithium alloy was used near the end of the program and weld processes and weld repair techniques had to be refined. Development and implementation of friction stir welding was a substantial technology development incorporated during the Program. Automated thermal protection system application processes were developed for the majority of the tank surface. Material obsolescence was an issue throughout the multi-decade program. Process controls were implemented to assure cleanliness in the production environment, to control contaminants, and to preclude corrosion. Each tank was accepted via rigorous inspections, including non-destructive evaluation techniques, proof testing, and all systems testing. In the post STS-107 era, the project focused on ascent debris risk reduction. This was accomplished via stringent process controls, post flight assessment using substantially improved imagery, and selective redesigns. These efforts were supported with a number of test programs to simulate combined environments. The debris risk was reduced by two orders of magnitude. During this time a major natural disaster was overcome when hurricane Katrina damaged the manufacturing facility. Numerous lessons from these efforts, the manufacturing and material processing issues, the key design features, and evolution of the design will be discussed.

Pilet, Jeffery C.↗

Optimization of Residual Stresses in MMC's through Process Parameter Control and the use of Heterogeneous Compensating/Compliant Interfacial Layers. OPTCOMP2 User's Guide

A user's guide for the computer program OPTCOMP2 is presented in this report. This program provides a capability to optimize the fabrication or service-induced residual stresses in unidirectional metal matrix composites subjected to combined thermomechanical axisymmetric loading by altering the processing history, as well as through the microstructural design of interfacial fiber coatings. The user specifies the initial architecture of the composite and the load history, with the constituent materials being elastic, plastic, viscoplastic, or as defined by the 'user-defined' constitutive model, in addition to the objective function and constraints, through a user-friendly data input interface. The optimization procedure is based on an efficient solution methodology for the inelastic response of a fiber/interface layer(s)/matrix concentric cylinder model where the interface layers can be either homogeneous or heterogeneous. The response of heterogeneous layers is modeled using Aboudi's three-dimensional method of cells micromechanics model. The commercial optimization package DOT is used for the nonlinear optimization problem. The solution methodology for the arbitrarily layered cylinder is based on the local-global stiffness matrix formulation and Mendelson's iterative technique of successive elastic solutions developed for elastoplastic boundary-value problems. The optimization algorithm employed in DOT is based on the method of feasible directions.

Pindera, Marek-Jerzy↗

Change in terrestrial ecosystem water‐use efficiency over the last three decades

Abstract Defined as the ratio between gross primary productivity ( GPP ) and evapotranspiration ( ET ), ecosystem‐scale water‐use efficiency ( EWUE ) is an indicator of the adjustment of vegetation photosynthesis to water loss. The processes controlling EWUE are complex and reflect both a slow evolution of plants and plant communities as well as fast adjustments of ecosystem functioning to changes of limiting resources. In this study, we investigated EWUE trends from 1982 to 2008 using data‐driven models derived from satellite observations and process‐oriented carbon cycle models. Our findings suggest positive EWUE trends of 0.0056, 0.0007 and 0.0001 g C m −2 mm −1 yr −1 under the single effect of rising CO 2 (‘ CO 2 ’), climate change (‘ CLIM ’) and nitrogen deposition (‘ NDEP ’), respectively. Global patterns of EWUE trends under different scenarios suggest that (i) EWUE ‐ CO 2 shows global increases, (ii) EWUE ‐ CLIM increases in mainly high latitudes and decreases at middle and low latitudes, (iii) EWUE ‐ NDEP displays slight increasing trends except in west Siberia, eastern Europe, parts of North America and central Amazonia. The data‐driven MTE model, however, shows a slight decline of EWUE during the same period (−0.0005 g C m −2 mm −1 yr −1 ), which differs from process‐model (0.0064 g C m −2 mm −1 yr −1 ) simulations with all drivers taken into account. We attribute this discrepancy to the fact that the nonmodeled physiological effects of elevated CO 2 reducing stomatal conductance and transpiration ( TR ) in the MTE model. Partial correlation analysis between EWUE and climate drivers shows similar responses to climatic variables with the data‐driven model and the process‐oriented models across different ecosystems. Change in water‐use efficiency defined from transpiration‐based WUE t ( GPP / TR ) and inherent water‐use efficiency ( IWUE t , GPP × VPD / TR ) in response to rising CO 2 , climate change, and nitrogen deposition are also discussed. Our analyses will facilitate mechanistic understanding of the carbon–water interactions over terrestrial ecosystems under global change.

Huang, Mengtian↗

Comparative ionospheres. I - The inner planets. II - The outer planets

A description is given first of the fundamental physical and chemical processes controlling the thermospheres and ionospheres of the inner planets, Venus and Mars. A comparison is made between the neutral composition and temperature structure of Venus and Mars and those of the earth. Consideration is then given to the chemical and diffusion processes in the ionosphere. After a brief treatment of the ionospheric energetics and heat sources, the mechanisms underlying the maintenance of the nightside ionosphere of Venus are reviewed. A description is then given of the upper atmospheres and ionospheres of the major planets, Jupiter and Saturn. The treatment of the temperature structure and composition of the thermospheres of the major planets includes a description of the physical and chemical processes controlling the hydrocarbons and atomic hydrogen. A comparison is then made between the ionospheres of the major planets and those of the inner planets. It is noted that Io and Titan also have atmospheres and ionospheres, and these are treated briefly. Even though comets cannot be classed as planets, they have atmospheres and ionospheres that are not gravitationally confined.

Cravens, T. E.↗

Lower Tropospheric Processes: A Control on the Global Mean Precipitation Rate

The spread in global mean precipitation among climate models is explored in two ensembles using the complementary perspectives of surface evaporation and energy budgets. Models with higher global mean precipitation have stronger oceanic evaporation, driven by drier near-surface air. The drier surface conditions occur alongside increases in near-surface temperature and moisture at 925 hPa, which point to stronger boundary layer mixing. Correlations suggest that the degree of lower tropospheric mixing explains 18%–49% of the intermodel precipitation variance. To test this hypothesis, the degree of mixing is indirectly varied in a single-model experiment by adjusting the relative humidity threshold that controls low-cloud fraction. Indeed, increasing lower tropospheric mixing results in more global mean precipitation. Energetically, increased precipitation rates are associated with more downwelling longwave radiation to the surface and weaker sensible heat fluxes. These results highlight how lower-tropospheric processes must be better constrained to reduce the precipitation discrepancy among climate models.

58 GEOSCIENCES↗

Creep and microstructural processes in a low-alloy 2.25%Cr1.6%W steel (ASTM Grade 23)

A low-alloy 2.25%Cr1%Mo steel (ASTM Grade 22) has been greatly improved by the substitution of almost all of the 1%Mo by 1.6%W. The improved material has been standardized as P/T23 steel (Fe–2.25Cr–1.6W–0.25V–0.05Nb–0.07C). The present investigation was conducted on T23 steel in an effort to obtain a more complete description and understanding of the role of the microstructural evolution and deformation processes in high-temperature creep. Constant load tensile creep tests were carried out in an argon atmosphere in the temperature range 500–650 °C at stresses ranging from 50 to 400 MPa. It was found that the diffusion in the matrix lattice is the creep-rate controlling process. The results of an extensive transmission electron microscopy (TEM) analysis programme to investigate microstructure evolution as a function of temperature are described and compared with the thermodynamic calculations using the software package Thermo-Calc. The significant creep-strength drop of T23 steel after long-term creep exposures can be explained by the decrease in dislocation hardening, precipitation hardening and solid solution hardening due to the instability of the microstructure at high temperature. - Highlights: • The constant load creep tests of T23 steel were carried out at 500–650 °C. • The stress exponents of the creep rate correspond to power law (dislocation) creep. • Diffusion in the matrix lattice is the creep-rate controlling process. • The microstructure instability is the main creep degradation process in T23 steel.

36 MATERIALS SCIENCE↗

Causal Trends for Occurrences at Sandia National Laboratories

A variety of issues and occurrences are reported at Sandia National Laboratories every year. The challenge is to filter through these occurrences and determine whether there are any notable trends related to work planning and control processes and whether some of the common problems can be mitigated or prevented. The hope is that some of the more common issues can be improved through training, communication, and/or documentation. These causal trends may also help to improve current training and work planning and control processes by revealing some opportunities for improvement.

42 ENGINEERING↗

Development of a Computer-Controlled Polishing Process for X-Ray Optics

The future X-ray observatory missions require grazing-incidence x-ray optics with angular resolution of < 5 arcsec half-power diameter. The achievable resolution depends ultimately on the quality of polished mandrels from which the shells are replicated. With an aim to fabricate better shells, and reduce the cost/time of mandrel production, a computer-controlled polishing machine is developed for deterministic and localized polishing of mandrels. Cylindrical polishing software is also developed that predicts the surface residual errors under a given set of operating parameters and lap configuration. Design considerations of the polishing lap are discussed and the effects of nonconformance of the lap and the mandrel are presented.

Khan, Gufran S.↗

Containerless High Temperature Property Measurements by Atomic Fluorescence

Laser induced fluorescence (LIF) provides a noncontact method for measuring high temperature properties. It is used with aerodynamic and/or electromagnetic levitation, and electromagnetic and/or CW CO2 laser heating to develop new methods for containerless high temperature property measurements and process control. The capabilities and limitations of Earth-based experiments are demonstrated and the information necessary to design improved experiments in space is obtained. The LIF methods were developed to measure temperature and component activities, which will be applied to containerless property measurements on liquids and to process control in synthesis experiments. Component activities will be obtained from relative LIF intensities over a compound and its components at the same temperature.

Nordine, P. C.↗