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At least 469 records · Page 26

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NASA NTRS1984

SPAR X Technical Report for Experiment 76-22 Directional Solidification of Magnetic Composites

The effects of gravity on Bridgman-Stockbarger directional solidification of off-eutectic Bi/MnBi were studied in reduced gravity aboard the SPAR X flight and compared to normal-gravity investigations and previous eutectic Bi/MnBi SPAR flight experiments. The directional solidification of off-eutectic Bi/MnBi results in either a dendritic structure connected with local cooperative growth or a coupled low volume fraction faceted/non faceted aligned rod eutectic whose Mn macrosegregation, MnBi rod size, interrod spacing, and thermal and magnetic properties are sensitive functions of the solidification processing conditions. Two hypoeutectic and two hypereutectic samples were solidified during 605 sec of furnace travel, with an initial 265 sec low-gravity interval. Comparison Earth-gravity samples were solidified in the same furance assembly under identical processing conditions. Macrosegregation in the low-g samples was consistent with a metastable increase in Mn solubility in the Bi matrix, in partial agreement with previous Bi/MnBi SPAR findings of MnBi volume reduction.

Bethin, J.↗

NASA NTRS1985

Gravity Perception in a Cladoceran-zooplankter: Anatomy of Antennal Socket Setae of Daphnia Magna

Night orientation in Daphnia magna was recently associated with setae on the basal socket of the swimming antennae. Daphnids are suspected of maintaining nocturnal equilibrium by monitoring the gravity vector through upward setal deflections caused by sinking between antennal swimming strokes. Setae appear to be hydrodynamic rheoceptors that sense the gravity vector indirectly by mechanoreceptivity to the direction and velocity of water currents. Neuroanatomical stains have revealed cell bodies at the base of the setal shafts, dendritic connections through to the distal ends of the shafts, and axonal tracts around the antennal socket connecting with an additional cell body and continuing toward the brain. These anatomical observations combined with previous scanning electron microscopy studies suggest that the setae are similar to mechanoreceptors and propreceptors used by higher crustaceans to sense water currents and gravity, and maintained balance.

Meyers, D. G.↗

NASA NTRS1985

Role of Hydrogen and Structure on CMSX-2

The goal was to characterize and understand the detailed effect of hydrogen on the tensile and fatigue behavior of single crystals of CMSX-2. Specimens were solutionized, air cooled, and then aged in one of two ways. The resultant macro and microstructure included a pronounced dendritic structure with numerous low angle boundaries in the interdendritic region and on the average a high level of porosity with a large variation in size and distribution. Hydrogen permeability and diffusivity in this material was found to be very low at room temperature. Hydrogen concentration studies on thin samples yielded values significantly higher than found for similar charging conditions in nickel and stainless steels. The tensile mechanical properties were found to depend on hydrogen concentration. SEM observations of the brittle subsurface zone revealed a strong correlation between crack initiation sites and voids just beneath the surface. The hollow and solid samples were compared to better understand the influence of increased charged volume on the fatigue behavior.

Baker, C. L.↗

NASA NTRS1984

Simultaneous junction formation

High-risk, high-payoff improvements to a baseline process sequence of simultaneous junction formation of silicon solar cells are discussed. The feasibility of simultaneously forming front and back junctions of solar cells using liquid dopants on dendritic web silicon was studied. Simultaneous diffusion was compared to sequential diffusion. A belt furnace for the diffusion process was tested.

Campbell, R. B.↗

NASA NTRS1984

Temperature-stress modeling

Temperature-stress modeling for silicon dendritic web growth is described. Temperature/stress fields near growth front are examined. The effects of lateral temperature gradients are also explored.

Seidensticker, R. G.↗

NASA NTRS1984

Advanced module development overview

Crystalline silicon solar power modules are examined for reliability and cost effectiveness. A goal of 12% solar energy conversion efficiency is considered feasible at a cost of 12/kWh, and a decision is made to limit consideration to float zone silicon wafer and dendritic web silicone modules. A preliminary module packaging configuration of glass/ethylene vinyl acetate/plastic film is selected. Anticipated module efficiency levels are 12.6% at 25 C and 11.5% at NOCT (Nominal Operating Cell Temperature).

Smokler, M. I.↗

NASA NTRS1984

Convection-induced distortion of a solid-liquid interface

Measurements of convective flow fields and solid-liquid interface shapes during the solidification of a pure and a slightly alloyed transparent material reveal that the convective transport of solute can cause a macroscopic depression to develop in the solid-liquid interface. This effect occurs under conditions close to those which are predicted to produce morphological instability of a planar interface. A cellular or dendritic microstructure later develops within the interface depression. The convection is attributed to the effect of radial temperature gradients in the crystal growth apparatus.

Schaefer, R. J.↗

NASA NTRS1984

The mechanisms of formation and prevention of channel segregation during alloy solidification

Using a base chilled configuration, conditions for the formation and prevention of segregation channels are studied in the ammonium chloride-water and lead-tin systems. Such channels develop when the rejected solute is less dense than the solvent and are therefore a result of density inversion, but slow (less than 5 rpm) rates of mold rotation, about axes inclined to the vertical by 20 to 30 deg, throughout the time of solidification, effectively prevent the formation or propagation of these channels. In experiments with artificially created or blocked channels, a simultaneous solute plume in the bulk liquid must be present in order for a channel to develop. The results indicate that channels originate not within the dendritic array, but immediately ahead of the growth front as a result of perturbation from the less dense boundary layer into the bulk liquid. The effect of mold movement is to translate laterally the bulk liquid relative to the growth front so that perturbations are sheared off. The nature of the liquid movement is considered and shown to be a function of the mold dimensions.

Hellawell, A.↗

NASA NTRS1985

Superalloy microstructural variations induced by gravity level during directional solidification

The Ni-base superalloy MAR-M246 (Hf) was directionally solidified during low gravity maneuvers aboard a NASA KC-135 aircraft. Gravity force variations during this process yielded a concomitant variation in microstructure and microsegregation. Secondary dendrite arm spacings are noted to be larger in the low-g portion; this, in turn, decreases the extent of interdendritic segregation. The amount of Hf in both the carbides and interdendritic eutectic increases as the gravity force diminishes. Fewer carbides are present in the low-g regions.

Johnston, M. H.↗

NASA NTRS1984

Recombination-active defects in silicon ribbon and polycrystalline solar cells

This paper reports results from a study of recombination-active structural defects in silicon ribbon and polycrystalline solar cells using the electron beam induced current (EBIC) technique in a scanning electron microscope. It is demonstrated that low temperature EBIC measurements can reveal a range of defects that are not observable at room temperature, including slip dislocations in silicon dendritic web ribbons as well as decorated twin boundaries and dislocation complexes in cast polycrystalline silicon solar cell materials.

Cheng, L. J.↗

NASA NTRS1986

Pulling-Speed Control for Silicon-Web Growth

Proposed control system for dendritic-web growth of silicon ribbons varies ribbon speed according to melt temperature. System prevents too fast or too slow withdrawal of silicon web, which cause pullout of web or excessive web thickness, respectively. System also enables semiautomatic startup of web growth by automatically increasing web speed from zero to optimum value.

Richter, R.↗

NASA NTRS1985

Fluid Flow in Crystal Growth: Analysis of the Verticle Bridgman and Floating Zone Process

Research is aimed at the fundamental understanding of the interactions of heat and mass transport and fluid mechanics in crystal growth from the melt, especially in how it pertains to experiments supported by the Microgravity Science and Applications program. Emphasis has been on studies of the vertical Bridgman system, on small-scale floating zone systems proposed for space flight, and on quantitative prediction of nonlinear transitions in melt/solid interface morphologies leading to the formation of dendrites in directional solidification. The analysis of vertical Bridgman growth has lead to the complete numerical analysis of transport phenomena in directional solidification and to a detailed comparison of calculations to the GaGe growth experiments of Wang and Witt. Calculations show the central role of the ampoule material in determining the radial temperature gradients in the melt and thus, the intensity of convection. Results indicate that diffusion-controlled growth can not be achieved on Earth with conventional growth systems, but are feasible in microgravity

Brown, R. A.↗

NASA NTRS1985

Influence of Melt Convection on Solid-Liquid Interface Under Terrestrial and Reduced Gravity Environments

Solidification and crystal growth processes involve thermal and solutal gradients within a molten phase. In the presence of gravity, such gradients result in convective flows which interact with diffusion fields at the solid-liquid interface. Dendritic growth kinetics was studied in transparent model systems which freeze similarily to most metals. Succinonitrile shows a strong influence of convection at supercoolings below about 1K. Fluid flows adjacent to solid-liquid interfaces and the behavior of shear flows in vertical annular geometries are studied. Novel low-frequency eigenstates were discovered and classified as coupled modes, for their involvement with interfacial deformation coupled to the fluid flow, and are unknown in systems without deformable interfaces. The dependence of coupled convection modes on interfacial geometry, gravity, fluid properties, and transformation characteristics studied for several annual flow arrangements with nominally pure solid-liquid systems.

Glicksman, M. E.↗

NASA NTRS1985

Theoretical Problems in Materials Science

Interactions between theoretical physics and material sciences to identify problems of common interest in which some of the powerful theoretical approaches developed for other branches of physics may be applied to problems in materials science are presented. A unique structure was identified in rapidly quenched Al-14% Mn. The material has long-range directed bonds with icosahedral symmetry which does not form a regular structure but instead forms an amorphous-like quasiperiodic structure. Finite volume fractions of second phase material is advanced and is coupled with nucleation theory to describe the formation and structure of precipitating phases in alloys. Application of the theory of pattern formation to the problem of dendrite formation is studied.

Langer, J. S.↗

NASA NTRS1985

Structure-property characterization of rheocast and VADER processed IN-100 superalloy

Two recent solidification processes have been applied in the production of IN-100 nickel-base superalloy: rheocasting and vacuum arc double electrode remelting (VADER). A detailed microstructural examination has been made of the products of these two processes; associated tensile strength and fatigue crack propagation (FCP) rate at an elevated temperature were evaluated. In rheocasting, processing variables that have been evaluated include stirring speed, isothermal stirring time and volume fraction solid during isothermal stirring. VADER processed IN-100 was purchased from Special Metals Corp., New Hartford, NY. As-cast ingots were subjected to hot isostatic pressing (HIP) and heat treatment. Both rheocasting and VADER processed materials yield fine and equiaxed spherical structures, with reduced macrosegregation in comparison to ingot materials. The rheocast structures are discussed on the basis of the Vogel-Doherty-Cantor model of dendrite arm fragmentation. The rheocast ingots evaluated were superior in yield strength to both VADER and commercially cast IN-100 alloy. Rheocast and VADER ingots may have higher crack propagation resistance than P/M processed material.

Cheng, J. J. A.↗

NASA NTRS1985

The status of silicon ribbon growth technology for high-efficiency silicon solar cells

More than a dozen methods have been applied to the growth of silicon ribbons, beginning as early as 1963. The ribbon geometry has been particularly intriguing for photovoltaic applications, because it might provide large area, damage free, nearly continuous substrates without the material loss or cost of ingot wafering. In general, the efficiency of silicon ribbon solar cells has been lower than that of ingot cells. The status of some ribbon growth techniques that have achieved laboratory efficiencies greater than 13.5% are reviewed, i.e., edge-defined, film-fed growth (EFG), edge-supported pulling (ESP), ribbon against a drop (RAD), and dendritic web growth (web).

Ciszek, T. F.↗

NASA NTRS1986

Undercooled and rapidly quenched Ni-Mo alloys

Hypoeutectic, eutectic, and hypereutectic nickel-molybdenum alloys were rapidly solidified by both bulk undercooling and melt spinning techniques. Alloys were undercooled in both electromagnetic levitation and differential thermal analysis equipment. The rate of recalescence depended upon the degree of initial undercooling and the nature (faceted or nonfaceted) of the primary nucleating phase. Alloy melts were observed to undercool more in the presence of primary Beta (NiMo intermetallic) phase than in gamma (fcc solid solution) phase. Melt spinning resulted in an extension of molybdenum solid solubility in gamma nickel, from 28 to 37.5 at % Mo. Although the microstructures observed by undercooling and melt spinning were similar the microsegregation pattern across the gamma dendries was different. The range of microstructures evolved was analyzed in terms of the nature of the primary phase to nucleate, its subsequent dendritic growth, coarsening and fragmentation, and final solidification of interfenderitic liquid.

Tewari, S. N.↗

NASA NTRS1985

An advanced material science payload for GAS

The aim of the experiments is to study solidification phenomena in metal alloys. Especially the dendritic growth and the effect of the absence of natural convection are of particular interest for the scientist, professor Hasse Fredriksson at the Royal Institute of Technology (RIT) in Stockholm. The results from the flight processed samples will be compared with results from a lot of earth-processed samples in order to investigate the influence of the natural convection on the solidification process.

R. Jonsson↗