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At least 451 records · Page 25

LDEF-space environmental effects on materials: Composites and silicone coatings

The effects of long term low Earth orbit environments on thermal control coatings and organic matrix/fiber reinforced composites are discussed. Two diverse categories are reported here: silicone coatings and composites. For composites physical and structural properties were analyzed; results are reported on mass/dimensional loss, microcracking, short beam shear, coefficient of thermal expansion (CTE), and flexural properties. The changes in thermal control properties, mass, and surface chemistry and morphology are reported and analyzed for the silicone coatings.

Petrie, Brian C.↗

Environmental fatigue in aluminum-lithium alloys

Aluminum-lithium alloys exhibit similar environmental fatigue crack growth characteristics compared to conventional 2000 series alloys and are more resistant to environmental fatigue compared to 7000 series alloys. The superior fatigue crack growth behavior of Al-Li alloys 2090, 2091, 8090, and 8091 is due to crack closure caused by tortuous crack path morphology and crack surface corrosion products. At high R and reduced closure, chemical environment effects are pronounced resulting in accelerated near threshold da/dN. The beneficial effects of crack closure are minimized for small cracks resulting in rapid growth rates. Limited data suggest that the 'chemically small crack' effect, observed in other alloy system, is not pronounced in Al-Li alloys. Modeling of environmental fatigue in Al-Li-Cu alloys related accelerated fatigue crack growth in moist air and salt water to hydrogen embrittlement.

Piascik, Robert S.↗

Microstructural analysis of the 2195 aluminum-lithium alloy welds

The principal objective of this research was to explain a tendency of 2195 Al-Li alloy to crack at elevated temperature during welding. Therefore, a study was made on the effect of welding and thermal treatment on the microstructure of Al-Li Alloy 2195. The critical roles of precipitates, boundaries, phases, and other features of the microstructure were inferred from the crack propagation paths and the morphology of fracture surface of the alloy with different microstructures. Particular emphasis was placed on the microstructures generated by the welding process and the mechanisms of crack propagation in such structures. Variation of the welding parameters and thermal treatments were used to alter the micro/macro structures, and they were characterized by optical and scanning electron microscopy. A theoretical model is proposed to explain changes in the microstructure of welded material. This model proposes a chemical reaction in which gases from the air (i.e., nitrogen) release hydrogen inside the alloy. Such a reaction could generate large internal stresses capable to induce porosity and crack-like delamination in the material.

Talia, George E.↗

The Pluto fast flyby mission: Completing the reconnaissance of the solar system

The concept of a fast flyby mission to Pluto has been advanced as a means to complete the reconnaissance of the known solar system. In order to acquire data on the Pluto system at the earliest possible time, and within the professional lifetime of investigators now active in the field, concepts are being developed for relatively small spacecraft in the mass range of 70 Kg to 350 Kg with flight times to Pluto of 7 to 13 years. Necessarily, the science complement on such a mission will be very mass and power limited. The challenge will be to define a spacecraft and an instrument package that will maximize the scientific return within these limitations. Cost, of course, will be a major consideration, and funds for new technology development specific to this mission will not be extensive. Consequently, innovative ways to incorporate elegant simplicity into the designs must be found. In order to facilitate exploration of the Pluto-Charon system, fully integrated science payloads must be developed. Two proposed mission designs involving limited mass and power science payloads have been presented to the Outer Planets Science Working Group (OPSWG). These payload mass allocations range from 5 to 30 kilograms with power allocations as low as 5 watts. The drivers behind these low mass and power allocations are that they enable developing missions to fit within the moderate mission cost profile and allow fast flight times to Pluto (7 to 13 years). The OPSWG has prioritized science goals for this class of reconnaissance mission. Three specific science objectives were identified as the highest priority required for the first Pluto mission. These goals were: (1) study of the neutral atmosphere, (2) geology and morphology, and (3) surface compositional mapping. In order to achieve these science goals within the constraints of low mass, power and cost, it may be necessary to combine the functions of 3 conventional instruments (CCD camera, Ultra-Violet Spectrometer, and Infrared Spectrometer) into one fully integrated payload. Where possible, this payload would share optics, mechanisms, electronics and packaging.

Henry, Paul K.↗

Integration of AIRSAR and AVIRIS data for Trail Canyon alluvial fan, Death Valley, California

Combining quantitative geophysical information extracted from the optical and microwave wavelengths provides complementary information about both the surface mineralogy and morphology. This study combines inversion results from two remote sensing instruments, a polarimetric synthetic aperture radar, AIRSAR, and an imaging spectrometer, AVIRIS, for Trail Canyon alluvial fan in Death Valley, California. The NASA/JPL Airborne Synthetic Aperture Radar (AIRSAR) is a quad-polarization, three frequency instrument. AIRSAR collects data at C-band = 5.66 cm, L-band = 23.98 cm, and P-band = 68.13 cm. The data are processed to four-looks and have a spatial resolution of 10 m and a swath width of 12 km. The AIRSAR data used in this study were collected as part of the Geologic Remote Sensing Field Experiment (GRSFE) over Death Valley on 9/14/89. The Airborne Visible/Infrared Imaging Spectrometer (AVIRIS) is a NASA/JPL instrument that flies in an ER-2 aircraft at an altitude of 20 km. AVIRIS uses four spectrometers to collect data in 224 spectral channels from 0.4 micrometer to 2.45 micrometer. The width of each spectral band is approximately 10 nm. AVIRIS collects data with a swath width of 11 km and a pixel size of 20 m. The AVIRIS data used in this study were collected over Death Valley on 5/31/92.

Kierein-Young, Kathryn S.↗

Experiment 2: Vapor Transport Crystal Growth of Mercury Cadmium Telluride in Microgravity- USML-2

The new epitaxial growth experiments of Hg(l-x)Cd(x)Te on (100) CdTe substrates by chemical vapor transport (CVT), using HgI2 as a transport agent, were performed in the transient growth regime of this ternary, heteroepitaxial system at normal and reduced gravity during the USML-2 flight. The surface and interface morphology, the compositional and structural uniformity, and carrier mobility of the epitaxial layer and islands grown in microgravity are measurably improved relative to ground specimens. These observations demonstrate the effects of convective flow on the transport, deposition, and growth processes of this solid-vapor system even in the transient growth regime. The properties of the Hg(l-x)Cd(x)Te layer grown in a microgravity environment compare quite favorably to those of layers obtained by other techniques.

Wiedemeier, H.↗

Interferometric Study of the Ice Stream in Interior Northeast Greenland

Initial work in Greenland with ERS-1 synthetic aperture radar (SAR) imagery led to the discovery of a large ice stream which carries much of the ice discharge from the northeast quadrant of the ice sheet. The ice stream was identified based on the morphology of the surface, which indicated the influence of localized rapid ice flow. Continued investigations using repeat-pass interferometry from ERS-1 and ERS-2 allowed the character of the rapid motion to be determined, mapping the onset region in the deep interior of the ice sheet as well as more rapid motion downstream. Markers were placed on the ice sheet and are being tracked with the global positioning system (GPS) survey to provide tie-points for the interferometry, which will allow the absolute velocities to be determined in this very remote area.

Fahnestock, Mark↗

Burner Rig Hot Corrosion of a Single Crystal Ni-48Al-Ti-Hf-Ga Alloy

The hot corrosion resistance of a single crystal Ni-48Al-1Ti-0.5Hf-0.2Ga alloy was examined in a Mach 0.3 burner rig at 900 C for 300 hours. The combustion chamber was doped with 2 ppmw synthetic sea salt. The hot corrosion attack produced a random mound morphology on the surface. Microstructurally, the hot corrosion attack appeared to initiate with oxide-filled pits which were often broad and shallow. At an intermediate stage, the pits increased in size to incorporate unoxidized Ni islands in the corrosion product. The rampant attack stage, which was observed only at sharp sample corners, was characterized by rapid inward growth of alumina in finger-like protrusions incorporating significant amounts of Al-depleted Ni islands. Aluminum consumption in the oxide fingers resulted in the growth of a gamma' layer ahead of the advancing oxide fingers.

Nesbitt, James A.↗

Growth and maintenance of an embryogenic cell culture of daylily (Hemerocallis) on hormone-free medium

Callus cultures of the diploid daylily (Hemerocallis) clone Autumn Blaze' were initiated and maintained in hormone-containing nutrient medium. At various times (from 6 weeks to 1 year) after being initiated, hormone-derived cultures were evaluated for their ability to be maintained and to multiply on hormone-free medium at low pH (between pH 4 and 4.5). Cultures had to be exposed to hormone-containing medium for at least 12 weeks before they could be maintained on hormone-free medium at low pH. The transition to maintainability on low pH hormone-free medium included the production of many aberrant embryonal forms ( neomorphs'). However, all hormone-derived cultures tested consisted entirely of preglobular stage proembryos (PGSPs) after 12-24 weeks on low pH hormone-free medium. PGSP cultures have been maintained and multiplied as such for over 1 year on low pH hormone-free medium. PGSPs continue their development into various somatic embryo stages when cultured on hormone-free medium buffered at pH 5.8. The production of well-formed somatic embryos was greatly enhanced when PGSPs were plated on activated charcoal impregnated filter papers that were placed on top of the agar surface. The gross morphology and histology of the PGSPs and stages of somatic embryo development are presented. The work shows that the ability of hormone-free medium at low pH to permit PGSP multiplication without development into later stages of embryo development is not restricted to carrot.

Non-NASA Center↗

(abstract) Sciencecraft

The technological capabilities are now at hand to design an integrated system that combines science instruments, spacecraft, and propulsion elements into a single system. The authors have called this a sciencecraft since it is intended to provide automatic scientific observations of planetary and astrophysical objects. Integration of function allows lower mass and cost and supports a short development cycle. A specific science mission is described in this paper, a flyby of Neptune, Triton, and an object in the Kuiper belt. The SCIENCECRAFT system is described. It has electric propulsion and is capable of measuring the surface constituents and morphology of objects visited and characterizing their atmospheres both in emission and adsorption (against the Sun). Miniature fields and particles experiments are incorporated that will provide interplanetary information together with details of the magnetic and electric attributes of each object. The Sciencecraft is Delta launched and has a flight time to the Kuiper belt of 7 years. The design is such that the craft functions in a largely autonomous mode to provide low cost mission operations.

planetary astrophysics science instruments spacecr↗

Use of Atomic Oxygen for Increased Water Contact Angles of Various Polymers for Biomedical Applications

The purpose of this study was to determine the effect of atomic oxygen (AO) exposure on the hydrophilicity of nine different polymers for biomedical applications. Atomic oxygen treatment can alter the chemistry and morphology of polymer surfaces, which may increase the adhesion and spreading of cells on Petri dishes and enhance implant growth. Therefore, nine different polymers were exposed to atomic oxygen and water-contact angle, or hydrophilicity, was measured after exposure. To determine whether hydrophilicity remains static after initial atomic oxygen exposure, or changes with higher fluence exposures, the contact angles between the polymer and water droplet placed on the polymer s surface were measured versus AO fluence. The polymers were exposed to atomic oxygen in a 100-W, 13.56-MHz radio frequency (RF) plasma asher, and the treatment was found to significantly alter the hydrophilicity of non-fluorinated polymers. Pristine samples were compared with samples that had been exposed to AO at various fluence levels. Minimum and maximum fluences for the ashing trials were set based on the effective AO erosion of a Kapton witness coupon in the asher. The time intervals for ashing were determined by finding the logarithmic values of the minimum and maximum fluences. The difference of these two values was divided by the desired number of intervals (ideally 10). The initial desired fluence was then multiplied by this result (2.37), as was each subsequent desired fluence. The flux in the asher was determined to be approximately 3.0 x 10(exp 15) atoms/sq cm/sec, and each polymer was exposed to a maximum fluence of 5.16 x 10(exp 20) atoms/sq cm.

deGroh, Kim↗

Hydrocarbon Rocket Technology Impact Forecasting

Ever since the Apollo program ended, the development of launch propulsion systems in the US has fallen drastically, with only two new booster engine developments, the SSME and the RS-68, occurring in the past few decades.1 In recent years, however, there has been an increased interest in pursuing more effective launch propulsion technologies in the U.S., exemplified by the NASA Office of the Chief Technologist s inclusion of Launch Propulsion Systems as the first technological area in the Space Technology Roadmaps2. One area of particular interest to both government agencies and commercial entities has been the development of hydrocarbon engines; NASA and the Air Force Research Lab3 have expressed interest in the use of hydrocarbon fuels for their respective SLS Booster and Reusable Booster System concepts, and two major commercially-developed launch vehicles SpaceX s Falcon 9 and Orbital Sciences Antares feature engines that use RP-1 kerosene fuel. Compared to engines powered by liquid hydrogen, hydrocarbon-fueled engines have a greater propellant density (usually resulting in a lighter overall engine), produce greater propulsive force, possess easier fuel handling and loading, and for reusable vehicle concepts can provide a shorter turnaround time between launches. These benefits suggest that a hydrocarbon-fueled launch vehicle would allow for a cheap and frequent means of access to space.1 However, the time and money required for the development of a new engine still presents a major challenge. Long and costly design, development, testing and evaluation (DDT&E) programs underscore the importance of identifying critical technologies and prioritizing investment efforts. Trade studies must be performed on engine concepts examining the affordability, operability, and reliability of each concept, and quantifying the impacts of proposed technologies. These studies can be performed through use of the Technology Impact Forecasting (TIF) method. The Technology Impact Forecasting method is a normative forecasting technique that allows the designer to quantify the effects of adding new technologies on a given design. This method can be used to assess and identify the necessary technological improvements needed to close the gap that exists between the current design and one that satisfies all constraints imposed on the design. The TIF methodology allows for more design knowledge to be brought to the earlier phases of the design process, making use of tools such as Quality Function Deployments, Morphological Matrices, Response Surface Methodology, and Monte Carlo Simulations.2 This increased knowledge allows for more informed decisions to be made earlier in the design process, resulting in shortened design cycle time. This paper will investigate applying the TIF method, which has been widely used in aircraft applications, to the conceptual design of a hydrocarbon rocket engine. In order to reinstate a manned presence in space, the U.S. must develop an affordable and sustainable launch capability. Hydrocarbon-fueled rockets have drawn interest from numerous major government and commercial entities because they offer a low-cost heavy-lift option that would allow for frequent launches1. However, the development of effective new hydrocarbon rockets would likely require new technologies in order to overcome certain design constraints. The use of advanced design methods, such as the TIF method, enables the designer to identify key areas in need of improvement, allowing one to dial in a proposed technology and assess its impact on the system. Through analyses such as this one, a conceptual design for a hydrocarbon-fueled vehicle that meets all imposed requirements can be achieved.

Stuber, Eric↗

The Porous Microstructure Analysis (PuMA) software

The open-source Porous Microstructure Analysis (PuMA) software was implemented to offer an efficient framework for determining material characteristics from 3D microstructures. Its development was inspired by progress in X-ray microtomography, an imaging technology that captures the internal structure of materials in 3D, and even in a 4D temporal context. Over recent years, this method has transformed the domain of materials science due to its capability to non-destructively examine material microstructures while presenting digital data about their geometrical details. It has provided insights into materials relevant to several NASA missions, including heatshields, parachute fabrics, meteorites, and other advanced composites. PuMA, in its current version 3, delivers an array of features, spanning from basic geometric insights of a microstructure to intricate anisotropic thermo-elastic and chemical behavior. Specifically, the software evaluates morphological attributes (specific surface area, volume fractions, mean intercept lengths, orientation) and physical characteristics (conductivity, elasticity, permeability, and tortuosity). Additionally, it can model material degradation processes, such as oxidation and surface chemistry interactions. The software can generate synthetic microstructures, from straightforward geometrical designs to intricate woven and non-woven geometries. Coupling material generation and characterization enable parametric studies and sensitivity analysis to optimize the microstructural performance and inform design decisions and reliability assessment based on uncertainty quantification. A recent addition to PuMA includes the TomoSAM plugin, devised to incorporate the cutting-edge Segment Anything Model (SAM). SAM is a promptable deep learning model that can identify objects and create image masks in a zero-shot manner, based only on a few user clicks. The synergy between these tools aids in the segmentation of complex 3D datasets from tomography or other imaging techniques, which would otherwise require a laborious manual segmentation process.

Tomography↗

Tensile Behavior and High-Cycle Fatigue Durability of a SiC/SiC Ceramic-Matrix Composite Without and With Simulated Cooling Holes

High-cycle fatigue (HCF) behavior of a melt-infiltrated, prepreg SiC/SiC composite was investigated using specimens without and with simulated cooling holes at 816 and 1,316 °C. The ceramic-matrix composite (CMC) material used for this study was fabricated by GE Aviation and had a ply configuration of [0/90/0] 3 . HCF tests were conducted with an R-ratio of 0.6 and a cyclic frequency of 30 Hz. Maximum tensile gross-section stresses used in the HCF tests ranged from 152 to 359 MPa. Runout in HCF was defined as 30 million cycles (278 h) at both temperatures. Monotonic tensile tests were conducted at room temperature (RT) on as-received CMC specimens and on HCF runout specimens without and with holes to determine residual tensile strengths. Digital image correlation (DIC) and acoustic emission (AE) techniques were used to monitor progression of damage in RT tensile tests on specimens without and with holes. Fractography was performed on a limited number of specimens without and with holes to determine morphology of fracture surfaces. Representative RT stress-strain behavior, elevated temperature HCF behavior at the two temperatures, and RT residual tensile strengths of HCF runout specimens are documented in this report. Select examples of DIC and AE data from RT tensile tests on specimens without and with holes and typical features observed on fracture surfaces of specimens tested under tensile and HCF conditions are also discussed.

Ceramic matrix composite↗

The Porous Microstructure Analysis (PuMA) software

The open-source Porous Microstructure Analysis (PuMA) software was created to offer an efficient framework for determining material properties from 3D microstructures. Its development was inspired by progress in X-ray microtomography, an imaging technology that captures the internal structure of materials in 3D, and even in a 4D temporal context. Over recent years, this method has transformed the domain of materials science due to its capability to non-destructively examine material microstructures while presenting digital data about their geometrical details. It has provided insights into materials relevant to several NASA missions, including heatshields, parachute fabrics, meteorites, and other advanced composites. PuMA, in its current version 3, delivers an array of features, spanning from basic geometric insights of a microstructure to intricate anisotropic thermo-elastic and chemical behavior. Specifically, the software evaluates morphological attributes (specific surface area, volume fractions, mean intercept lengths, orientation) and physical characteristics (conductivity, elasticity, permeability, and tortuosity). Additionally, it can model material degradation processes, such as oxidation and surface chemistry interactions. The software can generate synthetic microstructures, from straightforward geometrical designs to intricate woven and non-woven geometries. Coupling material generation and characterization enables parametric studies and sensitivity analysis to optimize the microstructural performance and inform design decisions and reliability assessment based on uncertainty quantification. A recent addition to PuMA includes the TomoSAM plugin, devised to incorporate the cutting-edge Segment Anything Model (SAM) into our image segmentation workflow. SAM is a promptable deep learning model that can identify objects and create image masks in a zero-shot manner, based only on a few user clicks. The synergy between these tools aids in the segmentation of complex 3D datasets from tomography and other imaging techniques, which would otherwise require a laborious manual segmentation process.

Tomography↗

Geological-morphological description of the Lakshmi planum (photomap of the Venusian surface sheet B-4)

The Lakshmi Planum and its surrounding area (together comprising a single structure) are described in morphological terms on the basis of Venera 15 and 16 photomap data. Plume ascent from the planetary interior and subsequent horizontal spreading represent the underlying mechanisms behind structural formation: folding and/or imbricating accompany these processes. In effect, the Laksmi structure can be regarded as a local spreading center. Its structural dimensions attest to the role that asthenospheric currents played in its formation.

Pronin, A. A.↗

Mars Field Geology, Biology, and Paleontology Workshop: Summary and Recommendations

Current NASA planning envisions human missions to Mars as early as 2013, on a mission that would send six crew members for a 500-day stay on the surface of Mars. While our understanding of how we would get there and back is fairly mature, the planning for what the crew would do to explore while on the surface for 500 days is less detailed. Mission objectives are to understand the composition and geo- morphology of the martian surface, and to continue to investigate and sample the geologic history of Mars. Special emphasis will focus on exploring for possible biogenic signatures, past or present, and on analyzing pre-biotic chemistry. The purpose of this workshop was to explore the strategies, desired capabilities, skills, and operational realities required to lend success to the first human missions to Mars. Current mission planning dictates that there will be considerable mobility, sampling and analytical capability available to human crews, at a site warranting long-term geologic and possibly biological interest. However, the details of specific capabilities are not yet clearly defined.

Budden, Nancy Ann↗

Mars Field Geology, Biology. and Paleontology Workshop: Summary and Recommendations

Current NASA planning envisions human missions to Mars as early as 2013, on a mission that would send six crew members for a 500-day stay on the surface of Mars. While our understanding of how we would get there and back is fairly mature, the planning for what the crew would do to explore while on the surface for 500 days is less detailed. Mission objectives are to understand the composition and geo- morphology of the martian surface, and to continue to investigate and sample the geologic history of Mars. Special emphasis will focus on exploring for possible biogenic signatures, past or present, and on analyzing pre-biotic chemistry. The purpose of this workshop was to explore the strategies, desired capabilities, skills, and operational realities required to lend success to the first human missions to Mars. Current mission planning dictates that there will be considerable mobility, sampling and analytical capability available to human crews, at a site warranting long-term geologic and possibly biological interest. However, the details of specific capabilities are not yet clearly defined.

Budden, Nancy Ann↗