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At least 451 records · Page 25

Developing time-resolved x-ray diffraction diagnostics at the National Ignition Facility (invited)

As part of a program to measure phase transition timescales in materials under dynamic compression, we have designed new x-ray imaging diagnostics to record multiple x-ray diffraction measurements during a single laser-driven experiment. Our design places several ns-gated hybrid CMOS (hCMOS) sensors within a few cm of a laser-driven target. The sensors must be protected from an extremely harsh environment, including debris, electromagnetic pulses, and unconverted laser light. Another key challenge is reducing the x-ray background relative to the faint diffraction signal. Building on the success of our predecessor (Target Diffraction In Situ), we implemented a staged approach to platform development. First, we built a demonstration diagnostic (Gated Diffraction Development Diagnostic) with two hCMOS sensors to confirm we could adequately protect them from the harsh environment and also acquire acceptable diffraction data. This allowed the team to quickly assess the risks and address the most significant challenges. Here, we also collected scientifically useful data during development. Leveraging what we learned, we recently developed a much more ambitious instrument (Flexible Imaging Diffraction Diagnostic for Laser Experiments) that can field up to eight hCMOS sensors in a flexible geometry and participate in back-to-back shots at the National Ignition Facility (NIF). The design also allows for future iterations, such as faster hCMOS sensors and an embedded x-ray streak camera. The enhanced capabilities of the new instrument required a much more complex design, and the unexpected issues encountered on the first few shots at NIF remind us that complexity has consequences. Our progress in addressing these challenges is described herein, as is our current focus on improving data quality by reducing x-ray background and quantifying the uncertainties of our diffraction measurements.

36 MATERIALS SCIENCE↗

Fiber coupled laser ultrasound system using a single mode hollow core fiber for excitation laser: Theory and demonstration for on-machine thickness gauging

Laser ultrasound (LU) is a technique that uses a pump laser and a probe laser to optically generate and detect elastic waves in a material. Despite its advantages over traditional contact transducer-based ultrasound, industrial adoption has been limited by complex optical setups and the inability of multi-mode fibers to deliver a stable Gaussian profile for the pump laser. Here, we report a fully fiber-coupled thermoelastic LU system that uses an anti-resonant hollow-core single-mode fiber to deliver 1 mJ nanosecond pulses of 1064 nm light, while preserving the fundamental Gaussian mode (pump laser). When combined with a fiber-coupled interferometer (probe laser), a small, flexible, and environmentally robust sensor capable of optically generating and detecting high frequency broadband ultrasound is realized. We demonstrate such an LU system implemented in situ on a four-axis precision lathe. High-resolution thickness gauging is performed, before and after precision cutting, by exciting and measuring a zero-group velocity guided wave mode. The measurements are verified with ex-situ traceable coordinate measuring machine data. Mean absolute deviations of 0.1%, of nominal thickness, before cutting, and 0.2% and 0.3%, after stepped and tapered cuts, respectively, are reported. A theoretical background for thermoelastic ultrasound generation in an elastic waveguide is also presented. Attention is given to the effect of the pump laser profile on wave generation to elucidate the importance of using single-mode laser light. The fiber-coupled system demonstrated is well-suited for use in scientific and engineering sensing applications and facilitates the adoption of LU for industrial non-destructive testing.

Engineering↗

Micromotion-synchronized pulsed Doppler cooling of trapped ions

Here we propose and demonstrate a new method for Doppler cooling trapped-ion crystals where the distribution of micromotion amplitudes may be large and uneven. The technique uses pulses of Doppler cooling light synchronized with the trap RF that selectively target ions when their velocity is near a node, leading to more uniform cooling across a crystal by a single tone of cooling light. We lay out a theoretical framework that describes where this technique is practical, and provide a simple experimental demonstration.

79 ASTRONOMY AND ASTROPHYSICS↗

A measurement of the fast luminescent decay time of P-15 phosphor

During the development of a delayed coincidence apparatus for the study of atomic decays, the need arose for a bright, fast, and inexpensive light source with known decay characteristics. A sample of P-15 phosphor was obtained for use as a calibration light source. A short pulse duration was employed to preferentially excite the short lifetime components relative to the longer-lived ones. The computer analysis revealed that the raw MCA decay curve data could be described well by a sum of three exponentials with decay times of about 88 nsec, about 6.5 nsec, and 1.04 + or - 2%.

Sutton, J. F.↗

Disproportionation of Fe2SiO4 to 2FeO plus SiO2 at pressures up to 250kbar and temperatures up to 3000 C

A sample of Fe2SiO4 (spinel) at approximately 250 kbar in a diamond anvil press was heated to approximately 3000 C for a duration of some ms using a focused light beam from a pulsed ruby laser. After quenching and unloading, X-ray diffraction patterns indicated that the portion of the sample that had been heated contained wustite and stishovite. A sample of Fe2SiO4 (fayalite) at approximately 200 kbar in a diamond anvil press has been heated to 800 C for 20 min in a furnace. After quenching and unloading, the sample was found to have concentric zones with the fayalite phase at the lowest pressure, the spinel phase at the intermediate pressure, and a dark region at the center where the pressure was highest. An X-ray diffraction pattern of the dark central region indicated the presence of wustite. A microprobe analysis of a sample produced by a similar procedure indicated that SiO2 is apparently evolved along with wustite but is not sufficiently crystalline to be detected by X-ray diffraction.

Bassett, W. A.↗

An experiment in manipulator control with proximity sensors

Optical proximity sensors were used in a feedback loop to automatically position a manipulator hand for grasping. The experiment was a simplified one, involving two dimensional motion only. Two proximity sensors were mounted on the hand, and control signals derived from their outputs were used to drive the hand vertically and horizontally. The sensors employ a pulsed gallium arsenide light-emitting diode together with a silicon detector. They indicate, without contact, the approximate distance between the manipulator hand and object in the range from 5 to 12 cm. Positioning within approximately + or - 5 mm was observed. Extension of the technique to general three-dimensional control is briefly discussed.

Johnston, A. R.↗

Plans for a fast image recording system at ESO

A 256 diode-array will be installed as detector on the ESO OPTRONICS S-3000 measuring machine in order to increase the acquisition rate. A high intensity LED will be used as light source in a pulse mode. The data will be stored on a random access mass storage device as density values for later education. The scanning time for a 30 cm x 30 cm plate with a step size of 10 micron will be less than 10 hours while the dynamic range of the data is expected to be 2.5 density units with an offset of at least 1 unit.

Grosboel, P. J.↗

Generating Independent Preionizing Pulses for Lasers

Simple pulse-coupling winding on saturable reactor core lets core act as pulse transformer, passing preionizing pulse from winding to tapered transmission line, then to laser. Laser prepared for independent firing pulse, which follows preionizing pulse. Winding is simple, light in weight, low in bulk and power consumption, and inexpensive.

Pacala, T. J.↗

Flat-plate solar array project process development area: Process research of non-CZ silicon material

Several different techniques to simultaneously diffuse the front and back junctions in dendritic web silicon were investigated. A successful simultaneous diffusion reduces the cost of the solar cell by reducing the number of processing steps, the amount of capital equipment, and the labor cost. The three techniques studied were: (1) simultaneous diffusion at standard temperatures and times using a tube type diffusion furnace or a belt furnace; (2) diffusion using excimer laser drive-in; and (3) simultaneous diffusion at high temperature and short times using a pulse of high intensity light as the heat source. The use of an excimer laser and high temperature short time diffusion experiment were both more successful than the diffusion at standard temperature and times. The three techniques are described in detail and a cost analysis of the more successful techniques is provided.

Campbell, R. B.↗

Fluorescence yields from photodissociative excitation of HCOOH, HCOOCH3, and CH3COOH in the vacuum-ultraviolet region

The photoexcitation processes of HCOOH, HCOOCH3, and CH3COOH were studied in the vacuum-ultraviolet region by using synchroton radiation and a pulsed discharge lamp as light sources. The absorption and fluorescence cross sections of these molecules were measured in the 106-250-nm region. Fluorescences were detected from photoexcitation of HCOOH and HCOOCH3, but not from CH3COOH. Fluorescence produced at 123.9 nm was dispersed and identified as the excited OH and HCOO radicals. Fluorescence quantum yields of HCOOH and HCOOCH3 increase with decreasing excitation wavelengths with maxima of 5 and 0.3 percent at 106 nm, respectively.

Suto, Masako↗

Two-Dimensional Acousto-Optical Spectrum Analyzer

State-of-the-art two-dimensional acousto-optical spectrum analyzer processes input radio-frequency signal in real time into components in any number of spectral channels up to about 10(Sup5). Input radio-frequency signal to be analyzed launched via transducer into acousto-optical device along x axis. Acousto-optical device becomes Bragg cell. Pulsed plane waves of light from laser aimed at Bragg cell, which spatially modulates phases of plane waves and diffracts waves according to pattern of acoustic signal.

Ansari, Homayoon↗

Photographic System Makes Path Of Vortex Visible

System making rapid flows visible developed to record track followed by ring vortex when encountering object near its path. Schlieren optical setup includes standard Z-configuration mirror arrangement and pulsed, synchronized source of light. System proves valuable in determining position, velocity, and acceleration of vortex as it passes over and interacts with object in its path.

Jones, Stephen B.↗

SALI chemical analysis of provided samples

SRI has completed the chemical analysis of all the samples supplied by NASA. The final batch of four samples consisted of: one inch diameter MgF2 mirror, control 1200-ID-FL3; one inch diameter neat resin, PMR-15, AO171-IV-55, half exposed and half unexposed; one inch diameter chromic acid anodized, EOIM-3 120-47 aluminum disc; and AO-exposed and unexposed samples of fullerene extract material in powdered form, pressed into In foil for analysis. Chemical analyses of the surfaces were performed by the surface analysis by laser ionization (SALI) method. The analyses emphasize surface contamination or general organic composition. SALI uses nonselective photoionization of sputtered or desorbed atoms and molecules above but close (approximately one mm) to the surface, followed by time-of-flight (TOF) mass spectrometry. In these studies, we used laser-induced desorption by 5-ns pulse-width 355-nm light (10-100 mJ/sq cm) and single-photon ionization (SPI) by coherent 118-nm radiation (at approximately 5 x 10(exp 5) W/sq cm). SPI was chosen primarily for its ability to obtain molecular information, whereas multiphoton ionization (not used in the present studies) is intended primarily for elemental and small molecule information. In addition to these four samples, the Au mirror (EOIM-3 200-11, sample four) was depth profiled again. Argon ion sputtering was used together with photoionization with intense 355-nm radiation (35-ps pulsewidths). Depth profiles are similar to those reported earlier, showing reproducibility. No chromium was found in the sample above noise level; its presence could at most be at the trace level. Somewhat more Ni appears to be present in the Au layer in the unexposed side, indicating thermal diffusion without chemical enhancement. The result of the presence of oxygen is apparently to tie-up/draw out the Ni as an oxide at the surface. The exposed region has a brownish tint appearance to the naked eye.

Becker, Christopher H.↗

Instrumentation for Studies of Electron Emission and Charging From Insulators

Making measurements of electron emission properties of insulators is difficult since insulators can charge either negatively or positively under charge particle bombardment. In addition, high incident energies or high fluences can result in modification of a material s conductivity, bulk and surface charge profile, structural makeup through bond breaking and defect creation, and emission properties. We discuss here some of the charging difficulties associated with making insulator-yield measurements and review the methods used in previous studies of electron emission from insulators. We present work undertaken by our group to make consistent and accurate measurements of the electron/ion yield properties for numerous thin-film and thick insulator materials using innovative instrumentation and techniques. We also summarize some of the necessary instrumentation developed for this purpose including fast response, low-noise, high-sensitivity ammeters; signal isolation and interface to standard computer data acquisition apparatus using opto-isolation, sample-and-hold, and boxcar integration techniques; computer control, automation and timing using Labview software; a multiple sample carousel; a pulsed, compact, low-energy, charge neutralization electron flood gun; and pulsed visible and UV light neutralization sources. This work is supported through funding from the NASA Space Environments and Effects Program and the NASA Graduate Research Fellowship Program.

Thomson, C. D.↗

100-kHz Interferometric Rayleigh Scattering Flow Diagnostics at 266 nm

Interferometric Rayleigh scattering (IRS) is a laser-based technique capable of spatially and temporally resolved measurement of gas velocity and temperature in unseeded gaseous flows. In the present embodiment of the technique, IRS is performed at 266 nm for the first time. IRS at 266 nm is potentially much less susceptible to interferences from particles and other stray light sources. A pulse-burst laser and high-speed camera provided image rates of 100 kHz, allowing simultaneous space- and time-resolved measurement in high speed flow at multiple points along a line. The use of 266 nm excitation and detection is compared with prior work that used 532 nm. New experimental interferogram modelling and fitting techniques for single and multi-velocity-component IRS were demonstrated in a study of the spatial and temporal variation of the flow along a line through a supersonic jet. Single component velocity and temperature measurements using 266 nm were successfully made and compared with prior 532 nm results. Two-component velocity measurements at 266 nm, using the reflected image method, were compared to single-component measurements.

Andrew D Cutler↗

Pulse transducer with artifact signal attenuator

An artifact signal attenuator for a pulse rate sensor is described. The circuit for attenuating background noise signals is connected with a pulse rate transducer which has a light source and a detector for light reflected from blood vessels of a living body. The heart signal provided consists of a modulated dc signal voltage indicative of pulse rate. The artifact signal resulting from light reflected from the skin of the body comprises both a constant dc signal voltage and a modulated dc signal voltage. The amplitude of the artifact signal is greater and the frequency less than that of the heart signal. The signal attenuator circuit includes an operational amplifier for canceling the artifact signal from the output signal of the transducer and has the capability of meeting packaging requirements for wrist-watch-size packages.

Cash, W. H., Jr.↗