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NASA NTRS2016

Development of X-Ray Microcalorimeter Imaging Spectrometers for the X-Ray Surveyor Mission Concept

Four astrophysics missions are currently being studied by NASA as candidate large missions to be chosen inthe 2020 astrophysics decadal survey.1 One of these missions is the X-Ray Surveyor (XRS), and possibleconfigurations of this mission are currently under study by a science and technology definition team (STDT). Oneof the key instruments under study is an X-ray microcalorimeter, and the requirements for such an instrument arecurrently under discussion. In this paper we review some different detector options that exist for this instrument,and discuss what array formats might be possible. We have developed one design option that utilizes eithertransition-edge sensor (TES) or magnetically coupled calorimeters (MCC) in pixel array-sizes approaching 100kilo-pixels. To reduce the number of sensors read out to a plausible scale, we have assumed detector geometriesin which a thermal sensor such a TES or MCC can read out a sub-array of 20-25 individual 1 pixels. In thispaper we describe the development status of these detectors, and also discuss the different options that exist forreading out the very large number of pixels.

multiplexing↗
NASA NTRS2016

Performance Assessment of Different Pulse Reconstruction Algorithms for the ATHENA X-Ray Integral Field Unit

The X-ray Integral Field Unit (X-IFU) microcalorimeter, on-board Athena, with its focal plane comprising 3840 Transition Edge Sensors (TESs) operating at 90 mK, will provide unprecedented spectral-imaging capability in the 0.2-12 keV energy range. It will rely on the on-board digital processing of current pulses induced by the heat deposited in the TES absorber, as to recover the energy of each individual events. Assessing the capabilities of the pulse reconstruction is required to understand the overall scientific performance of the X-IFU, notably in terms of energy resolution degradation with both increasing energies and count rates. Using synthetic data streams generated by the X-IFU End-to-End simulator, we present here a comprehensive benchmark of various pulse reconstruction techniques, ranging from standard optimal filtering to more advanced algorithms based on noise covariance matrices. Beside deriving the spectral resolution achieved by the different algorithms, a first assessment of the computing power and ground calibration needs is presented. Overall, all methods show similar performances, with the reconstruction based on noise covariance matrices showing the best improvement with respect to the standard optimal filtering technique. Due to prohibitive calibration needs, this method might however not be applicable to the X-IFU and the best compromise currently appears to be the so-called resistance space analysis which also features very promising high count rate capabilities.

microcalorimeters↗
NASA NTRS2014

The X-ray Integral Field Unit (X-IFU) for Athena

Athena is designed to implement the Hot and Energetic Universe science theme selected by the European Space Agency for the second large mission of its Cosmic Vision program. The Athena science payload consists of a large aperture high angular resolution X-ray optics (2 m2 at 1 keV) and twelve meters away, two interchangeable focal plane instruments: the X-ray Integral Field Unit (X-IFU) and the Wide Field Imager. The X-IFU is a cryogenic X-ray spectrometer, based on a large array of Transition Edge Sensors (TES), oering 2.5 eV spectral resolution, with approximately 5" pixels, over a field of view of 5' in diameter. In this paper, we present the X-IFU detector and readout electronics principles, some elements of the current design for the focal plane assembly and the cooling chain. We describe the current performance estimates, in terms of spectral resolution, effective area, particle background rejection and count rate capability. Finally, we emphasize on the technology developments necessary to meet the demanding requirements of the X-IFU, both for the sensor, readout electronics and cooling chain.

X-ray↗
NASA NTRS2017

PIPER Continuous Adiabatic Demagnetization Refrigerator

We report upon the development and testing of a 4-stage adiabatic demagnetization refrigerator (ADR) capable of continuous cooling at 0.100 Kelvin. This cooler is being built to cool the detector array aboard NASA's Primordial Inflation Polarization Explorer (PIPER) observatory. The goal of this balloon mission is to measure the primordial gravitational waves that should exist if the theory of cosmological inflation is correct. At altitude, the ADR will hold the array of transition-edge sensors at 100 mK continuously while periodically rejecting heat to a 1.2 K pumped helium bath. During testing on ground, the array is held at the same temperature but heat is rejected to a 4.2 K helium bath indicating the flexibility in this coolers design.

Magnetic Cooling Sub-Kelvin ADR↗
NASA NTRS2017

Performance of an X-Ray Microcalorimeter with a 240 Micron Absorber and a 50 Micron TES Bilayer

We have been developing superconducting transition-edge sensor (TES) microcalorimeters for a variety of potential astrophysics missions, including Athena. The X-ray Integral Field Unit (X-IFU) instrument on this mission requires close-packed pixels on a 0.25 mm pitch, and high quantum efficiency between 0.2 and 12 keV. The traditional approach within our group has been to use square TES bilayers on molybdenum and gold that are between 100 and 140 microns in size, deposited on silicon nitride membranes to provide a weak thermal conductance to a 50 mK heat bath temperature. It has been shown that normal metal stripes on top of the bilayer are needed to keep the unexplained noise at a level consistent with the expected based upon estimates for the non-equilibrium non-linear Johnson noise.In this work we describe a new approach in which we use a square TES bilayer that is 50 microns in size. While the weak link effect is much stronger in this size of TES, we have found that excellent spectral performance can be achieved without the need for any normal metal strips on top of the TES. A spectral performance of 1.58 eV at 6 KeV has been achieved, the best resolution seen in any of our devices with this pixel size. The absence of normal metal stripes has led to more uniform transition shapes, and more reliable excellent spectral performance. The smaller TES size has meant that that the thermal conductance to the heat bath, determined by the perimeter length of the TES and the membrane thickness, is lower than on previous devices, and thus has a lower count rate capability. This is an advantage for low count-rate applications where the slower speed enables easier multiplexing in the read-out, thus potential higher multiplexing factors. In order to recover the higher count rate capabilities, a potential path exits using thicker silicon nitride membranes to increase the thermal conductance to the heat bath.

Miniussi, Antoine R.↗
NASA NTRS2017

Design of Magnetic Shielding and Field Coils for a TES X-Ray Microcalorimeter Test Platform

The performance of Transition-Edge Sensors (TES) and their SQUID multiplexed read-outs are very sensitive to the ambient magnetic field from Earth and fluctuations that can arise due to fluctuating magnetic fields outside of the focal plane assembly from the Adiabatic Demagnetization Refrigerator (ADR).Thus, the experimental platform we are building to test the FPA of the X-ray Integral Field Unit (X-IFU) of the Athena mission needs to include a series of shields and a coil in order to meet the following requirement of magnetic field density and uniformity.

Miniussi, Antoine R.↗
NASA NTRS2017

High Count-Rate Study of Two TES X-Ray Microcalorimeters With Different Transition Temperatures

We have developed transition-edge sensor (TES) microcalorimeter arrays with high count-rate capability and high energy resolution to carry out x-ray imaging spectroscopy observations of various astronomical sources and the Sun. We have studied the dependence of the energy resolution and throughput (fraction of processed pulses) on the count rate for such microcalorimeters with two different transition temperatures T(sub c). Devices with both transition temperatures were fabricated within a single microcalorimeter array directly on top of a solid substrate where the thermal conductance of the microcalorimeter is dependent upon the thermal boundary resistance between the TES sensor and the dielectric substrate beneath. Because the thermal boundary resistance is highly temperature dependent, the two types of device with different T(sub c)(sup s) had very different thermal decay times, approximately one order of magnitude different. In our earlier report, we achieved energy resolutions of 1.6 and 2.eV at 6 keV from lower and higher T(sub c) devices, respectively, using a standard analysis method based on optimal filtering in the low flux limit. We have now measured the same devices at elevated x-ray fluxes ranging from 50 Hz to 1000 Hz per pixel. In the high flux limit, however, the standard optimal filtering scheme nearly breaks down because of x-ray pile-up. To achieve the highest possible energy resolution for a fixed throughput, we have developed an analysis scheme based on the socalled event grade method. Using the new analysis scheme, we achieved 5.0 eV FWHM with 96 Percent throughput for 6 keV x-rays of 1025 Hz per pixel with the higher T(sub c) (faster) device, and 5.8 eV FWHM with 97 Percent throughput with the lower T(sub c) (slower) device at 722 Hz.

Lee, Sang-Jun↗
NASA NTRS2018

Microcalorimeter Array Development for the ATHENA X-Ray Integral Field Unit

The X-ray integral field unit (X-IFU) for ESA's Athena X-ray observatory will consist of 3840 AC-biased transition edge sensors (TESs), read out using frequency domain multiplexing (FDM). In this paper we describe details of the latest pixels geometries that are being designed for the current baseline array configuration. This includes details on how important TES properties (transition parameters, thermal design of the pixels, absorber composition) are being optimized to meet the target energy resolution, count-rate and quantum efficiency. We also present the latest design optimizations specifically targeted at mitigating AC-bias phenomena in Mo/Au TESs that can degrade performance.

Smith, Stephen↗
NASA NTRS2018

Performance of an X-ray Microcalorimeter with a 240 μm Absorber and a 50 μm TES Bilayer

Superconducting transition-edge sensor (TES) microcalorimeters are being developed for a variety of potential astrophysics missions, including Athena. The X-ray integral field unit instrument on this mission requires close-packed pixels on a 0.25 mm pitch, and high quantum efficiency between 0.2 and 12 keV. In this work, we describe a new approach with 50 μm square TESs consisting of a Mo/Au bilayer, deposited on silicon nitride membranes to provide a weak thermal conductance to a ~50 mK heat bath. Larger TESs usually have additional normal metal stripes on top of the bilayer to reduce the noise. However, we have found that excellent spectral performance can be achieved without the need for any normal metal stripes on top of the TES. A spectral performance of 1.58+/-0.12 eV at 5.9 keV has been achieved, the best resolution seen in any of our devices with this pixel size.

Miniussi, Antoine R.↗
NASA NTRS2017

A Path to High Efficiency Optical Coupling for HIRMES

The high-resolution mid-infrared spectrometer (HIRMES) under development for SOFIA (Stratospheric Observatory for Infrared Astronomy) is an instrument operating in the 25-122 μm spectral range with a spectral resolution R= Δ ʎ /ʎ ~100,000 and has two absorber-coupled transition edge sensor (TES) bolometric detector focal planes. We have developed novel NbTiN low stress absorber coatings which have the required optical impedance across the HIRMES operating band. The low intrinsic stress of these coatings allow for a peak-to-valley corrugation amplitude < 5 μm of the 450 nm thick, 1.4 mm x 1.7 mm detector pixels. Furthermore, these coatings have a superconducting transition temperature ~ 10 K, which allows them to simultaneously serve as an absorber in the desired signal band and a rejection filter at long wavelengths. This attribute makes them especially attractive for ultrasensitive absorber-coupled bolometric detector applications, because it helps in controlling the optical loading from out-of band radiation. We also discuss a novel method for integrating a wedged reflective absorber-termination to the detector array.

bolometers↗
NASA NTRS2017

Characterization of Si-Membrane TES Bolometer Arrays for the HIRMES Instrument

The High Resolution Mid-Infrared Spectrometer (HIRMES) instrument will fly onboard NASA's airborne Stratospheric Observatory for Infrared Astronomy (SOFIA) in 2019. HIRMES will provide astronomers with a unique observing window (25 122 µm) for exploring the evolution of protoplanetary disks into young solar systems, and the composition of our Solar System. There are two focal plane detector arrays for the instrument: a high-resolution (/ = 100,000) 8x16 detector array with a target noise-equivalent power, NEP 3x10-18 W/Hz; and a low-resolution (/ = 2,000 19,000) 16x64 detector array with a target NEP 2x10-17 W/Hz. The detectors for both of these arrays are superconducting Mo/Au bilayer transition edge sensor (TES) bolometers on thin suspended single-crystal silicon membranes. Here we present our characterization results for the detectors in both arrays, including measurements of thermal conductance with comparison to phonon transport models, saturation power, noise, and array uniformity.

Instrumentation and Photography↗
NASA NTRS2018

The Primordial Inflation Polarization Explorer (PIPER): Current Status and Performance of the First Flight

The Primordial Inflation Polarization ExploreR (PIPER) is a balloon-borne instrument optimized to measure the polarization of the CMB at large angular scales. It will map 85% of the sky over a series of conventional balloon flights from the Northern and Southern hemispheres, measuring the B-mode polarization power spectrumover a range of multipoles from 2-300 covering both the reionization bump and the recombination peak, with sensitivity to measure the tensor-to-scalar ratio down to r = 0.007. PIPER will observe in four frequency bands centered at 200, 270, 350, and 600 GHz to characterize dust foregrounds. The instrument has background-limited sensitivity provided by fully cryogenic (1.7 K) optics focusing the sky signal onto kilo-pixel arrays of time-domain multiplexed Transition-Edge Sensor (TES) bolometers held at 100 mK. Polarization sensitivity and systematiccontrol are provided by front-end Variable-delay Polarization Modulators (VPMs). PIPER had its engineering flight in October 2017 from Fort Sumner, New Mexico. This papers outlines the major components in the PIPER system discussing the conceptual design as well as specific choices made for PIPER. We also report on the results of the engineering flight, looking at the functionality of the payload systems, particularly VPM, as well as pointing out areas of improvement.

Pawlyk, Samuel↗
NASA NTRS2019

Extended Line Spread Function of TES Microcalorimeters with Au/Bi Absorbers

Microcalorimeters have the potential to provide line shapes well-described by a single Gaussian broadening term of few-eV width. This attribute makes the detectors especially well suited for x-ray astrophysics observations; however, low-level non-Gaussian broadening terms are expected and must be characterized. These terms depend on the composition of the x-ray absorber, the detailed x-ray absorption physics, the device thermalization processes, and the incident x-ray energy. Here we present the first measurements targeted at understanding the extended line-spread function (LSF) of x-ray microcalorimeter pixels under development for the X-ray Integral Field Unit (XIFU) on the Athena X-ray Observatory. These pixels are comprised of Mo/Au transition-edge sensors (TESs) with overhanging electroplated Au/Bi absorbers. We measured the line shapes using monochromatic x-ray sources with < 1 eV width at several x-ray energies (0.85, 0.93, 1.25, 1.5, 5.4, and 8.0 keV) across the instrument bandpass (0.3-12 keV) and modeled the line profiles. These results are compared to the extended LSF of the Hitomi microcalorimeter pixels that used HgTe absorbers.

Superconducting devices↗
NASA NTRS2019

Design of Magnetic Shielding and Field Coils for a TES X-Ray Microcalorimeter Test Platform

The performance of transition-edge sensors (TES) and their SQUID multiplexed readouts is very sensitive to ambient magnetic field and its fluctuations. In order to run ground experiments on thousands of X-ray TES microcalorimeters with a small uniform ambient magnetic field (< 1 μT, with a uniformity < 0.1 μT), we need a very low ambient field to be trapped into the superconducting magnetic shields. We have designed a sub-Kelvin test platform to reach these specifications. For this purpose, we modeled a new design for the shielding consisting of a series of different mu-metal and superconducting shields, including a niobium shield at 50 mK, a cryoperm (A4K) shield at 3 K, and a mu-metal shield at 300 K. A magnetic field coil is used to vary the local perpendicular magnetic field over the TES array. To optimize this field, we have studied a number of different field-coil designs and the impact of the different shield geometries, in order to reach the required field uniformity.

Miniussi, Antoine R.↗
NASA NTRS2019

Method for Deriving Telescope Specifications for Earth-Detecting Coronagraphs and Its Use in Prioritizing Technology Development Investments

Different potential exoplanet mission concepts require different enabling and enhancing technologies. Decisions regarding prioritizing the development of these technologies can be made using a Science-Driven Systems-Engineering framework. The white paper makes the following specific recommendations. (1) Any potential telescope/coronagraph combination should develop a wavefront stability error budget using the method described in this white paper. That error budget will inform discussions about what technology development will be needed to enable the mission. (2) Enhancing and enabling technologies requiring investment include: low noise reaction wheels or control moment gyros; micro-thruster technology; active vibration isolation; materials and design practice for making lightweight stiff structures and optical components; 200-hertz wavefront sensing and control; 500-hertz sub-picometer-precision edge sensor and position actuators; non-destructive process to quantify CTE (Coefficient of Thermal Expansion) homogeneity of 4-meter class mirrors to an uncertainty of plus or minus 1 parts per billion per degree Kelvin over a 100 by 100 sampling; laser gauge positional metrology system; and predictive active thermal control.

Space Mirror Technology↗
NASA NTRS2019

Sub-Kelvin Cooling for Two Kilopixel Bolometer Arrays in the PIPER Receiver

The Primordial Inflation Polarization Explorer (PIPER) is a balloon-borne telescope mission to search for inflationary gravitational waves from the early universe. PIPER employs two 32 × 40 arrays of superconducting transition-edge sensors, which operate at 100 mK. An open bucket Dewar of liquid helium maintains the receiver and telescope optics at 1.7 K. We describe the thermal design of the receiver and sub-Kelvin cooling with a continuous adiabatic demagnetization refrigerator (CADR). The CADR operates between 70 and 130 mK and provides ≈10 μW cooling power at 100 mK, nearly five times the loading of the two detector assemblies. We describe electronics and software to robustly control the CADR, overall CADR performance in flightlike integrated receiver testing, and practical considerations for implementation in the balloon float environment.

Switzer, E. R.↗
NASA NTRS2020

First Operation of TES Microcalorimeters in Space with the Micro-X Sounding Rocket

Micro-X is a sounding rocket-borne instrument that uses a microcalorimeter array to perform high-resolution X-ray spectroscopy. This instrument flew for the first time on July 22nd, 2018, from the White Sands Missile Range, USA. This flight marks the first successful operation of a transition-edge sensor array and its time-division multiplexing readout system in space. This launch was dedicated to the observation of the supernova remnant Cassiopeia A. A failure in the attitude control system prevented the rocket from pointing and led to no time on target. The onboard calibration source provided X-rays in flight, and it is used to compare detector performance during preflight integration, flight, and after the successful post-flight recovery. This calibration data demonstrate the capabilities of the detector in a space environment as well as its potential for future flight.

TES↗
NASA NTRS2020

Extension of the energy range accessible with a TES using bath temperature variations

The energy range of transition-edge sensor (TES) X-ray microcalorimeters with a multiplexed readout depends upon the width and shape of the TES superconducting transition, and also on the dynamic range of the readout. In many detector systems, the multiplexed readout slew rate capability will be the limiting factor for the energy range. In these cases, if we are willing to accept some energy resolution degradation, we can significantly extend the energy range by increasing the bath temperature of operation, essentially creating a second “extended energy range” mode of operation. For example, if we require the very highest energy resolution up to 7 keV, and wish to optimize the design up to this energy, for some measurements it could be very beneficial to have a mode where we can extend the energy range to 15–20 keV even if some energy resolution is sacrificed. In this paper, we explore the trade-off between dynamic range and energy resolution from changing the bath temperature of the TES. We present measurements of TES resolution and slew rate as a function of bath temperature and compare to numerical simulations.

S Beaumont↗