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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 451 records · Page 25
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Time-Resolved Radioluminescence of the Copper(I) Cluster Cu4I62-. Temporal responses to Photo, X-ray, Beta-ray, and alpha-ray Excitation.

Described are time-resolved radioluminescence (TRRL) properties of the Cu(I) cluster Cu4I62– upon pulsed X-ray, β-ray or α-particle excitation. The longer (>2 μs) TRRL component displayed exponential decay comparable to pulsed UV excitation; however, temporal behavior at shorter times indicates that high local excited state density provides an alternative decay channel.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2023

Systems and methods for regioselective carbonylation of 2,2-disubstituted epoxides for the production of alpha,alpha-disubstituted beta-lactones

Provided are methods of producing carbonyl compounds (e.g., carbonyl containing compounds) and catalysts for producing carbonyl compounds. Also provided are methods of making polymers from carbonyl compounds and polymers formed from carbonyl compounds. A method may produce carbonyl compounds, such as, for example α,α-disubstituted carbonyl compounds (e.g., α,α-disubstituted β-lactones). The polymers may be produced from α,α-disubstituted β-lactones, which may be produced by a method described herein.

Coates, Geoffrey W.↗
DOE OSTI2024

Alpha(v)beta(6) integrin-binding peptides and methods of use thereof

The present invention provides peptide conjugates that target an integrin such as α v β 6 integrin. In particular embodiments, the peptide conjugates comprise a moiety such as a PEG moiety, an imaging agent, or a therapeutic agent. The peptide conjugates of the present invention are particularly useful for imaging a tumor, organ, or tissue. Compositions and kits containing the peptide conjugates of the present invention are also provided herein.

Tang, Yng↗
DOE OSTI2026

Modulating Mid-Gap Electronic States Through Site-Selective Modification in B-Pbx/B'-CuyV2O5/CdS Heterostructures for Photocatalytic Hydrogen Evolution

We interfaced ..beta..-Pbx/..beta..'-CuyV2O5 compounds, with varying stoichiometries of precisely positioned Pb-ions (x) and Cu-ions (y) in interstitial sites along a tunnel-structured ?-V2O5 framework, with cysteine-capped CdS (cysCdS) quantum dots (QDs) to yield heterostructured photocatalysts. ..beta..-Pbx/..beta..'-CuyV2O5 compounds exhibit midgap electronic states with orbital contributions from both Cu 3d and stereochemically active Pb 6s states that show distinctive light-initiated reactivity with photoexcited QDs. ..beta..-Pbx/..beta..'-CuyV2O5/CdS heterostructures were prepared by linker-assisted assembly (LAA). Scanning and transmission electron microscopy, energy-dispersive X-ray spectroscopy, and Raman spectroscopy revealed that cysCdS QDs were deposited onto surfaces of ..beta..-Pbx/..beta..'-CuyV2O5 via LAA. HAXPES revealed that the site-selective positioning of Pb-ions and Cu-ions promoted close energetic alignment of the midgap states of ..beta..-Pbx/..beta..'-CuyV2O5 compounds with the valence-band maximum of cysCdS QDs. Transient absorption spectroscopy revealed that photogenerated holes were transferred from CdS QDs to midgap states of ..beta..-Pbx/..beta..'-CuyV2O5 compounds on time scales <50 ps. Finally, photoelectrochemical and photochemical experiments revealed that ..beta..-Pbx/..beta..'-CuyV2O5/CdS heterostructures promoted the photocatalytic reduction of H+ to H2. In photoelectrochemical experiments, under oxidative conditions, for all ..beta..-Pbx/..beta..'-CuyV2O5/CdS heterostructures, H2 was evolved at a Pt counter electrode while a sacrificial donor was oxidized at the heterostructure-functionalized working electrode. In contrast, under reductive conditions, for ..beta..-Pb0.152V2O5/CdS and ..beta..-Pbx/..beta..'-CuyV2O5/CdS heterostructures, H2 was evolved at the working electrode. In photochemical experiments, dispersed ..beta..-Pbx/..beta..'-CuyV2O5/CdS heterostructures promoted the reduction of H+ to H2 under white-light illumination; ..beta..'-Cu0.55V2O5/CdS and ..beta..-Pbx/..beta..'-CuyV2O5/CdS heterostructures, for which midgap states have Cu 3d orbital character, generated 2-fold more H2 than ..beta..-Pb0.152V2O5/CdS heterostructures. Cu-ion insertion thus appends additional acceptor surface states that improve ligand-mediated hole transfer from photoexcited QDs, but such states are intrinsically limited in mediating hole transport to the substrate as a result of the low mobility of holes in narrow Cu 3d-states. Our results reveal that the density and orbital character of midgap states of ..beta..-Pbx/..beta..'-CuyV2O5 compounds, tunable through recently developed site-selective ion insertion strategies, determine efficiencies of charge-transfer and charge-transport mechanisms that underpin photocatalysis.

36 MATERIALS SCIENCE↗
DOE OSTI2020

New results from the CUORE experiment

The Cryogenic Underground Observatory for Rare Events (CUORE) is the first cryogenic experiment searching for neutrinoless double-beta ($0\nu\beta\beta$) decay that has been able to reach the one-ton scale. The detector, located at the Laboratori Nazionali del Gran Sasso in Italy, consists of an array of 988 TeO$_2$ crystals arranged in a compact cylindrical structure of 19 towers. Following the completion of the detector construction in August 2016, CUORE began its first physics data run in 2017 at a base temperature of about 10 mK. Following multiple optimization campaigns in 2018, CUORE is currently in stable operating mode. In 2019, CUORE released its 2\textsuperscript{nd} result of the search for $0\nu\beta\beta$ with a TeO$_2$ exposure of 372.5 kg$\cdot$yr and a median exclusion sensitivity to a $^{130}$Te $0\nu\beta\beta$ decay half-life of $1.7\cdot 10^{25}$ yr. We find no evidence for $0\nu\beta\beta$ decay and set a 90\% C.I. (credibility interval) Bayesian lower limit of $3.2\cdot 10^{25}$ yr on the $^{130}$Te $0\nu\beta\beta$ decay half-life. In this work, we present the current status of CUORE's search for $0\nu\beta\beta$, as well as review the detector performance. Finally, we give an update of the CUORE background model and the measurement of the $^{130}$Te two neutrino double-beta ($2\nu\beta\beta$) decay half-life.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2023

Integrated RMP-based ELM-crash-control process for plasma performance enhancement during ELM crash suppression in KSTAR

The integrated Resonant Magnetic Perturbation (RMP)-based Edge-Localized Mode (ELM)-crash-control process aims to enhance the plasma performance during the RMP-driven ELM crash suppression, where the RMP induces an unwanted confinement degradation. In this study, the normalized beta ($\beta_\textrm{N}$) is introduced as a metric for plasma performance. The integrated process incorporates the latest achievements in the RMP technique to enhance $\beta_\textrm{N}$ efficiently. The integrated process triggers the n = 1 Edge-localized RMP (ERMP) at the L–H transition timing using the real-time Machine Learning (ML) classifier. The pre-emptive RMP onset can reduce the required external heating power for achieving the same $\beta_\textrm{N}$ by over 10% compared to the conventional onset. During the RMP phase, the adaptive feedback RMP ELM controller, demonstrating its performance in previous experiments, plays a crucial role in maximizing $\beta_\textrm{N}$ during the suppression phase and sustaining the $\beta_\textrm{N}$-enhanced suppression state by optimizing the RMP strength. The integrated process achieves $\beta_\textrm{N}$ up to ~2.65 during the suppression phase, which is ~10% higher than the previous KSTAR record but ~6% lower than the target of the K-DEMO first phase ($\beta_\textrm{N}$ = 2.8), and maintains the suppression phase above the lower limit of target $\beta_\textrm{N}$ (= 2.4) for ~4 s (~60$\tau_\textrm{E}$). In addition to $\beta_\textrm{N}$ enhancement, the integrated process demonstrates quicker restoration of the suppression phase and recovery of $\beta_\textrm{N}$ compared to the adaptive control with the n = 1 Conventional RMP (CRMP). The post-analysis of the experiment shows the localized effect of the ERMP spectrum in radial and the close relationship between the evolution of $\beta_\textrm{N}$ and the electron temperature.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2021

On the shear-current effect: toward understanding why theories and simulations have mutually and separately conflicted

ABSTRACT The shear-current effect (SCE) of mean-field dynamo theory refers to the combination of a shear flow and a turbulent coefficient β21 with a favourable negative sign for exponential mean-field growth, rather than positive for diffusion. There have been long-standing disagreements among theoretical calculations and comparisons of theory with numerical experiments as to the sign of kinetic ($\beta ^u_{21}$) and magnetic ($\beta ^b_{21}$) contributions. To resolve these discrepancies, we combine an analytical approach with simulations, and show that unlike $\beta ^b_{21}$, the kinetic SCE $\beta ^u_{21}$ has a strong dependence on the kinetic energy spectral index and can transit from positive to negative values at $\mathcal {O}(10)$ Reynolds numbers if the spectrum is not too steep. Conversely, $\beta ^b_{21}$ is always negative regardless of the spectral index and Reynolds numbers. For very steep energy spectra, the positive $\beta ^u_{21}$ can dominate even at energy equipartition urms ≃ brms, resulting in a positive total β21 even though $\beta ^b_{21}\lt 0$. Our findings bridge the gap between the seemingly contradictory results from the second-order-correlation approximation versus the spectral-τ closure, for which opposite signs for $\beta ^u_{21}$ have been reported, with the same sign for $\beta ^b_{21}\lt 0$. The results also offer an explanation for the simulations that find $\beta ^u_{21}\gt 0$ and an inconclusive overall sign of β21 for $\mathcal {O}(10)$ Reynolds numbers. The transient behaviour of $\beta ^u_{21}$ is demonstrated using the kinematic test-field method. We compute dynamo growth rates for cases with or without rotation, and discuss opportunities for further work.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2022

Latest Results from the CUORE Experiment

Abstract The Cryogenic Underground Observatory for Rare Events (CUORE) is the first cryogenic experiment searching for $$0\nu \beta \beta $$ 0 ν β β decay that has been able to reach the one-tonne mass scale. The detector, located at the Laboratori Nazionali del Gran Sasso (LNGS) in Italy, consists of an array of 988 $${\mathrm{TeO}}_{2}$$ TeO 2 crystals arranged in a compact cylindrical structure of 19 towers. CUORE began its first physics data run in 2017 at a base temperature of about 10 mK and in April 2021 released its $$3{\mathrm{rd}}$$ 3 rd result of the search for $$0\nu \beta \beta $$ 0 ν β β , corresponding to a tonne-year of $$\mathrm{TeO}_{2}$$ TeO 2 exposure. This is the largest amount of data ever acquired with a solid state detector and the most sensitive measurement of $$0\nu \beta \beta $$ 0 ν β β decay in $${}^{130}\mathrm{Te}$$ 130 Te ever conducted . We present the current status of CUORE search for $$0\nu \beta \beta $$ 0 ν β β with the updated statistics of one tonne-yr. We finally give an update of the CUORE background model and the measurement of the $${}^{130}\mathrm{Te}$$ 130 Te $$2\nu \beta \beta $$ 2 ν β β decay half-life and decay to excited states of $${}^{130}\mathrm{Xe}$$ 130 Xe , studies performed using an exposure of 300.7 kg yr.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2020

High–level β–carotene production from xylose by engineered Saccharomyces cerevisiae without overexpression of a truncated HMG1 (t HMG1 )

Beta-carotene is a natural pigment and health-promoting metabolite, and has been widely used in the nutraceutical, feed, and cosmetic industries. Here, we engineered a GRAS yeast Saccharomyces cerevisiae to produce beta-carotene from xylose, the sec- ond most abundant and inedible sugar component of lignocellulose biomass. Specifically, a beta-carotene biosynthetic pathway containing crtYB, crtI, and crtE from Xanthophyllomyces dendrorhous was introduced into a xylose-fermenting S. cerevisiae. Here, the resulting strain produced beta-carotene from xylose at a titer threefold higher than from glucose. Interestingly, overexpression of tHMG1, which has been reported as a critical genetic perturbation to enhance metabolic fluxes in the mevalonate pathway and beta-carotene production in yeast when glucose is used, did not further improve the production of beta-carotene from xylose. Through fermentation profiling, metabolites analysis, and transcriptional studies, we found the advantages of using xylose as a carbon source, instead of glucose, for beta-carotene production to be a more respiratory feature of xylose consumption, a larger cytosolic acetyl!CoA pool, and an upregulated expression level of rate-limiting genes in the beta-carotene!producing pathway, including ACS1 and HMG1. As a result, 772.8 mg/L of beta-carotene was ob- tained in a fed-batch bioreactor culture with xylose feeding. Considering the in- evitable large scale production of xylose when cellulosic biomass!based bioeconomy is implemented, our results suggest xylose utilization is a promising strategy for overproduction of carotenoids and other isoprenoids in engineered S. cerevisiae.

09 BIOMASS FUELS↗
DOE OSTI2025

Constraining the phase shift of relativistic species in DESI BAOs

In the early Universe, neutrinos decouple quickly from the primordial plasma and propagate without further interactions. The impact of free-streaming neutrinos is to create a temporal shift in the gravitational potential that impacts the acoustic waves known as baryon acoustic oscillations (BAOs), resulting in a non-linear spatial shift in the Fourier-space BAO signal. In this work, we make use of and extend upon an existing methodology to measure the phase shift amplitude $\beta _{\phi }$ and apply it to the Dark Energy Spectroscopic Instrument (DESI) Data Release 1 (DR1) BAOs with an anisotropic BAO fitting pipeline. We validate the fitting methodology by testing the pipeline with two publicly available fitting codes applied to highly precise cubic box simulations and realistic simulations representative of the DESI DR1 data. We find further study towards the methods used in fitting the BAO signal will be necessary to ensure accurate constraints on $\beta _{\phi }$ in future DESI data releases. Using DESI DR1, we present individual measurements of the anisotropic BAO distortion parameters and the $\beta _{\phi }$ for the different tracers, and additionally a combined fit to $\beta _{\phi }$ resulting in $\beta _{\phi } = 2.7 \pm 1.7$. After including a prior on the distortion parameters from constraints using Planck we find $\beta _{\phi } = 2.7^{+0.60}_{-0.67}$ suggesting $\beta _{\phi } > 0$ at 4.3$\sigma$ significance. This result may hint at a phase shift that is not purely sourced from the standard model expectation for $N_{\rm {eff}}$ or could be a upwards statistical fluctuation in the measured $\beta _{\phi }$; this result relaxes in models with additional freedom beyond Lambda-cold dark matter.

79 ASTRONOMY AND ASTROPHYSICS↗