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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 433 records · Page 24
All sourcesNASA NTRSDOE OSTI
DOE OSTI2020

Freestanding Photoresist Film: A Versatile Template for Three-Dimensional Micro- and Nanofabrication

Ultrathin freestanding films with well-defined micro/nanostructures and robust mechanical properties are applied in many engineering applications including microelectronics, optics, filtration and separation, biomedical engineering, and nanotechnology. Although considerable efforts have been made toward the fabrication of freestanding thin films, it is still a significant challenge to develop a simple and reliable process for producing freestanding films with ultrathin thickness, well-regulated micro/nanopatterns, robust mechanical properties, macroscopic coverage area, and multi-layered composite structures. In this work, a significant advancement is reported in this regard. This study shows a new sacrificial-layer-free (SLF) lifting-off process, integrated with conventional micro- and nanolithography, enabling the release of micro- and nanopatterned photoresist (PR) films from the supporting substrate with unprecedented pattern coverage and structure characteristics. The freestanding PR film is resilient, can withstand significant bending and deformation, and is sufficiently flexible to be transferred onto substrates with 3D topography as a conformal soft stencil for further technological processing and applications. Moreover, the SLF lifting-off process provides a simple approach to prepare single-layered and multi-layered freestanding composite films. The results suggest that the novel SLF lifting-off process can significantly extend the capability of 3D micro-/nanofabrication.

36 MATERIALS SCIENCE↗
DOE OSTI2022

CO 2 absorption intensification using three-dimensional printed dynamic polarity packing in a bench-scale integrated CO 2 capture system

Postcombustion carbon capture using a chemical absorbent is a promising technology to reduce CO 2 emission. However, the overall construction and operating costs remain a major challenge. In order to intensify the absorption process and to reduce these costs, a novel dynamic polarity structured packing (DP packing) with alternate patterns of surface polarity has been developed to enhance local macro-scale turbulence within the advanced viscous solvent to reduce the mass transfer diffusion resistance. Here, three DP structured packings that incorporate multiple polymeric materials were fabricated using three-dimensional printing technique and evaluated through parametric testing using a bench-scale integrated CO 2 capture unit with 76.2 mm ID absorber. At optimized operating conditions, the DP packing showed a relative 22.7% increase in absorption and 20.0% decrease in energy penalty.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2022

Microwave Heating-Induced Temperature Gradients in Liquid–Liquid Biphasic Systems

Microwaves (MWs) can enable the electrification and intensification of chemical manufacturing. They have been applied to various unit separations, such as drying, distillation, and extraction, entailing gas–liquid and solid–liquid systems. However, a limited quantitative understanding of MW-heated liquid–liquid biphasic systems related to extraction exists. This work measures the temporal and spatial temperature difference between an aqueous and an organic phase in batch and continuous microfluidic modes. We demonstrate permanent temperature differences between phases over 35 °C and spatiotemporal periodic and quasiperiodic oscillations modulated by the flow patterns. The temperature differences are primarily driven by the faster absorption rate of MW irradiation by the aqueous phase versus the slower heat transfer from the aqueous phase to the organic phase. These are amplified by low specific interfacial area and modifications of the electromagnetic field. We employ a multiphysics model to predict the temperature difference in a batch system. The model is in good agreement with the experiments. We demonstrate a strong effect of input power, dielectric properties of organic solvents, the volume of solvents, and the volume ratio between phases on the temperature difference. A simple analytical model describes the temperature difference and provides design principles. Furthermore, the combined approach offers new insights into the design and optimization of the MW-heated biphasic systems.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

On the role of asymmetric molecular geometry in high-performance organic solar cells

Although asymmetric molecular design has been widely demonstrated effective for organic photovoltaics (OPVs), the correlation between asymmetric molecular geometry and their optoelectronic properties is still unclear. To access this issue, we have designed and synthesized several symmetric-asymmetric non-fullerene acceptors (NFAs) pairs with identical physical and optoelectronic properties. Interestingly, we found that the asymmetric NFAs universally exhibited increased open-circuit voltage compared to their symmetric counterparts, due to the reduced non-radiative charge recombination. From our molecular-dynamic simulations, the asymmetric NFA naturally exhibits more diverse molecular interaction patterns at the donor (D):acceptor (A) interface as compared to the symmetric ones, as well as higher D:A interfacial charge-transfer state energy. Moreover, it is observed that the asymmetric structure can effectively suppress triplet state formation. These advantages enable a best efficiency of 18.80%, which is one of the champion results among binary OPVs. Therefore, this work unambiguously demonstrates the unique advantage of asymmetric molecular geometry, unveils the underlying mechanism, and highlights the manipulation of D:A interface as an important consideration for future molecular design.

14 SOLAR ENERGY↗
DOE OSTI2022

Binary pseudo-random array standards for calibration of 3D optical surface profilers used for metrology with aspheric x-ray optics

High-accuracy surface metrology is vitally important in manufacturing ultra-high-quality free-form mirrors designed to manipulate x-ray light with nanometer-scale wavelengths. The current and potential capabilities of x˗ray mirror manufacturing are limited by inherent imperfections of the integrated metrology tools. Metrology tools are currently calibrated with super-polished flat test-standard/reference mirrors. This is acceptable for fabrication of slightly curved x-ray optics. However, for even moderately curved aspherical x-ray mirrors the flat-reference calibration is not sufficiently accurate. For micro-stitching interferometry developed for surface measurements with curved x-ray mirrors, the tool aberration errors are known to be transferred into the optical surface topography of x-ray mirrors. Our approach to improving metrology is to thoroughly calibrate the measuring tool and apply the results of the calibration to deconvolution of the measured data. Here we explore the application of a recently developed technique for calibrating the instrument transfer function (ITF) of 3D optical surface profilers to metrology with significantly curved x-ray optics. The technique, based on test standards patterned with two-dimensional (2D) binary pseudo-random arrays (BPRAs), employs the unique properties of the BPRA patterns in the spatial frequency domain. The inherent 2D power spectral density of the pattern has a deterministic white-noise-like character that allows direct determination of the ITF with uniform sensitivity over the entire spatial frequency range and field of view of an instrument. The high efficacy of the technique has been previously demonstrated in application to metrology with flat and slightly curved optics. Here, we concentrate on development of an efficient fabrication process for production of highly randomized (HR) BPRA test standards on flat and 500-mm spherical optical substrates. We also compare and discuss the results of the ITF calibration of an interferometric microscope when using the HR BPRA standards on flat and curved substrates.

Munechika, Keiko↗
DOE OSTI2021

Transfer Learning using Denoising Auto-Encoders for Cellular-Level Annotation of Tumor in Pathology Slides

Adversarial examples can produce altered classifications using only seemingly innocuous, imperceptible perturbations to the original image. The imperceptibility of adversarial perturbations suggests that the corresponding classifiers use decision criteria different than those of a human. In a medical setting, inexplicable decision criteria confound a pathologist’s willingness to trust machine-generated annotations. Here, we analyze denoising tumor detection models to see if they are robust to imperceptible adversarial perturbations. Moreover, to be more fully trusted by pathologists, we require tumor detectors that generate interpretable annotations which segment pathology slides into tumorous and normal regions at the cellular level. We therefore compare transfer learning based on two different autoencoder architectures, one derived from a deep denoising bottleneck autoencoder and one from an over-complete sparse autoencoder. Both autoencoders were first trained in an unsupervised manner on a set of pathology slides drawn from the Camelyon16 dataset. The latent representations produced by each autoencoder were then passed to separate neural networks that were trained in a supervised manner on binary tumor-normal masks generated by pathologists at cellular resolution. Both tumor detectors supported better than 90% AUC PR as measured by the area under the precision/recall curve on a held-out pathology slide. To assess the underlying decision criteria used by both tumor detectors, we constructed imperceptible adversarial examples which reduced the AUC PR of both models to less than 70%. Random noise of the same amplitude had almost no effect on the AUC PR of either model. Additionally, each tumor detector was resistant to adversarial “transfer” attacks targeting the other. The adversarial perturbations showed strong characteristic differences: the deep denoising models perturbations were a very diffuse, seemingly unrecognizable pattern while the sparse coding models perturbations showed traces of tissue cells.

47 OTHER INSTRUMENTATION↗
NASA NTRS1977

Computer simulation of hypersonic flow over the Space Shuttle Orbiter

Computer simulations of the flow field around the Space Shuttle Orbiter are described. Results of inviscid calculations are presented for the shock wave pattern and bottom centerline pressure distribution at 30 deg angle of attack. Results of viscous calculations are presented for wall pressure and heat transfer distributions for simple configurations representative of regions where shock wave-boundary layer interactions occur. The computer codes are verified by comparisons with wind-tunnel data and can be applied to flight conditions.

Inouye, M.↗
NASA NTRS1980

Analytical simulation of SPS system performance, volume 3, phase 3

The simulation model for the Solar Power Satellite spaceantenna and the associated system imperfections are described. Overall power transfer efficiency, the key performance issue, is discussed as a function of the system imperfections. Other system performance measures discussed include average power pattern, mean beam gain reduction, and pointing error.

Kantak, A. V.↗
NASA NTRS1980

Convective heating of solid propellant during ignition

A pattern search optimization procedure is used to deduce from test data on the solid rocket boosters of the Space Shuttle the convective heat transfer coefficients between the igniter and main motor combustion gases and the surface of the solid propellant by utilizing a spatial and temporal ignition transient analysis. The 'best' convective coefficients are found which will minimize the overall deviation of the analytical prediction from the ignition transient test data. Computationally, this is achieved by treating the motor in such a way that only four optimization variables must be determined. The resulting coefficients greatly improve the prediction capabilities of the ignition transient analysis for the Space Shuttle SRM.

Murph, J. E.↗
NASA NTRS1980

Upgrading the free flying rendezvous and docking simulator and the orbital servicer system

Recommendations are made for upgrading two teleoperator/robotics test and simulation systems based upon a review of latest technology advances in the involved disciplines. A second generation Free Flying Mobility Unit is recommended which adds a sixth degree of freedom and incorporates other improvements which greatly expand the center's capability to perform evaluation tests and demonstrations of advanced systems concepts for rendezvous and docking in support of the Teleoperator Maneuvering System (TMS) Program. The Orbital Servicer System provides the capability for testing and demonstrating concepts for on orbit servicing of compatibly designed satellites/payloads. The TMS is to be the transporting vehicle for the servicer. The manipulator arm of the Orbital service System is presently computer controlled in the trajectory portion of the module transfer operation. The ultimate objective is to fully automte its operation requiring additional capabilities in sensors, artificial intelligence, image analysis, communications, computer programming, pattern recognition, kinematics, and manipulator design. It is recommended that the Electronics and Control Laboratory move to acquire the basic competencies in robotics necessary to achieve full automation.

Eastman, R. M.↗
NASA NTRS1980

NASA technology utilization program: The small business market

Technology transfer programs were studied to determine how they might be more useful to the small business community. The status, needs, and technology use patterns of small firms are reported. Small business problems and failures are considered. Innovation, capitalization, R and D, and market share problems are discussed. Pocket, captive, and new markets are summarized. Small manufacturers and technology acquisition are discussed, covering external and internal sources, and NASA technology. Small business and the technology utilization program are discussed, covering publications and industrial applications centers. Observations and recommendations include small business market development and contracting, and NASA management technology.

Vannoy, J. K.↗
NASA NTRS1986

A laboratory investigation of the variability of cloud reflected radiance fields

A method to determine the radiative properties of complex cloud fields was developed. A Cloud field optical simulator (CFOS) was constructed to simulate the interaction of cloud fields with visible radiation. The CFOS was verified by comparing experimental results from it with calculations performed with a Monte Carlo radiative transfer model. A software library was developed to process, reduce, and display CFOS data. The CFSOS was utilized to study the reflected radiane patterns from simulated cloud fields.

Mckee, T. B.↗
NASA NTRS1984

The spatial structure of terrain - A process signal in satellite digital images

Pattern recognition procedures applied to Landsat imagery carry an implicit assumption that the digital data are independently distributed. That assumption is incorrect over virtually any terrain. Deviations from independence occur because slopes follow a systematic pattern of variation arising from the slope-forming processes. That pattern can be identified using the stochastic process methodology of Box and Jenkins.Angles of adjacent slopes are autocorrelated and the bidirectional reflectance function transfers these systematic slope changes to the sensor. Imagery becomes autocorrelated through this transfer. Autocorrelation in the imagery can be removed through direct calculation from a digital elevation model or by use of stochastic process methodology. The latter has the advantage that the residuals are white noise; and it is applicable in any area, even where a D.E.M. is unavailable. The stochastic process signal can be used to study terrain processes.

Craig, R. G.↗
NASA NTRS1988

Crossflow vorticity sensor

A crossflow vorticity sensor for the detection of crossflow vorticity characteristics is described. The sensor is comprised of crossflow sensors which are noninvasively adhered to a swept wing laminar surface either singularly, in multi-element strips, in polar patterns, or in orthogonal patterns. These crossflow sensors are comprised of hot-film sensor elements which operate as a constant temperature anemometer circuit to detect heat transfer rate changes. Accordingly, crossflow vorticity characteristics are determined via cross-correlation. In addition, the crossflow sensors have a thickness which does not exceed a maximum value h in order to avoid contamination of downstream crossflow sensors.

Holmes, Bruce J.↗
NASA NTRS1998

Satellite Investigations of Aerosol Radiative Forcing

Biomass burning aerosols have a wide spatial distribution that is governed by the geographic distribution of their source regions and tropospheric circulation. Annually, more than 114 teragrams of smoke is produced that have residence times ranging from days to weeks depending upon their size and chemical composition. These aerosols reflect the incoming solar directly which is called the "direct effect" and they also modify the reflective properties of clouds which is called the "indirect effect". The direct top of atmosphere (TOA) globally averaged radiative forcing estimate range from -0.2 to -1.1 W/sq m . The uncertainties in this estimate are due to the various assumptions (see Introduction) involved in the calculations. While the TOA radiative forcing estimates provide valuable information on the effects of aerosols on climate, equally important are the downward shortwave irradiances (DSWI) at the surface and the atmospheric heating/cooling rate profiles. For example, the DSWI irradiance calculations show large discrepancies between measurements and calculations in the presence of biomass burning aerosols due to the inaccurate characterization of aerosols in radiative transfer models. The DSWI is an important component of the surface radiation balance and the atmospheric effects govern both local and regional circulation patterns. Very few studies have attempted to estimate the surface and atmospheric effects of biomass burning aerosols largely due to the lack of information on the microphysical and chemical properties of biomass burning aerosols. The major focus of this effort is to estimate the direct TOA radiative forcing of aerosols using satellite measurements.

Christopher, Sundar A.↗
NASA NTRS2004

Wind Flow Simulation Around NASA KSC Vehicle Assembly Building

A model of the wind flow conditions around Kennedy Space Center (KSC) Vehicle Assembly Building (VA B) is presented. An incompressible Navier-Stokes flow solver was used to compute the flow field around fixed Launch Complex 39 (LC-39) buildings and structures. The 3-D flow field. including velocity magnitude and velocity vectors, was established to simulate the localized wind speeds and directions at specified locations in and around LC-39 buildings and structures. The results of this study not only help explain the physical phenomena of the flow patterns around LC-39 buildings but also are useful to the Shuttle personnel. Current Operations and Maintenance Requirements and Specifications (OMRS) for vehicle transfer operations are based on empirically derived historical data, and no detailed mathematical analysis of wind conditions around LC-39 structures has ever been accomplished.

Vu, B. T.↗
NASA NTRS1976

The realities of recoil - Ar-39 recoil out of small grains and anomalous age patterns in Ar-39-Ar-40 dating

Excess Ar-39 in olivine from neutron-irradiated mixtures of olivine and K-rich glass was measured to determine the amount of Ar-39 transferred by recoil out of the glass and into the surrounding olivine grains. It was found that a total of 9.0% of the total Ar-39 recoiled out of the 3-micron glass grains and 2.45% out of the 15-micron glass grains. The mean depth of Ar-39 depletion of the surface of the glass grains was 0.1 micron.

Huneke, J. C.↗
NASA NTRS2022

Flow Visualization, Heat Transfer, and Critical Heat Flux of Flow Boiling in Earth Gravity with Saturated Liquid-Vapor Mixture Inlet Conditions – In Preparation for Experiments Onboard the International Space Station

This study investigates flow boiling of n-Perfluorohexane with saturated two-phase mixture inlet in a rectangular channel of dimensions 114.6-mm heated length, 2.5-mm width, and 5 mm-height. The experiments were performed as part of the Mission Sequence Testing of the Flow Boiling and Condensation Experiment’s (FBCE) Flow Boiling Module (FBM) in the vertical upflow configuration in Earth gravity using the same experimental system that was launched to the International Space Station (ISS) in August 2021. The operating parameters varied are heating configuration (single- and double-sided), mass velocity (380 – 2400 kg/m2s), inlet quality (0.011 – 0.519), and inlet pressure (120 – 179 kPa). High-speed video photographs are presented to explain the two-phase flow patterns within the channel’s heated length. Flow patterns are constituted by low-density and high-density fronts moving along the channel, with the high-density fronts gradually reducing in length due to evaporation. Heat transfer results in terms of flow boiling curves, streamwise wall temperature profiles, streamwise heat transfer coefficient profiles, and average heat transfer coefficients are presented and trends discussed. CHF data from the present experiments are combined with prior databases to compile a consolidated FBCE-CHF database for saturated inlet to expand the ranges of operating conditions and include other flow orientations in Earth gravity. Experimental CHF trends are also discussed. The interfacial lift-off model shows a good CHF predictive accuracy evidenced by a mean absolute error of 11.97% for this consolidated database after constraining it to mass velocities greater than or equal to 500 kg/m2s. Finally, this study confirmed reliability of the upcoming ISS experiments for saturated inlet conditions and the collected Earth-gravity data will be compared to ISS microgravity data.

Flow boiling↗