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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 433 records · Page 24
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Enhancing the activity of Fe-N-C oxygen reduction reaction electrocatalysts by high-throughput exploration of synthesis parameters

Here, the most active class of platinum group metal-free (PGM-free) oxygen reduction reaction (ORR) electrocatalysts in acidic electrolytes are those synthesized by heat treatment of iron, carbon, nitrogen precursors (Fe-N-C). Due to the large number of possible precursor compounds, a small fraction of the synthesis variable space has been explored. Correlation of synthesis variables with Fe speciation and ORR activity has been limited. In this work, an automation platform and a multi-port ball-milling were utilized to evaluate the effects of synthesis variables, such as identity of iron precursor, iron loading, and carbon and nitrogen sources on the ORR activity of iron -nitrogen-carbon catalysts in acidic electrolyte. The ORR activity is correlated with catalyst Fe speciation determined using Fe K-edge X-ray absorption spectroscopy (XAFS).

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