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At least 433 records · Page 24

High Efficiency Travelling Wave X-Band Linac With Tunable Output Energy

We are designing a compact and efficient electron linac with 500 W of average beam power and beam energy tunable from 5 to 10 MeV. The accelerator is of travelling wave type, and has little RF power reflected back to the RF source, eliminating the need for a large, lossy isolator. The structure is powered by a compact commercial 1.7 MW 9.3 GHz magnetron. To vary the beam energy we will change the current from the triode gun. We present an analysis of the structure, which includes varying the length from 60 cm to 80 cm, and the structure type, such as constant impedance versus constant gradient.

Romero, Agustin↗

Recent progress in shattered pellet injection technology in support of the ITER disruption mitigation system*

Shattered pellet injection (SPI) has been selected as the baseline technology for the disruption mitigation (DM) system for ITER. Typical SPI utilizes cryogenic cooling to desublimate low pressure (<100 mbar) gases onto a cold zone within a pipe gun barrel, forming a cylindrical pellet. Pellets are dislodged from the barrel and accelerated using either a gas driven mechanical punch or high-pressure light-gas delivered by a fast-opening valve. SPI technology developed at Oak Ridge National Laboratory is currently deployed and operational on DIII-D, JET, and KSTAR. These SPI systems are used in experiments for physics scaling to ITER thermal mitigation and runaway electron dissipation/avoidance. The pellet sizes used for these machines are in the range of 4 to 12.5 mm in diameter with length to diameter ratios (L/D) of ~1.5. The current plan for ITER SPI is to utilize pellets that are 28.5 mm in diameter with an L/D of ~2. Furthermore, the large pellet sizes, high steady-state magnetic fields, and limitations of operating in a radiation environment render much of the current technology unusable. In addition to technology improvements, a deeper understanding of pellet material properties, formation, and release is being developed for implementation in future SPI designs, specifically ITER.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

An R&D program for milliampere spin-polarized electron beams

The electron injector driving the positron conversion target for Ce+BAF requires a spin-polarized beam with at least 1 mA of average current. While the parameters are not unusual from a beam dynamics point of view, the high average current is challenging due to the finite charge lifetime of the GaAs-based high-polarization photocathodes, even when operated in state-of-the-art load-lock photo-guns. We discuss the dominant limitations and present a systematic experimental program at the Gun Test Stand aiming to overcome them. With a multi-pronged approach involving a redesign of the photo-gun electrodes and an optimized drive laser profile, we hope to demonstrate a charge lifetime in excess of 1 kC from a high-polarization photocathode, mitigating one of the main risks in the injector design.

Bruker, Max [Thomas Jefferson National Accelerator↗

Simulating Electron Impact Ionization using a General Particle Tracer (GPT) Custom Element

A new C++ custom element has been developed with the framework of General Particle Tracer (GPT) to simulate electron impact ionization of residual gas molecules. The custom element uses Monte-Carlo routines to determine both the ion production rate and the secondary electron kinetic energy based on user-defined gas densities and theoretical values for the ionization cross section and the secondary electron differential cross section. It then uses relativistic kinematics to track the secondary electron, the scattered electron, and the newly formed ion after ionization. The ion production rate and the secondary electron energy distribution determined by the custom element have been benchmarked against theoretical calculations and against simulations made using the simulation package IBSimu. While the custom element was originally built for particle accelerator simulations, it is readily extensible to other applications. The custom element will be described in detail and examples of applications at the Thomas Jefferson National Accelerator Facility will be presented for ion production in a DC high voltage photo-gun.

Yoskowitz, J. T.↗

Sputtering Erosion in Ion and Plasma Thrusters

Low energy sputtering of molybdenum, tantalum and boron nitride with xenon ions are being studied using secondary neutral and secondary ion mass spectrometry (SNMS/SIMS). An ultrahigh vacuum chamber was used to conduct the experiment at a base pressure of 1x10(exp -9) torr. The primary ion beam is generated by an ion gun which is capable of delivering ion currents in the range of 20 to 500 nA. The ion beam can be focused to a spot size of approximately 1 mm in diameter. The mass spectrometer is positioned 10 mm from the target and 90 deg to the primary ion beam direction. SNMS and SIMS spectra were collected at various incident angles and different ion energies. For boron nitride sputtering, the target was flooded with an electron beam to neutralize the charge buildup on the surface. In the SNMS mode, sputtering of Mo and Ta can be detected at an ion energy as low as 100 eV whereas in boron nitride the same was observed up to an energy of 300 eV. However, in the positive-SIMS mode, the sputtering of Mo was observed at 10 eV incident ion energy. The SIMS spectra obtained for boron nitride clearly identifies the two isotopes of boron as well as cluster ions such as B2(sup +) and molecular ions such as BN(sup +). From the angle versus yields measurements, it was found that the maximum SNMS yield shifts towards lower incident angles at low ion energies for all three samples.

Ray, Pradosh K.↗

X-ray emission from high temperature plasmas

The physical processes occurring in plasma focus devices were investigated with particular emphasis on X-ray emission. Topics discussed include: trajectories of high energy electrons; detection of ion trajectories; spatial distribution of neutron emission; space and time resolved emission of hard X-rays from a plasma focus; the staged plasma focus as a variation of the hypocloidal pinch; formation of current sheets in a staged plasma focus; and X-ray and neutron emission from a staged plasma focus. The possibility of operating dense plasma-focus type devices in multiple arrays beyond the scaling law for a single gun is discussed.

Harries, W. L.↗

Unveiling Clues from Spacecraft Missions to Comets and Asteroids through Impact Experiments

The Deep Impact Spacecraft mission was the first to boldly face the challenge of impacting the surface of a comet, 9P/Tempel 1, to investigate surface and subsurface 'pristine' materials. The Stardust mission to Comet 81P/Wild 2 brought back an exciting surprise: shocked minerals which were likely altered during the comet's lifetime. Signatures of shock in meteorites also suggest that the violent past of the solar system has left our small bodies with signatures of impacts and collisions. These results have led to the question: How have impacts affected the evolutionary path taken by comets and asteroids, and what signatures can be observed? A future planetary mission to a near-Earth asteroid is proposing to take the next steps toward understanding small bodies through impacts. The mission would combine an ESA led AIM (Asteroid Impact Mission) with a JHU/APL led DART (Double Asteroid Redirect Mission) spacecraft to rendezvous with binary near-Earth asteroid 65803 Didymus (1996 G2). DART would impact the smaller asteroid, 'Didymoon' while AIM would characterize the impact and the larger Didymus asteroid. With these missions in mind, a suite of experiments have been conducted at the Experimental Impact Laboratory (EIL) at NASA Johnson Space Center to investigate the effects that collisions may have on comets and asteroids. With the new capability of the vertical gun to cool targets in the chamber through the use of a cold jacket fed by liquid nitrogen, the effects of target temperature have been the focus of recent studies. Mg-rich forsterite and enstatite (orthopyroxene), diopside (monoclinic pyroxene) and magnesite (Mg-rich carbonate) were impacted. Target temperatures ranged from 25 deg to -100 deg, monitored by connecting thermocouples to the target container. Impacted targets were analyzed with a Fourier Transform Infrared Spectrometer (FTIR) and Transmission Electron Microscope (TEM). Here we present the evidence for impact-induced shock in the minerals through both spectra and TEM imaging and compare with unshocked samples.

Lederer, Susan M.↗

Non-Intrusive Load Monitoring of EBW Processes A Second Study [Slides]

The Objective is to Determine if induced off-nominal welding disturbances: (1) Beam arc out (weld on high vapor pressure aluminum plate); (2) Pulsed beam voltage; (3) Pulsed beam current; and (4) Pulsed beam focus current can be observed in the input power to the high-voltage cabinet powering the EB gun, ie Non-Instrusive Load Monitoring (NILM).

36 MATERIALS SCIENCE↗

The use of silica aerogel to collect interplanetary dust in space

We report on impact experiments to evaluate the suitability of silica aerogel as a capture medium for interplanetary dust particles in space. The structure of silica aerogel is such that even micrometer-sized hypervelocity particles may sense it as a target of very low density; consequently shock stresses and temperatures due to impact should be minimized. We performed impact experiments in a light gas gun that employed projectiles manufactured from forsterite, pyrrhotite, and calcite. From these experiments we have developed techniques that will permit the successful extrication of interplanetary dust particles from aerogel. We note a rough correlation between increasing particle penetration lengths and decreasing aerogel density, and there is a poor correlation of track lengths with impact velocity at laboratory-attainable velocities of 5-7 km/s. We conclude that aerogel track length should not be used even as (crude) velocity indicators. Transmission electron microscope studies show the re covered particulate residues are encased in melted silica aerogel, which possibly protects the residue from some impact damage. Individual minerals within interplanetary dust are expected to exhibit differential survival, and may be vaporized, melted, dehydrated, or structurally reordered. However, some mineral grains should successfully be captured in an unmelted state at encounter velocities less than 8 km/s.

Zolensky, Michael E.↗

X-Ray Microanalysis and Electron Energy Loss Spectrometry in the Analytical Electron Microscope: Review and Future Directions

This paper reviews and discusses future directions in analytical electron microscopy for microchemical analysis using X-ray and Electron Energy Loss Spectroscopy (EELS). The technique of X-ray microanalysis, using the ratio method and k(sub AB) factors, is outlined. The X-ray absorption correction is the major barrier to the objective of obtaining I% accuracy and precision in analysis. Spatial resolution and Minimum Detectability Limits (MDL) are considered with present limitations of spatial resolution in the 2 to 3 microns range and of MDL in the 0.1 to 0.2 wt. % range when a Field Emission Gun (FEG) system is used. Future directions of X-ray analysis include improvement in X-ray spatial resolution to the I to 2 microns range and MDL as low as 0.01 wt. %. With these improvements the detection of single atoms in the analysis volume will be possible. Other future improvements include the use of clean room techniques for thin specimen preparation, quantification available at the I% accuracy and precision level with light element analysis quantification available at better than the 10% accuracy and precision level, the incorporation of a compact wavelength dispersive spectrometer to improve X-ray spectral resolution, light element analysis and MDL, and instrument improvements including source stability, on-line probe current measurements, stage stability, and computerized stage control. The paper reviews the EELS technique, recognizing that it has been slow to develop and still remains firmly in research laboratories rather than in applications laboratories. Consideration of microanalysis with core-loss edges is given along with a discussion of the limitations such as specimen thickness. Spatial resolution and MDL are considered, recognizing that single atom detection is already possible. Plasmon loss analysis is discussed as well as fine structure analysis. New techniques for energy-loss imaging are also summarized. Future directions in the EELS technique will be the development of new spectrometers and improvements in thin specimen preparation. The microanalysis technique needs to be simplified and software developed so that the EELS technique approaches the relative simplicity of the X-ray technique. Finally, one can expect major improvements in EELS imaging as data storage and processing improvements occur.

Goldstein, J. I.↗

Spall and subsequent recompaction of copper under shock loading

Research was undertaken to study spall and subsequent recompaction of oxygen-free high-thermal-conductivity copper using a single-stage large-bore light gas gun capable of planar impacts. Gun experiments were conducted that produced an initial spall in the target with a subsequent recompaction of the spall damage/layer by the use of layered impactors. Symmetric spall experiments at similar conditions were also conducted as a control to the recompaction experiments. Photonic Doppler velocimetry was used to obtain the velocity history of the target’s back surface; these velocity histories were analyzed, and the results were compared to numerical simulations. After recovery of selected samples, the microstructure was analyzed using optical imaging microscopy and electron backscatter diffraction. Recompaction waves were clearly observed in the time-resolved data obtained at the back surface of the targets. Two different series of experiments were performed to understand the effect of damage morphology on the stress required for spall recompaction. In the initial series, the peak pressure of the first shock was systematically increased to alter the amount of damage in the material. While in the second series, the peak pressure of the second shock was increased, keeping the magnitude of the first shock relatively constant to understand the effect of peak stress on the recompaction process. Findings clearly show that recompaction results in a perturbed band of the microstructure at the location of the expected spall plane in all cases except where the peak stress of the second shock is lower than the critical value.

, recompaction↗

Thermal Excitation System for Shearography (TESS)

One of the most convenient and effective methods of stressing a part or structure for shearographic evaluation is thermal excitation. This technique involves heating the part, often convectively with a heat gun, and then monitoring with a shearography device the deformation during cooling. For a composite specimen, unbonds, delaminations, inclusions, or matrix cracking will deform during cooling differently than other more structurally sound regions and thus will appear as anomalies in the deformation field. However, one of the difficulties that cause this inspection to be dependent on the operator experience is the conventional heating process. Fanning the part with a heat gun by hand introduces a wide range of variability from person to person and from one inspection to the next. The goal of this research effort was to conduct research in the methods of thermal excitation for shearography inspection. A computerized heating system was developed for inspection of 0.61 m (24 in.) square panels. The Thermal Excitation System for Shearography (TESS) provides radiant heating with continuous digital measurement of the surface temperature profile to ensure repeatability. The TESS device functions as an accessory to any electronic shearography device.

Lansing, Matthew D.↗

Fabrication and field emission properties of vertical, tapered GaN nanowires etched via phosphoric acid

The controlled fabrication of vertical, tapered, and high-aspect ratio GaN nanowires via a two-step top-down process consisting of an inductively coupled plasma reactive ion etch followed by a hot, 85% H 3 PO 4 crystallographic wet etch is explored. The vertical nanowires are oriented in the $[0001]$ direction and are bound by sidewalls comprising of $\{33\bar{6}2\}$ semipolar planes which are at a 12° angle from the [0001] axis. High temperature H3PO4 etching between 60 °C and 95 °C result in smooth semipolar faceting with no visible micro-faceting, whereas a 50 °C etch reveals a micro-faceted etch evolution. High-angle annular dark-field scanning transmission electron microscopy imaging confirms nanowire tip dimensions down to 8–12 nanometers. The activation energy associated with the etch process is 0.90 ± 0.09 eV, which is consistent with a reaction-rate limited dissolution process. The exposure of the $\{33\bar{6}2\}$ type planes is consistent with etching barrier index calculations. The field emission properties of the nanowires were investigated via a nanoprobe in a scanning electron microscope as well as by a vacuum field emission electron microscope. Finally, the measurements show a gap size dependent turn-on voltage, with a maximum current of 33 nA and turn-on field of 1.92 V nm -1 for a 50 nm gap, and uniform emission across the array.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

Test and Analysis Capabilities of the Space Environment Effects Team at Marshall Space Flight Center

Marshall Space Flight Center has developed world-class space environmental effects testing facilities to simulate the space environment. The combined environmental effects test system exposes temperature-controlled samples to simultaneous protons, high- and low-energy electrons, vacuum ultraviolet (VUV) radiation, and near-ultraviolet (NUV) radiation. Separate chambers for studying the effects of NUV and VUV at elevated temperatures are also available. The Atomic Oxygen Beam Facility exposes samples to atomic oxygen of 5 eV energy to simulate low-Earth orbit (LEO). The LEO space plasma simulators are used to study current collection to biased spacecraft surfaces, arcing from insulators and electrical conductivity of materials. Plasma propulsion techniques are analyzed using the Marshall magnetic mirror system. The micro light gas gun simulates micrometeoroid and space debris impacts. Candidate materials and hardware for spacecraft can be evaluated for durability in the space environment with a variety of analytical techniques. Mass, solar absorptance, infrared emittance, transmission, reflectance, bidirectional reflectance distribution function, and surface morphology characterization can be performed. The data from the space environmental effects testing facilities, combined with analytical results from flight experiments, enable the Environmental Effects Group to determine optimum materials for use on spacecraft.

Finckenor, M. M.↗

ISPAE Research Highlights 1995-1997

This paper presents ISPAE (Institute for Space Physics, Astrophysics and Education) research highlights from 1995-1997. The topics include: 1) High-Energy Astrophysics (Finding the smoking gun in gamma-ray bursts, Playing peekaboo with gamma ray bursts, and Spectral pulses muddle burst source study, Einstein was right: Black holes do spin, Astronomers find "one-man X-ray band", and Cosmic rays from the supernova next door?); 2) Solar Physics (Bright burst confirms solar storm model, Model predicts speed of solar wind in space, and Angry sunspots snap under the strain); 3) Gravitational Physics; 4) Tether Dynamics; and 5) Space Physics (Plasma winds blow form polar regions, De-SCIFERing thermal electrons, and UVI lets scientists see daytime aurora).

Harwell, Ken↗

High-current electron sources for Superconducting Radiofrequency injectors

Accelerators are finding increasing use in numerous fields such as medicine, industry accelerator-based nuclear energy programs and others. A recent survey reveals only 20 high-energy accelerators worldwide serve elementary-particle physics while thousands of accelerators are routinely used in hospitals and industry (packaging, food sterilization, etc.).

43 PARTICLE ACCELERATORS↗

Micas in experimentally shocked gneiss

Powder-propellant guns are used to shock biotites and muscovites from a gneiss at pressures between 18 and 70 GPa. It is shown that shock in biotite and muscovite can produce homogeneous and devolatilized glasses within microseconds. Shock-deformed micas are found to exhibit fracturing, kinking, and complex extinction patterns over the entire pressure range investigated. Localized melting of micas commences at 33 GPa and reaches completion at 70 GPa. Even though melted biotite and muscovite are opaque optically, they exhibit extensive microvesiculation and flow when observed with the SEM. It is confirmed through electron diffraction that biotite and muscovite have transformed to a glass. The distribution of vesicles in shock-vitrified mica reveals escape of volatiles within the short duration of the shock experiment. It is noted that experimentally shocked biotite and muscovite undergo congruent melting. It is noted that the compositions of the glasses are similar to the unshocked micas except for volatiles (H2O loss and and K loss). These unusual glasses produced from mica can be quenched by rapid cooling conditions during the shock experiment. On the basis of the results, it is pointed out that the extremely low H2O content of tektites can be reconciled with a terrestrial origin by impact.

Lambert, P.↗

Influence of Photoemission Geometry on Timing and Efficiency in 4D Ultrafast Electron Microscopy

Broader adoption of 4D ultrafast electron microscopy (UEM) for the study of chemical, materials, and quantum systems is being driven by development of new instruments as well as continuous improvement and characterization of existing technologies. Perhaps owing to the still-high barrier to entry, the full range of capabilities of laser-driven 4D UEM instruments has yet to be established, particularly when operated at extremely low beam currents (~fA). Accordingly, with an eye on beam stability, we have conducted particle tracing simulations of unconventional off-axis photoemission geometries in a UEM equipped with a thermionic-emission gun. Specifically, we have explored the impact of experimentally adjustable parameters on the time-of-flight (TOF), the collection efficiency (CE), and the temporal width of ultrashort photoelectron packets. The adjustable parameters include the Wehnelt aperture diameter (DW), the cathode set-back position (Ztip), and the position of the femtosecond laser on the Wehnelt aperture surface relative to the optic axis (Rphoto). Notable findings include significant sensitivity of TOF to DW and Ztip, as well as non-intuitive responses of CE and temporal width to varying Rphoto. As a means to improve accessibility, practical implications and recommendations are emphasized wherever possible.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗