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DOE OSTI2024

A globally sampled high-resolution hand-labeled validation dataset for evaluating surface water extent maps

Effective monitoring of global water resources is increasingly critical due to climate change and population growth. Advancements in remote sensing technology, specifically in spatial, spectral, and temporal resolutions, are revolutionizing water resource monitoring, leading to more frequent and high-quality surface water extent maps using various techniques such as traditional image processing and machine learning algorithms. However, satellite imagery datasets contain trade-offs that result in inconsistencies in performance, such as disparities in measurement principles between optical (e.g., Sentinel-2) and radar (e.g., Sentinel-1) sensors and differences in spatial and spectral resolutions among optical sensors. Therefore, developing accurate and robust surface water mapping solutions requires independent validations from multiple datasets to identify potential biases within the imagery and algorithms. However, high-quality validation datasets are expensive to build, and few contain information on water resources. For this purpose, we introduce a globally sampled, high-spatial-resolution dataset labeled using 3 m PlanetScope imagery. Our surface water extent dataset comprises 100 images, each with a size of 1024×1024 pixels, which were sampled using a stratified random sampling strategy covering all 14 biomes. We highlighted urban and rural regions, lakes, and rivers, including braided rivers and coastal regions. We evaluated two surface water extent mapping methods using our dataset – Dynamic World, based on Sentinel-2, and the NASA IMPACT model, based on Sentinel-1. Dynamic World achieved a mean intersection over union (IoU) of 72.16 % and F1 score of 79.70 %, while the NASA IMPACT model had a mean IoU of 57.61 % and F1 score of 65.79 %. Performance varied substantially across biomes, highlighting the importance of evaluating models on diverse landscapes to assess their generalizability and robustness. Our dataset can be used to analyze satellite products and methods, providing insights into their advantages and drawbacks. Our dataset offers a unique tool for analyzing satellite products, aiding the development of more accurate and robust surface water monitoring solutions. The dataset can be accessed via https://doi.org/10.25739/03nt-4f29.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2026

Comparability of Liquid Chromatography Tandem Mass Spectrometry Analysis of Dissolved Organic Matter across Laboratories

Non-targeted liquid chromatography tandem highresolution mass spectrometry (LC−MS/MS) is increasingly applied for the structure-resolved chemical analysis of dissolved organic matter (DOM). With new developments in MS instrumentation and analysis software, the approach has gained substantial momentum over the past decade. However, achieving high-quality analytical data that is reproducible and comparable across laboratories can be a bottleneck in non-targeted metabolomics and organic matter chemical analysis, especially for data reuse in repository-scale analyses. Understanding the capabilities as well as challenges of comparing LC−MS/MS data from different laboratories is necessary for inferring global trends from public data sets. To illuminate instrumentation factors that drive differences and variability, we used a standardized data analysis pipeline, including classical (CMN) and featurebased molecular networking (FBMN), to analyze data from a ring trial by 24 laboratories on identical sample sets of algal and DOM extracts that were mixed in predefined concentrations and spiked with standards. Our results showed that data sets from similar mass spectrometer types with unified instrument parameters were qualitatively comparable, resolving the same general trends and shared mass spectral features. Interlaboratory comparability was best for high-intensity features, while low-intensity features showed greater detection variability. Our analysis also highlights challenges when comparing data from instruments with different acquisition rates or operating with less standardized methods. Lastly, we provide recommendations for data integration, public data sharing, standardization, and best practices for standardized LC−MS/MS data acquisition, which will be critical for long-term time series and intercomparability of DOM chemical analyses.

DOM↗

DOE OSTI2020

Pacific Northwest National Laboratory Annual Site Environmental Report for Calendar Year 2019 (Final Report)

The PNNL Annual Site Environmental Report is prepared to meet the requirements of DOE Order 231.1B, Environmental, Safety and Health Reporting, and DOE Order 458.1, Radiation Protection of the Public and the Environment, assuring that the public is informed of any PNNL Richland Campus or PNNL Sequim Campus event that could adversely affect the health and safety of the public, site staff, or the environment. The report provides a synopsis of ongoing environmental management performance and compliance activities for operations that occur on the PNNL Richland Campus in Richland, Washington, and at the PNNL Sequim Campus near Sequim, Washington. It describes the location of and background for each facility; addresses compliance with applicable DOE, federal, state, and local regulations and site-specific permits; documents environmental monitoring efforts and their status; presents potential radiation doses to staff and the public in the surrounding areas; and describes DOE-required data quality assurance methods used for data verification.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2023

An Alternating, Current-Induced Electromagnetic Field for Membrane Fouling and Scaling Control during Desalination of Secondary Effluent from Municipal Wastewater

Membrane treatment of secondary effluent for reuse applications is a promising approach to expand water supplies and provide flexibility to water resources management. However, effective control of membrane fouling and scaling is crucial for cost-effective treatment and system resilience. This study compared the performance of antiscalants to an alternating, current-induced electromagnetic field (EMF) as an alternative pretreatment method to reverse osmosis. Compared to the no-EMF control experiments, the EMF device resulted in 13% higher water recovery and 366% lower flux decline at 60% of water recovery, along with 2–8 times lower precipitation of fouling and scaling, as evidenced by scanning electron microscope, energy dispersive X-ray spectroscopy, and chemical extraction analysis. The combination of the EMF with antiscalant was more effective for reducing membrane fouling and scaling, increasing water recoveries up to 89.3%, as compared to the EMF (67.5%) and antiscalant-only (73.6%) configurations. This is the first study to demonstrate synergistic effects of using an EMF in combination with antiscalants and could lead to lower pretreatment costs. Additional research is required to quantify the economics of this approach and to fully understand the fundamental mechanisms governing fouling and scaling control by an EMF.

42 ENGINEERING↗

DOE OSTI2021

Pacific Northwest National Laboratory Annual Site Environmental Report for Calendar Year 2020. Final Report

The U.S. Department of Energy requires that all its site facilities develop an annual site environmental report to comply with DOE Order 231.1B, Chg 1, and DOE Order 458.1, Admin Chg 4. This report provides a synopsis of calendar year 2020 information related to environmental management performance and compliance efforts at Pacific Northwest National Laboratory. It summarizes site compliance with federal, state, and local environmental laws, regulations, policies, directives, permits, and Orders, and provides environmental management performance benchmarks and their status to the public, regulatory agencies, community officials, Native American tribes, and public interest groups.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2022

Pacific Northwest National Laboratory Annual Site Environmental Report for Calendar Year 2021 (Final Report)

The U.S. Department of Energy requires that all its site facilities develop an annual site environmental report to comply with DOE Order 231.1B Chg 1 and DOE Order 458.1 Admin Chg 4. This report provides a synopsis of calendar year 2021 information related to environmental management performance and compliance efforts at the Pacific Northwest National Laboratory. It summarizes site compliance with federal, state, and local environmental laws, regulations, policies, directives, permits, and Orders, and provides environmental management performance benchmarks and their status to the public, regulatory agencies, community officials, Native American tribes, and public interest groups.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2023

Pacific Northwest National Laboratory Annual Site Environmental Report for Calendar Year 2022 (Final Report)

Pacific Northwest National Laboratory (PNNL), one of the U.S. Department of Energy (DOE) Office of Science’s 10 national laboratories, provides innovative science and technology development in the areas of energy and the environment, fundamental and computational science, and national security. There are three DOE offices within the Richland area. Two are responsible for the Hanford Site, whereas the Pacific Northwest Site Office (PNSO) oversees PNNL. PNNL prepares this Annual Site Environmental Report to meet the requirements of DOE Order 231.1B, Environmental, Safety and Health Reporting, and DOE Order 458.1, Radiation Protection of the Public and the Environment, assuring that the public is informed of any PNNL-Richland Campus or PNNL-Sequim Campus event that could adversely affect the health and safety of the public, site staff, or the environment. The report provides a synopsis of ongoing environmental management performance and compliance activities for operations that occur on the PNNL-Richland Campus in Richland, Washington, and at the PNNL-Sequim Campus near Sequim, Washington. It describes the location of and background for each facility; addresses compliance with applicable DOE, federal, state, and local regulations, and site-specific permits; documents environmental monitoring efforts and their status; presents potential radiation doses to staff and the public in the surrounding areas; and describes DOE-required data quality assurance methods used for data verification. The ASER summarizes site compliance with federal, state, and local environmental laws, regulations, policies, directives, permits, and Orders, and provides environmental management performance benchmarks and their status to the public, regulatory agencies, community officials, Native American tribes, and public interest groups.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2025

Data for Kim et al., "Variations in the optical and molecular composition of dissolved organic matter exported from coastal wetlands"

Knowledge about sources and composition of marsh-derived dissolved organic matter (DOM) is critical for understanding the role of marshes in coastal biogeochemical cycling and the fate of marsh-derived DOM in the ocean. To investigate tidal variability in composition of marsh-derived DOM, Kim et al. examined the optical and molecular characteristics of hourly surface water samples at three tidal creeks in the Chesapeake Bay. Groundwater samples along the terrestrial landscape gradient as well as estuarine water from the adjacent estuary at each site were also collected to help resolve sources of surface water DOM. Samples were collected in summer 2024 at three sites – SWH: Sweet Hall Marsh, GCW: Kirkpatrick Marsh, and GWI: Goodwin Islands – which are part of synoptic sites in the Chesapeake Bay region of the COMPASS-FME (Coastal Observations, Mechanisms, and Predictions Across Systems and Scales - Field, Measurements, and Experiments) project. Surface water samples were collected hourly over a 48-hour period at each site. Groundwater and estuarine water samples were collected once. This dataset includes- Surface water depth and salinity- Dissolved organic carbon (DOC) and total dissolved nitrogen (TDN) concentrations- Optical indices and relative composition of parallel factor analysis (PARAFAC) components- High resolution mass spectrometry data.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2021

Redefining Net-Zero Water for Resilient Aquifers

Groundwater has long been a critical source of potable water, supplying one-third of all global water withdrawals and providing strategic reserves in times of drought (Konikow, 2012; Famiglietti, 2014). The risk in relying on groundwater is that it is often pumped at rates far greater than it can be naturally replenished. With increasing population and a changing climate, the depletion of potable water supplies has become an ever-growing concern (Srinivasan et al., 2012). Recently, the concept of “resilience” has been applied to groundwater, leaving many questions to be explored in terms of what resilience should mean for aquifers (Foster and MacDonald, 2014; Grönwall and Oduro-Kwarteng, 2017). The term is commonly used to indicate resilience to impacts of climate change specifically, but here we consider resilience in the context of more general water insecurity. Relatedly, the concept of “sustainable yield” has emerged in an attempt to determine a metric that can ensure the long-term resilience of groundwater systems, but the definition is fraught with inherent uncertainties and its quantification poses challenges (Rudestam and Langridge, 2014; Grönwall and Oduro-Kwarteng, 2017). At the heart of these concepts is a focus on sustainable management of aquifers. A sustainable approach to managing groundwater resources usually involves balancing long-term abstraction with the long-term recharge taking into account the needs for environmental flows and implementing drought-preparedness measures (Robins et al. 2006; Foster and MacDonald, 2014). At a high level, a sustainable balance of groundwater abstraction versus aquifer recharge may be considered “Net Zero” (NZ) or “Net Positive” (NP) in cases where recharge is equal to or in excess of abstraction, respectively. However, NZ/NP water management programs that address these concerns have varied definitions of compliance, which include considerations for the application at hand (ILFI, 2020; USGBC, 2020). Locations with high risk of low or poor water supply may be particularly interested in pursuing NZ/NP water. The AQUEDUCT Water Risk Atlas (World Resources Institute, 2019) indicates long-term availability, providing risk levels for quantity and quality of water at specific locations across the globe, for existing and predicted future conditions. This paper follows the U.S. Department of Energy (DOE) Federal Energy Management Program (FEMP) NZ water definition adopted by the U.S. Army for use at their installations, including Army Reserve Centers (ARCs). This definition also relates to the U.S. Army’s current focus on water resilience, which includes short-term and long-term availability of water resources.

net zero water, HUC12, Saipan, American Samoa, Mau↗

DOE OSTI2021

Experimental study of plate materials for evaporative air coolers

Following paper presents an experimental study on eight potential plate materials for evaporative air coolers. There are three groups of materials: currently used plate materials (kraft papers), new natural origin plate materials (cotton fibers), and new synthetic plate materials (synthetic fibers). Proposed materials were examined in terms of different properties such as upward and downward distribution height, water capacity, durability and diffusivity. The results were compared with data presented by other authors. It was established that, synthetic materials are characterized by superior water distribution qualities in comparison to the materials of natural origin. Basalt paper-like synthetic fiber allowed to rise water vertically to 40 cm during 120 min tests. The highest water rise obtained in other studies was 18 cm, hence basalt paper-like fiber is visibly superior in comparison with the currently known materials. In terms of downward water distribution, two new synthetic surfactant non-wovens show better performance than the existing materials by quickly and evenly distributing water over the entire length of the sample. The durability of synthetic fibers and non-wovens is higher comparing with the materials of natural origin. The results show that synthetic materials are better suited to the role of plate materials in evaporative air coolers.

Experiment↗

DOE OSTI2025

From Pure to Seawater Electrolysis: Unveiling the Impact of Ionic Species and Contaminants on Electrocatalysis

Water electrolysis, including seawater splitting to produce hydrogen and oxygen, stands as a promising approach for the efficient storage of intermittent energy. However, the half-reactions of water splitting, the oxygen evolution reaction (OER) and hydrogen evolution reaction (HER), are known to be very sensitive toward the quality of water employed and are susceptible to contaminants originating from various sources, including the electrolyte or the electrodes. Those contaminants have a profound impact on the activity of these reactions of water splitting by modifying the electronic and physical structures of electrocatalysts as well as electrode–electrolyte interfaces. For seawater electrolysis, the unintentional presence of impurities, such as anions, cations, and organic compounds, affects the catalyst stability, selectivity, and activity. Despite the existence of numerous comprehensive reviews that delve into various aspects of catalysts and their structure–property relationships for several electrocatalytic reactions, the impact of contaminants has often been ignored. This critical review endeavors to address this issue by providing an overview of the diverse sources of contaminants influencing electrocatalytic water splitting and seawater splitting reactions, delineating the trends in electrochemical parameters and detailing different characterization methods for elucidating the physical and electronic changes of the electrode and electrolyte.

HER↗

DOE OSTI2021

Controlled dehumidification to extract clean water from a multicomponent gaseous mixture of organic contaminants

Rapid expansion of the unconventional oil and gas extraction has increased American energy independence, but also led to increased production of large amounts of contaminated water. Wastewater from the oil and gas industry contains a wide range of contaminants. Injecting such contaminated water into disposal wells or discharging it to the environment jeopardizes freshwater resources. Conventional and membrane-based wastewater treatment techniques are often not effective choices to treat highly contaminated wastewater; however, a suitable way to remove contaminants from wastewater is to selectively separate water in a process analogous to humidification-dehumidification (HDH). Only a few studies have investigated the use of HDH for wastewater treatment. In this study, a novel HDH system is introduced for treating highly contaminated water, such as oil and gas flowback and produced water. In this HDH process, a non-condensable gas, such as air, mixes with wastewater vapor to facilitate the separation of contaminants. As a result, clean water condenses from the multicomponent gaseous mixture while air carries organic contaminants out of the dehumidification section. A laboratory apparatus was constructed and experiments were performed to investigate the HDH process for wastewater treatment and to study the effects of flow dynamics including air flow rate on the composition of treated water. Different contaminants including benzene, toluene, 2-propanol and 2-butoxyethanol were tested. Experimental results showed that the system can be successfully applied for removing volatile and/or toxic organic contaminants from wastewater. A representative multicomponent mixture of fracking wastewater was successfully treated using the experimental setup and clean water with quality of 98.3% was obtained. It was revealed that increasing the air-to-vapor mass ratio improves purity of treated water. Quantitative analysis showed that by increasing the air-to-vapor mass ratio from 0.6 to 5.9, the fraction of separated 2-propanol through the air was improved from 43% to more than 96% of the initial amount. ASPEN software was employed to simulate equilibrium conditions. Finally, experimental results were observed to have lower mass fraction of residual contaminant in the treated water compared to equilibrium state.

42 ENGINEERING↗

DOE OSTI2023

Sea–Level Rise Impacts on Tidal Marshes and Estuarine Biogeochemical Processes

We used a numerical model to investigate the effects of sea-level rise (SLR) on the biogeochemical processes in the York River Estuary with extensive tidal marshes. The fully-coupled hydrodynamic-water quality-marsh model accounts for the spatial and temporal variations of physical-biogeochemical interactions between the tidal marshes and surrounding waters. This study focuses on an SLR scenario where the vertical accretion of tidal marshes keeps pace with the rising sea levels. Results show that SLR amplifies the tidal range and prolongs flooding duration, which results in enhanced porewater exchanges of materials between the tidal marshes and the surrounding waters. The increased availability of shallow-water habitats and enhanced light utilization in the shallow areas under SLR promote phytoplankton production (PP) in the shallow-water regions of the York River. Consequently, the organic carbon in the open water is fueled by the contributions from shallow waters and the enhanced export of organic carbon from the marshes. The change in the dissolved oxygen (DO) budget in the York River Estuary is attributed to changes in water column respiration, net metabolism of the benthic layer, reaeration, PP, and increased stratification under SLR. The net DO flux out of the York River increases at the York River mouth. Diel DO variation, especially in the marshes in the upper estuary, promotes phosphorus release from the sediment. The changes in dissolved nitrogen under SLR are relatively minimal.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2021

SPRUCE Outflow Chemistry Data for Experimental Plots Beginning in 2016

This data set includes the chemistry of outflow waters in the SPRUCE experiment plots located in the S1 bog of the USDA Forest Service Marcell Experimental Forest (MEF) in northern Minnesota, 40 km north of Grand Rapids. These data are post-treatment data from the warming and elevated carbon dioxide (CO2) treatments associated with the SPRUCE experiment. There are ten experimental plots in SPRUCE: five temperature treatments (+0, +2.25, +4.5, +6.75, +9°C) at ambient CO2, and the same five temperature treatments at elevated CO2 (+500 ppm). Sample collection and analyses started in March of 2016 and will continue for the duration of the experiment. Samples were analyzed for pH, specific conductivity, anion concentrations (chloride, sulfate), cation concentrations (calcium, potassium, magnesium, sodium, aluminum, iron, manganese, silicon, strontium), nutrient concentrations (ammonium, nitrate, soluble reactive phosphorus, total nitrogen, total phosphorus), and total organic carbon (TOC) concentrations. Subsets of the samples have been analyzed for natural-abundance stable isotopes of water (δ18O-H2O and δD-H2O), dissolved carbon dioxide (δ13C-CO2), and dissolved methane (δ13C-CH4), and concentrations of total mercury (Thg), methylmercury (MeHg), ferrous iron (Fe2+), ferric iron (Fe3+), dissolved inorganic carbon (DIC), and dissolved methane (CH4).

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2021

Quality Data Essential for Modeling Water Cycles Effectively

The experimental and observational data is the backbone of effective modeling of all aspects of water cycles. As the computer technology used for these data gathering efforts has improved dramatically in the recent decades, the environmental conditions these instruments are subjected to remain pretty much the same. These measuring instruments are exposed to the sun light, wind, rain, snow and ice; and they are immersed in dirt, water and mud. All of these are damaging to the electronics components used for data gathering, storage, and transmission, which creates many different kinds of data quality issues that affect the quality and reliability of modeling and prediction efforts.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2024

Environmental Performance Report 2023: Annual Site Environmental Report per the U.S. Department of Energy Order 231.1B Chg 1

The National Renewable Energy Laboratory's (NREL's) Environmental Performance Report provides a description of the laboratory's environmental management activities in calendar year 2023, including information on environmental and sustainability performance, environmental compliance activities and status, and environmental protection programs, highlights, and successes. The purpose of this report is to ensure that the U.S. Department of Energy (DOE) and the public receive timely, accurate information about events that have positively affected or could adversely affect the health and safety of the public or workers, the environment, or the operations of DOE facilities. This report meets the DOE requirements of the Annual Site Environmental Report (ASER) and has been prepared in accordance with DOE Order 231.1B Chg 1, Environment, Safety and Health Reporting.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

DOE OSTI2022

Discovery of Graphene-Water Membrane Structure: Toward High-Quality Graphene Process

It is widely accepted that solid-state membranes are indispensable media for the graphene process, particularly transfer procedures. But these membranes inevitably bring contaminations and residues to the transferred graphene and consequently compromise the material quality. This study reports a newly observed free-standing graphene-water membrane structure, which replaces the conventional solid-state supporting media with liquid film to sustain the graphene integrity and continuity. Experimental observation, theoretical model, and molecular dynamics simulations consistently indicate that the high surface tension of pure water and its large contact angle with graphene are essential factors for forming such a membrane structure. More interestingly, water surface tension ensures the flatness of graphene layers and renders high transfer quality on many types of target substrates. This report enriches the understanding of the interactions on reduced dimensional material while rendering an alternative approach for scalable layered material processing with ensured quality for advanced manufacturing.

36 MATERIALS SCIENCE↗

DOE OSTI2026

Guideline for Characterizing and Evaluating a Candidate Project Site for Solar Thermal Applications

This document presents a structured procedure for characterizing and evaluating candidate project sites for concentrating solar power (CSP) and solar heat for industrial processes (SHIP) applications. The objective is to provide project developers, researchers, and other stakeholders with a consistent, technology-agnostic framework for early-stage site assessment, enabling informed decision-making prior to significant investment in project development. Site selection is a critical factor in project success or failure for both CSP and SHIP projects. Key factors such as solar resource availability, land characteristics, environmental and regulatory constraints, infrastructure availability, and community context are determined by the choice of project site and can materially impact project performance, cost, schedule, and overall viability. This procedure is designed to systematically evaluate these factors, identify potential fatal flaws, and prioritize the most favorable candidate sites for further development. The process begins with rapid screening-level evaluation, using publicly available data to assess solar resource, land availability and suitability, zoning and land-use compatibility, and exclusion zones such as protected lands or sensitive habitats. Sites that meet the minimum screening criteria advance to a more detailed characterization. Subsequent sections of this report provide guidance for a next-level assessment of the most important technical and environmental parameters, including: 1) Solar resource quality, variability, and uncertainty using multiyear datasets and, where appropriate, on-site measurement campaigns; 2) Meteorological conditions such as wind, temperature, extreme weather events, and soiling impacts; 3) Land characteristics including slope, shading, and geotechnical conditions; and 4) Environmental and regulatory considerations, including permitting processes, endangered species, cultural resources, and visual impacts. The procedure also addresses infrastructure and integration considerations, including: 1) Grid interconnection requirements for CSP power generation projects; 2) Electrical and operational integration for SHIP facilities; 3) Water availability, quality, and permitting constraints, which are particularly critical for CSP in arid regions; and 4) Site access, construction logistics, and availability of workforce and supporting services. Recognizing the importance of social and economic context, the procedure includes evaluation of community engagement factors, such as stakeholder sentiment, proximity to sensitive visual receptors, workforce development opportunities, and local economic incentives. The outputs of these assessments are synthesized in a cost and risk evaluation, translating site characteristics into expected impacts on capital cost, operating cost, schedule, and technical risk. This is complemented by screening-level performance modeling, including 8760 simulations and long-term projections, to quantify expected energy or thermal output, assess variability thereof, and support comparison between candidate sites. Finally, the procedure provides high-level guidance on a structured go/no-go decision framework, categorizing sites based on identified risks and constraints, and outlining a clear path forward to feasibility studies and front-end engineering design for viable projects. By standardizing the site characterization process across both CSP and SHIP applications, this guideline aims to: 1) Improve consistency and transparency in early-stage project evaluation; 2) Reduce development risk and avoid investment in nonviable project sites; 3) Support collaboration between developers, researchers, and public agencies; and 4) Accelerate successful deployment of concentrating solar technologies for both power generation and industrial process heat.

14 SOLAR ENERGY↗