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At least 433 records · Page 24

Analysis of Igniter/Promoter Material Effects on Burn Length Variability in Astm G124 Standard Testing

ASTM G124 refers to the “Standard Test Method for Determining the Combustion Behavior of Metallic Materials in Oxygen Enriched Atmospheres”. Major test parameters are well defined in the standard and a detailed description of how to set up and conduct the test is also included. However, one variable - the igniter/promoter system - is not clearly restricted or specified. Due to the fact that this igniter/promoter system is not definitively specified, multiple materials have been used. This lack of specificity in igniter/promoter material was identified as a potential source of variability in test results, and as such has been selected for this study as a parameter to analyze and identify if the igniters/promoters should be standardized. For that purpose, several igniter/promoter systems have been selected (that were currently in use at various laboratories) which would be tested via ASTM G124 with Inconel 718 test rods. Testing was conducted over two phases – the first for screening promoter effects in the transition region of the material, and the second for comparing measured flammability thresholds identified through testing by each igniter/promoter type. The results of this study have found that igniter/promoter material is not a statistically significant factor in the variability of burn length in test samples. Initial results showing variability was likely due to small sample size, as the issue became less pronounced once more samples were tested and more data generated. Each of the igniter/promoter systems tested were effective at determining flammability thresholds and so it is concluded that no specific igniter/promoter needs to be identified in the ASTM G124 test standard.

oxygen compatibility↗

NASA Earth Science Technology Office (ESTO) Advanced Information Systems Technology (AIST) Program: Earth Systems Digital Twins (ESDT) Standards for Interoperable Digital Twins Workshop Presentations

On September 18, 2023, NASA Earth Science Technology Office (ESTO) Advanced Information Systems Technology (AIST) Program conducted a mini-workshop that brought together seven experts to survey and discuss "Standards for Interoperable Digital Twins". Since three years, the AIST Program has been developing technologies and prototypes for Earth System Digital Twins (ESDT). During those developments and after the ESDT Workshop held in October 2022, it became clear that standard for ESDT interoperability were needed and should be defined as soon as possible. To address this challenge, the AIST program will survey ongoing development for Digital Twins standards in various domains and the September 18, 2023 Workshop represented the first step towards this understanding. Speakers during this event included: Michael Grieves (Digital Twin Institute), Siri Jodha Singh Khalsa (IEEE GRSS Standards), Trent Tinker (OGC), Ryan Berkheimer (NOAA), John Stone (NVIDIA), Thomas Geenen (ECMWF-DestinE) and Arne Berre (SINTEF-Iliad DTO and EDITO). This presentation regroups all the speakers' presentations.

Earth Science Remote Sensing; Information Systems↗

Standards for Interoperable Digital Twins

On September 18, 2023, NASA Earth Science Technology Office (ESTO) Advanced Information Systems Technology (AIST) Program conducted a mini-workshop that brought together seven experts to survey and discuss "Standards for Interoperable Digital Twins". Since three years, the AIST Program has been developing technologies and prototypes for Earth System Digital Twins (ESDT). During those developments and after the ESDT Workshop held in October 2022, it became clear that standard for ESDT interoperability were needed and should be defined as soon as possible. To address this challenge, the AIST program will survey ongoing development for Digital Twins standards in various domains and the September 18, 2023 Workshop represented the first step towards this understanding. Speakers during this event included: Michael Grieves (Digital Twin Institute), Siri Jodha Singh Khalsa (IEEE GRSS Standards), Trent Tinker (OGC), Ryan Berkheimer (NOAA), John Stone (NVIDIA), Thomas Geenen (ECMWF-DestinE) and Arne Berre (SINTEF-Iliad DTO and EDITO). This movie represents the recording of this event.

Earth Science Remote Sensing↗

Overview of the Findings of the Extreme Environment Power Systems Standards Evaluation and Gap Analysis

This lightning talk gives an overview of the findings of the NASA funded Extreme Environment Power Systems Standards Evaluation and Gap Analysis. This document highlighted the gaps between terrestrial distribution system component standards and future lunar distribution system component standards. This shows that existing standards cannot be applied with small modifications for the lunar environment.

electrical power↗

Enabling Open and Interoperable Science: Multi-Omics Data Processing Platform with NASA GeneLab Standardized Bioinformatics Workflows for Space and Earth Research

Multi-omics biological data continues to be generated at an astounding pace. Genomics, transcriptomics, metabolomics, and proteomics, or collectively known as multi-omics data, are used to assess biological functions, and provide invaluable insights into human, animal, plant, and environmental health both on Earth and in Space. Despite the abundance of these valuable data, the need for bioinformatics expertise, particularly as it relates to the niche filed of space biology, and a lack of accessible resources for processing these data limit their usefulness in deriving biological insights. The NASA Open Science Data Repository (OSDR) provides access to omics data from various spaceflight and analog studies. To enhance the accessibility and reusability of these data, GeneLab (part of OSDR) designs and implements standardized, community-driven, open-source bioinformatics workflows to transform raw omics data into standardized processed data. Currently, GeneLab-processed data from hundreds of space studies have been reused for meta-analyses. This has led to new insights and scientific publications that extend beyond the initial research, thereby enriching our understanding of molecular-scale biological responses to the space environment. To make these bioinformatics workflows open and accessible, GeneLab teamed up with DOE-funded initiatives, including the National Microbiome Data Collaborative (NMDC), to create the NASA EDGE [Empowering the Development of Genomics Expertise] Bioinformatics web-based platform. NASA EDGE utilizes shared compute resources to run the GeneLab standardized bioinformatics workflows, which eliminates the need for researchers to have their own high performance computing cluster. The web-based platform makes complicated biological analyses incredibly easy to perform, thus expanding the reach of these analyses to bioinformatics novices, students, and even citizen scientists enabling them to contribute to scientific discoveries and progress. The authors will demonstrate how the NASA EDGE platform can be used to process microbial omics data hosted on OSDR as well as user-generated omics datasets using GeneLab’s standard workflows.

Amanda M. Saravia-Butler↗

BETO 2021 Peer Review - Analytical Development and Standardization for Biomass-Derived Thermochemical Liquids

This project began in FY14 to address the lack of standard chemical characterization analytical methods for bio-oils. Bio-oils are very complex and present numerous analytical challenges; yet reliable chemical information (quantification of both individual compounds and chemical functional groups) is needed to inform upgrading research and refinery co-processing. In this project, analysis needs are first determined from engaging the bioenergy community. Next, standard methods are developed to meet these needs, and then subsequently validated via inter-laboratory studies. Methods that are successfully validated (< 10% variability) are then shared as Laboratory Analytical Procedures (LAPs), which are free and publicly available. We have been tracking LAP use and have seen sustained usage as evidenced by an average of 500 pages views and 100 downloads per quarter, demonstrating the value of these methods to the bioenergy community. LAP methods that are particularly useful and reliable will be chosen for the next-level of standardization through ASTM. We have recently achieved approval by ASTM for our carbonyl titration method. This method (ASTM E3146) is the first example of an ASTM standard solely focused on the chemical characterization of bio-oils. Work in this project is meeting the analysis needs of the bioenergy community and will ultimately help enable the commoditization of bio-oils.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

Standard Analytical Methods for Pyrolysis Bio-Oils

There has been significant recent interest in the production of renewable fuels and chemicals from biomass and waste feedstocks. Pyrolysis pathways produce a liquid bio-oil product, which must be processed further, or upgraded, to yield fuel or chemical products. Bio-oils are very complex and often unstable samples, and research and development on upgrading processes needs reliable analytical information. In particular, chemical characterization techniques are needed to quantify both functional groups and individual compounds present in bio-oils. Reliable analytics are also needed to enable the bioenergy industry, as industrial facilities often have different analytical needs and capabilities than research facilities. In this presentation, we will discuss the development of a suite of standard analytical methods for pyrolysis bio-oils. Analytical methods to be discussed include: Determination of Carbon, Hydrogen, Nitrogen, and Oxygen in bio-oils; Accelerated Aging of Fast Pyrolysis Bio-oil using Carbonyl Titration; Determination of Water Content in Bio-oils by Volumetric Karl Fischer Titration; Determination of Carbon Functional Groups; Elemental Analysis of Bio-oils by Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES) - Na, K, Mg, Ca, S, P, and Fe; Determination of Phenolic Groups in Bio-oils using Revised Folin-Ciocalteu Methods: Single Cuvette and Plate Reader; Corrosivity of Bio-oils: Screening Test using Metal Leaching; Determination of Biogenic Content by 14C Measurement using Liquid Scintillation Counter. These new analytical methods are publicly available as Laboratory Analytical Procedures (https://www.nrel.gov/bioenergy/bio-oil-analysis.html), along with previously developed standard methods: GC-MS, Acid Titration, Carbonyl Titration, and 31P NMR. Additionally, the development of diffusion ordered NMR for characterization of bio-oil molecular weight will be discussed. Collectively, this suite of analytical methods represents the most comprehensive set of standard methods available for pyrolysis bio-oils. These standard methods are commonly used by the bioenergy community, and provide reliable information that enables research, scaleup, and industrial processing of biomass to produce renewable fuels and chemicals.

analytical↗

Methods of making proteins with non-standard amino acids

The disclosure provides methods of making a protein having a desired non-standard amino acid incorporated at its N-terminus in a cell and methods of screening for an amino acyl tRNA synthetase variant that preferentially selects a non-standard amino acid against its standard amino acid counterpart or undesired non-standard amino acids for incorporation into a protein in a cell.

Kunjapur, Aditya Mohan↗

Standards Quick Guide

This report contains a list of relevant standards developed or in development for the cybersecurity of solar energy resources. It outlines different types of standards, such as industry standards, enforceable regulations, and conceptual relevant cybersecurity studies. Users may use this quick guide as a tool to enhance understanding of existing standards and for brainstorming new ideas to help states improve the cybersecurity of solar energy resources in their jurisdiction through innovative policy.

14 SOLAR ENERGY↗

Results of an interlaboratory study on the working curve in vat photopolymerization II: Towards a standardized method

The working curve measurement in photopolymer additive manufacturing is a ubiquitous measure of the cure depth of a printing resin as a function of radiant exposure of light. The fit parameters from this measurement (the depth of light penetration D p and the critical exposure E c ) are used to evaluate and report a resin’s printability, optimize processing parameters, and inform print and resin quality control. Despite its widespread use, the working curve lacks a standard measurement method. Here, following up on our paper “Results of an Interlaboratory Study on the Working Curve in Vat Photopolymerization” from last year, an interlaboratory study on the working curve was performed using calibrated, reproducible, bandpass filtered light sources. With these light sources, the variability between labs in measured working curves was dramatically reduced from the initial interlaboratory study. Aggregate data from this experiment produced reliable D p and E c measurements at 385 nm of 39.2 ± 3.7 µm and 12.3 ± 3.0 mJ cm −2 , respectively. At 405 nm the values of D p and E c are 69.3 ± 3.8 µm and 17.9 ± 2.3 mJ cm −2 , respectively. The results are agnostic to the thickness measurement tool utilized by participants, ensuring broad applicability across laboratories. We also tested the generalizability of the proposed method of using a filtered light source by filtering a commercial 405 nm light source and obtaining a working curve in agreement with the aggregate data from the interlaboratory study. This interlaboratory study provides a basis for a documentary standard for the working curve, so that the entire photopolymer additive manufacturing industry can share reproducible and interoperable working curve data.

36 MATERIALS SCIENCE↗

Constraints on flavor-diagonal non-standard neutrino interactions from Borexino Phase-II

The Borexino detector measures solar neutrino fluxes via neutrino-electron elastic scattering. Observed spectra are determined by the solar-$\nu_{e}$ survival probability $P_{ee}(E)$, and the chiral couplings of the neutrino and electron. Some theories of physics beyond the Standard Model postulate the existence of Non-Standard Interactions (NSI's) which modify the chiral couplings and $P_{ee}(E)$. In this paper, we search for such NSI's, in particularly neutral-current-like interactions that modify the $\nu_e - e$ and $\nu_\tau - e$ couplings, using Borexino Phase II data. Standard Solar Model predictions of the solar neutrino fluxes for both high- and low-metallicity assumptions are considered. No indication of new physics is found at the level of sensitivity of the detector and constraints on the parameters of the NSI's are placed. In addition, with the same dataset the value of $\sin^2\theta_W$ is obtained with a precision comparable to that achieved in reactor antineutrino experiments.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Cost-Effectiveness of ANSI/ASHRAE/IES Standard 90.1-2019 for Alabama

This report describes the methodology and results of a state cost-effectiveness analysis of ASHRAE Standard 90.1-2019. Moving to the Standard 90.1-2019 edition from Standard 90.1-2016 is found to be cost-effective for the state. Annual energy cost savings, added construction costs, and life-cycle costs are all described and presented here for various building types and climate zones.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

Cybersecurity Standards for Distributed Energy Resources: Gaps and Harmonization Strategy

This report examines cybersecurity standards for Distributed Energy Resources (DERs) in light of their rapid growth and increasing integration into energy systems. It identifies critical gaps in existing frameworks, including inadequate coverage of DER-specific challenges, complexities in implementing comprehensive standards, integration issues with legacy systems, adoption hurdles for newer standards, and a lack of harmonization across regulatory landscapes. The analysis highlights vulnerabilities such as data integrity risks, unauthorized device control, and denial-of-service attacks across various DER technologies like solar PV, wind turbines, energy storage systems, and hydrogen fuel cells. The report proposes a harmonization strategy to address these deficiencies by developing unified cybersecurity requirements, certification programs, and training resources while fostering collaboration among stakeholders such as government agencies, industry groups, DER operators, manufacturers, and research institutions. A phased roadmap is outlined to refine and implement these measures through pilot testing and widespread adoption. Ultimately, the report underscores the urgent need for coordinated efforts to enhance DER cybersecurity and ensure the reliable operation of future energy systems.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

A standards perspective on genomic data reusability and reproducibility

Genomic and metagenomic sequence data provides an unprecedented ability to re-examine findings, offering a transformative potential for advancing research, developing computational tools, enhancing clinical applications, and fostering scientific collaboration. However, effective and ethical reuse of genomics data is hampered by numerous technical and social challenges. The International Microbiome and Multi’Omics Standards Alliance (IMMSA, https://www.microbialstandards.org/) and the Genomic Standards Consortium (GSC, https://gensc.org) hosted a 5-part seminar series “A Year of Data Reuse” in 2024 to explore challenges and opportunities of data reuse and reproducibility across disparate domains of the genomic sciences. Addressing these challenges will require a multifaceted approach, including common metadata reporting, clear communication, standardized protocols, improved data management infrastructure, ethical guidelines, and collaborative policies that prioritize transparency and accessibility. We offer strategies to enable responsible and technically feasible data reuse, recognition of data reproducibility challenges, and emphasizing the importance of cross-disciplinary efforts in the pursuit of open science and data-driven innovation.

59 BASIC BIOLOGICAL SCIENCES↗

Sterile neutrinos with non-standard interactions in β- and 0νββ-decay experiments

Charged currents are probed in low-energy precision β -decay experiments and at high-energy colliders, both of which aim to measure or constrain signals of beyond-the-Standard-Model physics. In light of future β -decay and LHC measurements that will further explore these non-standard interactions, we investigate what neutrinoless double- β decay (0 νββ ) experiments can tell us if a nonzero signal were to be found. Using a recently developed effective-field-theory framework, we consider the effects that interactions with right-handed neutrinos have on 0 νββ and discuss the range of neutrino masses that current and future 0 νββ measurements can probe, assuming neutrinos are Majorana particles. For non-standard interactions at the level suggested by recently observed hints in β decays, we show that next-generation 0 νββ experiments can determine the Dirac or Majorana nature of neutrinos, for sterile neutrino masses larger than $\mathcal{O}(10)$ eV.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Importance of Standardizing Analytical Characterization Methodology for Improved Reliability of the Nanomedicine Literature

Understanding the interaction between biological structures and nanoscale technologies, dubbed the nano-bio interface, is required for successful development of safe and efficient nanomedicine products. The lack of a universal reporting system and decentralized methodologies for nanomaterial characterization have resulted in a low degree of reliability and reproducibility in the nanomedicine literature. As such, there is a strong need to establish a characterization system to support the reproducibility of nanoscience data particularly for studies seeking clinical translation. Here, we discuss the existing key standards for addressing robust characterization of nanomaterials based on their intended use in medical devices or as pharmaceuticals. We also discuss the challenges surrounding implementation of such standard protocols and their implication for translation of nanotechnology into clinical practice. We, however, emphasize that practical implementation of standard protocols in experimental laboratories requires long-term planning through integration of stakeholders including institutions and funding agencies.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

Multi-lab study on the pure-gas permeation of commercial polysulfone (PSf) membranes: Measurement standards and best practices

Gas-separation membranes are a critical industrial component for a low-carbon and energy-efficient future. As a result, many researchers have been testing membrane materials over the past several decades. Unfortunately, almost all membrane-based testing systems are home-built, and there are no widely accepted material standards or testing protocols in the literature, making it challenging to accurately compare experimental results. Further, in this multi-lab study, ten independent laboratories collected high-pressure pure-gas permeation data for H 2 , O 2 , CH 4 , and N 2 in commercial polysulfone (PSf) films. Equipment information, testing procedures, and permeation data from all labs were collected to provide (1) accepted H 2 , O 2 , CH 4 , and N 2 permeability values at 35°C in PSf as a reference standard, (2) statistical analysis of lab-to-lab uncertainties in evaluating permeability, and (3) a list of best practices for sample preparation, equipment set-up, and permeation testing using constant-volume variable-pressure apparatuses. Results summarized in this work provide a reference standard and recommended testing protocols for pure-gas testing of membrane materials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

A standard capsule design for structural material testing in the Advanced Test Reactor

Nuclear materials testing is commonly completed in various material test and research reactors throughout the world, including the Advanced Test Reactor (ATR), but the current capsule design, analysis, and fabrication process can take years to complete. To decrease the costs and time associated with materials testing, a standard capsule has been designed which houses various specimen geometries and allows irradiation in virtually any ATR test position. The standard capsule features locking end caps which connect and lock together to form the capsule stack, eliminating the need for a basket and maximizing the quantity of specimens which are contained within the capsule. A customizable internal gas gap provides thermal resistance between the specimens and reactor coolant, making specimen temperatures from approximately 370 to 1000 K achievable. The flexibility of the capsule design allows experimenters to choose irradiation positions based off desired neutron flux, with typical fluences per cycle ranging from 8.8x10 19 to 2.3x10 21 n/cm 2 , depending on experiment position. Here this paper presents and discusses the standard capsule design and analysis.

36 MATERIALS SCIENCE↗