Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “Laboratory experiments”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 433 records · Page 24

Persistent mysteries of jet engines, formation, propagation, and particle acceleration: Have they been addressed experimentally?

Here, the physics of astrophysical jets can be divided into three regimes: (i) engine and launch (ii) propagation and collimation, (iii) dissipation and particle acceleration. Since astrophysical jets comprise a huge range of scales and phenomena, practicality dictates that most studies of jets intentionally or inadvertently focus on one of these regimes, and even therein, one body of work may be simply boundary condition for another. We first discuss long standing persistent mysteries that pertain the physics of each of these regimes, independent of the method used to study them. This discussion makes contact with frontiers of plasma astrophysics more generally. While observations theory, and simulations, and have long been the main tools of the trade, what about laboratory experiments? Jet related experiments have offered controlled studies of specific principles, physical processes, and benchmarks for numerical and theoretical calculations. We discuss what has been accomplished on these fronts. Although experiments have indeed helped us to understand certain processes, proof of principle concepts, and benchmarked codes, they have yet to solved an astrophysical jet mystery on their own. A challenge is that experimental tools used for jet-related experiments so far, are typically not machines originally designed for that purpose, or designed with specific astrophysical mysteries in mind. This presents an opportunity for a different way of thinking about the development of future platforms: start with the astrophysical mystery and build an experiment to address it.

79 ASTRONOMY AND ASTROPHYSICS↗

Vision in space travel

Laboratory experiments and Voskhod flight data on vision sharpness, efficiency, and perception during space flights

VISION↗

Laboratory and field observations of the growth of columnar and plate crystals from frozen droplets

A laboratory experiment was initiated to grow the banded columnar crystals found in cirrus clouds and to determine if they nucleated through a freezing nucleus. Banded columnar crystals were collected in cirrus clouds and also grown in a laboratory cold box over a temperature range of -20 to -46C. They were observed to grow from a frozen droplet through several distinct crystalline transitions. The first distinct crystalline form observed following the growth of a frozen droplet was a polyhedral crystal. With further growth, the polyhedral crystal developed end plates, and it appeared to be a 'double plate.' Then the separation between the plates nearly filled in to leave the characteristic band. Certain columns (-6 to -10C) and plates (-10 to -20C) were also observed to grow from a frozen droplet and showed similar crystalline transitions.

Heymsfield, A. J.↗

Some final conclusions and supporting experiments related to the search for organic compounds on the surface of Mars

The Viking molecular analysis experiment has demonstrated the absence (within the detection limits which range from levels of parts per million to below parts per billion) of organic substances in the Martian surface soil at the two Viking landing sites. Laboratory experiments with sterile and nonsterile antarctic samples further demonstrate the capability and reliability of the instrument. The circumstances under which organic components could have escaped detection, such as inaccessibility or extreme thermal stability of organic polymers, are discussed but are found to be unlikely. The inability of the instrument to detect free oxygen evolved from soil samples is pointed out.

Biemann, K.↗

Evaluation of Instability Phenomena in Sands: Plane Strain Versus Triaxial Conditions

Extensive research was carried out in the 1950s on theories of plasticity to extend the concepts developed for metals to materials that failed according to the Mohr-Coulomb criterion. The new ideas made it possible to merge the two distinct concepts (strength and deformation techniques) into one that relies on better understanding of plasticity and resulted in a rapid growth in the field of constitutive modeling of soil behavior. At the same time advanced experimental apparatuses and laboratory procedures were developed to calibrate the models. However, most laboratory experiments on granular materials are performed under Conventional Triaxial Conditions (CTC) for the purposes of evaluating constitutive behavior and stability properties, whereas most geotechnical field problems are closer to the Plane Strain (PS) condition. The triaxial tests performed in most laboratories comprise a simplification over in situ states and allow easier and robust experimentation. Most landslide problems, failure of soils beneath shallow and deep foundations, and failure of retaining structures, are cases that can generally be considered as plane strain. Strength and deformation characteristics of granular materials loaded in plane strain may be considerably different from those observed in CTC. Most studies on sands were limited to evaluating the constitutive behavior and in some cases extended to briefly describing the associated instability phenomena. This paper presents the results of a series of PS and CTC experiments performed on fine uniform silica sand known as F-75 Ottawa sand. Advanced analysis techniques were used to study the instability phenomena, which yielded very accurate measurements of shear bands occurrences and patterns. Destructive thin-sectioning technique along with monitoring the specimen surface deformation was used in the PS experiments and Computed Tomography (CT) was used to investigate the progress of primary and secondary shear bands in specimens subjected to CTC. Comparison between the two cases will be presented and discussed.

Alshibli, Khalid A.↗

Convection in a Very Compressible Fluid: Comparison of Simulations With Experiments

The time profile (Delta)T(t) of the temperature difference, measured across a very compressible fluid layer of supercritical He-3 after the start of a heat flow, shows a damped oscillatory behavior before steady state convection is reached. The results for (Delta)T(t) obtained from numerical simulations and from laboratory experiments are compared over a temperature range where the compressibility varies by a factor of approx. = 40. First the steady-state convective heat current j(sup conv) as a function of the Rayleigh number R(alpha) is presented, and the agreement is found to be good. Second, the shape of the time profile and two characteristic times in the transient part of (Delta)T(t) from simulations and experiments are compared, namely: 1) t(sub osc), the oscillatory period and 2) t(sub p), the time of the first peak after starting the heat flow. These times, scaled by the diffusive time tau(sub D) versus R(alpha), are presented. The agreement is good for t(sup osc)/tau(sub D), where the results collapse on a single curve showing a powerlaw behavior. The simulation hence confirms the universal scaling behavior found experimentally. However for t(sub p)/tau(sub D), where the experimental data also collapse on a single curve, the simulation results show systematic departures from such a behavior. A possible reason for some of the disagreements, both in the time profile and in t(sub p) is discussed. In the Appendix a third characteristic time, t(sub m), between the first peak and the first oscillation minimum is plotted and a comparison between the results of experiments and simulations is made.

Meyer, H.↗

Interstellar PAH Analogs in the Laboratory: Comparison with Astronomical Data

Polycyclic Aromatic Hydrocarbons (PAHs) are an important and ubiquitous component of carbon-bearing materials in space. PAHs are the best-known candidates to account for the IR emission bands (UIR bands) and PAH spectral features are now being used as new probes of the ISM. PAHs are also thought to be among the carriers of the diffuse interstellar absorption bands (DIBs). In the model dealing with the interstellar spectral features, PAHs are present as a mixture of radicals, ions and neutral species. PAH ionization states reflect the ionization balance of the medium while PAH size, composition, and structure reflect the energetic and chemical history of the medium. A major challenge for laboratory astrophysics is to reproduce (in a realistic way) the physical conditions that exist in the emission and/or absorption interstellar zones. An extensive laboratory program has been developed at NASA Ames to assess the physical and chemical properties of PAHs in such environments and to describe how they influence the radiation and energy balance in space and the interstellar chemistry. In particular, laboratory experiments provide measurements of the spectral characteristics of interstellar PAH analogs from the ultraviolet and visible range to the infrared range for comparison with astronomical data. This paper will focus on the recent progress made in the laboratory to measure the direct absorption spectra of neutral and ionized PAHs in the near-UV and visible range. Intrinsic band profiles and band positions of cold gas-phase PAHs can now be measured with high-sensitivity spectroscopy and directly compared to the astronomical data. Preliminary conclusions from the comparison of the laboratory data with astronomical observations will also be presented.

Salama, Farid↗

Major Scientific Challenges and Opportunities in Understanding Magnetic Reconnection and Related Explosive Phenomena in Heliophysics and Beyond

Magnetic reconnection underlies many explosive phenomena in the heliosphere and in laboratory plasmas. New research capabilities in theory/simulations, observations, and laboratory experiments provide the opportunity to solve the grand scientific challenges summarized in this white paper. Success will require enhanced and sustained investments from relevant funding agencies, increased interagency/international partnerships, and close collaborations among the heliophysics, astrophysics, and laboratory plasma communities. These investments will deliver transformative progress in understanding magnetic reconnection and related explosive phenomena including space weather events.

H. Ji↗

Electrostatic fields in a dusty Martian environment

While there have been several studies suggesting the possibility of electrical activity on Mars, to date there have been no measurements to search for evidence of such activity. In the absence of widespread water clouds and convective storm systems similar to those on the Earth and Jupiter, the most likely candidate for the creation of electrostatic charges and fields is triboelectric charging of dust, i.e., the friction between blown dust and the ground, and of dust particles with each other. Terrestrial experience demonstrates that electric fields 5 to 15 kV-m(exp -1) are not uncommon in dust storms and dust devils in desert regions, where the polarity varies according to the chemical composition and grain size. Simple laboratory experiments have demonstrated that modest electrostatic fields of roughly 5,000 V-m(exp -1) may be produced, along with electrical spark discharges and glow discharges, in a simulation of a dusty, turbulent Martian surface environment. While the Viking landers operated for several years with no apparent deleterious effects from electrostatic charging, this may have been at least partly due to good engineering design utilizing pre-1976 electronic circuitry to minimize the possibility of differential charging among the various system components. However, free roaming rovers, astronauts, and airborne probes may conceivably encounter an environment where electrostatic charging is a frequent occurrence, either by way of induction from a static electric field or friction with the dusty surface and atmosphere. This raises the possibility of spark discharges or current surges when subsequent contact is made with other pieces of electrical equipment, and the possibility of damage to modern microelectronic circuitry. Measurements of electrostatic fields on the surface of Mars could therefore be valuable for assessing this danger. Electric field measurements could also be useful for detecting natural discharges that originate in dust storms. This detection could be performed at distances ranging from 10s of km in the case of J-charge-like discharge signatures, to planetary distances if there exists a global electrical circuit or Schumann resonance spectrum.

Sentman, D. D.↗

A study of single and binary ion plasma expansion into laboratory-generated plasma wakes

Plasma expansion into the wake of a large rectangular plate immersed in a collisionless, supersonic plasma was investigated in laboratory experiments. The experimental conditions address both single ion and binary ion plasma flows for the case of a body whose size is large in comparison with the Debye length, when the potential difference between the body and the plasma is relatively small. A new plasma source was developed to generate equi-velocity, binary ion plasma flows, which allows access to new parameter space that have previously been unavailable for laboratory studies. Specifically, the new parameters are the ionic mass ratio and the ionic component density ratio. In a series of experiments, a krypton-neon plasma is employed where the ambient density ratio of neon to krypton is varied more than an order of magnitude. The expansion in both the single ion and binary ion plasma cases is limited to early times, i.e., a few ion plasma periods, by the combination of plasma density, plasma drift speed, and vacuum chamber size, which prevented detailed comparison with self-similar theory.

Wright, Kenneth Herbert, Jr.↗

The chemistry of phosphorus in dense interstellar clouds

Laboratory experiments show that the ion-molecule chemistry of phosphorus is significantly different from that of nitrogen in dense interstellar clouds. The PH3 molecule is not readily formed by gas-phase, ion-molecule reactions in these regions. Laboratory results used in a simple kinetic model indicate that the most abundant molecule containing phosphorus in dense clouds is PO.

Thorne, L. R.↗

Fluid management technology: Liquid slosh dynamics and control

Flight experiments were defined for the Cryogenic On-Orbit Liquid Depot Storage, Acquisition and Transfer Satellite (COLD-SAT) test bed satellite and the Shuttle middeck to help establish the influence of the gravitational environment on liquid slosh dynamics and control. Several analytical and experimental studies were also conducted to support the experiments and to help understand the anticipated results. Both FLOW-3D and NASA-VOF3D computer codes were utilized to simulate low Bond number, small amplitude sloshing, for which the motions are dominated by surface forces; it was found that neither code provided a satisfactory simulation. Thus, a new analysis of low Bond number sloshing was formulated, using an integral minimization technique that will allow the assumptions made about surface physics phenomena to be modified easily when better knowledge becomes available from flight experiments. Several examples were computed by the innovative use of a finite-element structural code. An existing spherical-pendulum analogy of nonlinear, rotary sloshing was also modified for easier use and extended to low-gravity conditions. Laboratory experiments were conducted to determine the requirements for liquid-vapor interface sensors as a method of resolving liquid surface motions in flight experiments. The feasibility of measuring the small slosh forces anticipated in flight experiments was also investigated.

Dodge, Franklin T.↗

Scattering Models and Basic Experiments in the Microwave Regime

The objectives of research over the next three years are: (1) to develop a randomly rough surface scattering model which is applicable over the entire frequency band; (2) to develop a computer simulation method and algorithm to simulate scattering from known randomly rough surfaces, Z(x,y); (3) to design and perform laboratory experiments to study geometric and physical target parameters of an inhomogeneous layer; (4) to develop scattering models for an inhomogeneous layer which accounts for near field interaction and multiple scattering in both the coherent and the incoherent scattering components; and (5) a comparison between theoretical models and measurements or numerical simulation.

Fung, A. K.↗

Investigations of the Formation of Carbon Grains in Circumstellar Outflows

The study of formation and destruction processes of cosmic dust is essential to understand and to quantify the budget of extraterrestrial organic molecules. Although dust with all its components plays an important role in the evolution of interstellar chemistry and in the formation of organic molecules, little is known on the formation and destruction processes of carbonaceous dust. PAHs are important chemical building blocks of interstellar dust. They are detected in interplanetary dust particles and in meteoritic samples. Additionally, observational, laboratory, and theoretical studies have shown that PAHs, in their neutral and ionized forms, are an important, ubiquitous component of the interstellar medium. Also, the formation of PAHs from smaller molecules has not been extensively studied. Therefore, it is imperative that laboratory experiments be conducted to study the dynamic processes of carbon grain formation from PAH precursors. Studies of interstellar dust analogs formed from a variety of PAH and hydrocarbon precursors as well as species that include the atoms O, N, and S, have recently been performed in our laboratory under conditions that simulate interstellar and circumstellar environments. The species formed in the pulsed discharge nozzle (PDN) plasma source are detected and characterized with a high-sensitivity cavity ringdown spectrometer (CRDS) coupled to a Reflectron time-of-flight mass spectrometer (ReTOF-MS), thus providing both spectroscopic and ion mass information in-situ. We report the first set of measurements obtained in these experiments and identify the species present in the experiments and the ions that are formed in the plasma process. From these unique measurements, we derive information on the size and the structure of interstellar dust grain particles, the growth and the destruction processes of interstellar dust and the resulting budget of extraterrestrial organic molecules.

Grains↗

Evaluation of Nuclear Spent Fuel Disposal in Clay-Bearing Rock - Process Model Development and Experimental Studies (M2SF-21SN010301072)

The DOE R&D program under the Spent Fuel Waste Science Technology (SFWST) campaign has made key progress in modeling and experimental approaches towards the characterization of chemical and physical phenomena that could impact the long-term safety assessment of heatgenerating nuclear waste disposition in deep-seated clay/shale/argillaceous rock. International collaboration activities such as heater tests, continuous field data monitoring, and postmortem analysis of samples recovered from these have elucidated key information regarding changes in the engineered barrier system (EBS) material exposed to years of thermal loads. Chemical and structural analyses of sampled bentonite material from such tests as well as experiments conducted on these are key to the characterization of thermal effects affecting bentonite clay barrier performance and the extent of sacrificial zones in the EBS during the thermal period. Thermal, hydrologic, and chemical data collected from heater tests and laboratory experiments has been used in the development, validation, and calibration of THMC simulators to model near-field coupled processes. This information leads to the development of simulation approaches (e.g., continuum and discrete) to tackle issues related to flow and transport at various scales of the host-rock, its interactions with barrier materials, and EBS design concept.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

The materials processing sciences glovebox

The Materials Processing Sciences Glovebox is a rack mounted workstation which allows on orbit sample preparation and characterization of specimens from various experiment facilities. It provides an isolated safe, clean, and sterile environment for the crew member to work with potentially hazardous materials. It has to handle a range of chemicals broader than even PMMS. The theme is that the Space Station Laboratory experiment preparation and characterization operations provide the fundamental glovebox design characteristics. Glovebox subsystem concepts and how internal material handling operations affect the design are discussed.

Traweek, Larry↗

Raman spectroscopy coupled with ambient ionization mass spectrometry: A forensic laboratory investigation into rapid and simple dual instrumental analysis techniques

We present a laboratory experiment, developed around a pair of instrumental analysis techniques, Raman spectroscopy and ambient ionization mass spectrometry (MS), conducted by senior chemistry undergraduate students for bulk analysis of over-the-counter drugs using benchtop versions of the two instruments, as well as trace analysis of illicit drugs utilizing the corresponding portable instruments. The identification and confirmation of seized drugs is a routine operation in forensic laboratories that can be simplified using these two instrumental techniques in tandem. Bulk samples are readily analyzed using conventional Raman spectroscopy followed by paper cone spray ionization (PCSI) MS, while trace analysis is allowed by a simple single-substrate dual-analyzer method using surface enhanced Raman spectroscopy (SERS) from paper followed by paper spray ionization (PSI) MS. The introduction of these novel strategies to the students exposed them to potential career paths in forensic science by means of a hands-on experience that provided fundamental knowledge about this set of analytical methods, including intercomparisons of their performance, as well as practical issues like costs, regulations and databases. The use of portable instrumentation represents an additional learning experience for the students, considering that it is cutting-edge technology that is just now being transferred from academic to industrial labs and that it allows a valuable discussion of the advantages and disadvantages of bringing the laboratory to the field.

47 OTHER INSTRUMENTATION↗

Astrochemistry: Recent Advances in the Study of Carbon Molecules in Space

Carbon molecules and ions play an important role in space. Polycyclic Aromatic Hydrocarbons (PAHs) are the best-known candidates to account for the infrared emission bands (UIR bands) and PAH spectral features are now being used as probes of the interstellar medium in Galactic and extra-galactic environments. PAHs are also thought to be among the carriers of the diffuse interstellar absorption bands (DIBs). In the model dealing with the interstellar spectral features, PAHs are present as a mixture of radicals, ions and neutral species. PAH ionization states reflect the ionization balance of the medium while PAH size, composition, and structure reflect the energetic and chemical history of the medium. A major challenge for laboratory Astrochemistry is to reproduce (in a realistic way) the physical conditions that exist in the emission and absorption interstellar zones. An extensive laboratory program has been developed in various laboratories to characterize the physical and chemical properties of PAHs in astrophysical environments and to describe how they influence the radiation and energy balance in space and the interstellar chemistry. In particular, laboratory experiments provide measurements of the spectral characteristics of interstellar PAH analogs from the ultraviolet and visible range to the infrared range for comparison with astronomical data. The harsh physical conditions of the interstellar medium - characterized by a low temperature, an absence of collisions and strong ultraviolet radiation fields - are simulated in the laboratory by associating a molecular beam with an ionizing discharge to generate a cold plasma expansion. PAH ions are formed from the neutral precursors in an isolated environment at low temperature (of the order of 100 K). The spectra of neutral and ionized PAHs are measured using the high sensitivity methods of cavity ring down spectroscopy (CRDS). These experiments provide unique information on the spectra of free, cold large carbon molecules and ions in the gas phase.

Salama, Farid↗