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At least 433 records · Page 24

Hyperspectral Raman imaging using a spatial heterodyne spectrometer (SHS)

Savannah River National Laboratory, and the larger community, has limited chemical-specific imaging capabilities, which would be beneficial for remote detection of threat chemicals or use in inaccessible and harsh environments, as well as in-line process monitoring. Chemical imaging technology would support multiple directorates through stand-off detection of chemicals (National Security), and imaging of chemical distributions in a process (Nuclear Materials Management, Clean Energy) and in waste tanks (Environmental Stewardship). Chemical-specific imaging is underdeveloped due to issues of sensitivity, stable alignment and calibration, and ease of operation associated with most optical instruments. The project objective is to develop a novel, rugged, highly sensitive spectrometer to support real-time, chemically specific imaging using hyperspectral Raman spectroscopy. Raman spectroscopic analysis will provide chemical specificity and using a spatial heterodyne spectrometer (SHS) will increase the sensitivity due to the high light throughput design. The SHS design does not require moving parts allowing for a very stable system, reducing alignment and calibration issues. The instrument will be assembled and initially applied to Raman gas detection of the Saltstone disposal unit headspace gas concentrations. Raman gas analysis is the most impacted by sensitivity issues and will be used to demonstrate the increased light collection capability of the SHS over a conventional dispersive spectrometer. The system will be later modified to image spectral information in a spatial domain to provide information on the spatial distribution of a sample scene.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Breadboard linear array scan imager using LSI solid-state technology

The performance of large scale integration photodiode arrays in a linear array scan (pushbroom) breadboard was evaluated for application to multispectral remote sensing of the earth's resources. The technical approach, implementation, and test results of the program are described. Several self scanned linear array visible photodetector focal plane arrays were fabricated and evaluated in an optical bench configuration. A 1728-detector array operating in four bands (0.5 - 1.1 micrometer) was evaluated for noise, spectral response, dynamic range, crosstalk, MTF, noise equivalent irradiance, linearity, and image quality. Other results include image artifact data, temporal characteristics, radiometric accuracy, calibration experience, chip alignment, and array fabrication experience. Special studies and experimentation were included in long array fabrication and real-time image processing for low-cost ground stations, including the use of computer image processing. High quality images were produced and all objectives of the program were attained.

Tracy, R. A.↗

A block matching-based registration algorithm for localization of locally advanced lung tumors

Purpose: To implement and evaluate a block matching-based registration (BMR) algorithm for locally advanced lung tumor localization during image-guided radiotherapy. Methods: Small (1 cm{sup 3}), nonoverlapping image subvolumes (“blocks”) were automatically identified on the planning image to cover the tumor surface using a measure of the local intensity gradient. Blocks were independently and automatically registered to the on-treatment image using a rigid transform. To improve speed and robustness, registrations were performed iteratively from coarse to fine image resolution. At each resolution, all block displacements having a near-maximum similarity score were stored. From this list, a single displacement vector for each block was iteratively selected which maximized the consistency of displacement vectors across immediately neighboring blocks. These selected displacements were regularized using a median filter before proceeding to registrations at finer image resolutions. After evaluating all image resolutions, the global rigid transform of the on-treatment image was computed using a Procrustes analysis, providing the couch shift for patient setup correction. This algorithm was evaluated for 18 locally advanced lung cancer patients, each with 4–7 weekly on-treatment computed tomography scans having physician-delineated gross tumor volumes. Volume overlap (VO) and border displacement errors (BDE) were calculated relative to the nominal physician-identified targets to establish residual error after registration. Results: Implementation of multiresolution registration improved block matching accuracy by 39% compared to registration using only the full resolution images. By also considering multiple potential displacements per block, initial errors were reduced by 65%. Using the final implementation of the BMR algorithm, VO was significantly improved from 77% ± 21% (range: 0%–100%) in the initial bony alignment to 91% ± 8% (range: 56%–100%;p < 0.001). Left-right, anterior-posterior, and superior-inferior systematic BDE were 3.2, 2.4, and 4.4 mm, respectively, with random BDE of 2.4, 2.1, and 2.7 mm. Margins required to include both localization and delineation uncertainties ranged from 5.0 to 11.7 mm, an average of 40% less than required for bony alignment. Conclusions: BMR is a promising approach for automatic lung tumor localization. Further evaluation is warranted to assess the accuracy and robustness of BMR against other potential localization strategies.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

NASA Tech Briefs, December 2012

The topics include: Pattern Generator for Bench Test of Digital Boards; 670-GHz Down- and Up-Converting HEMT-Based Mixers; Lidar Electro-Optic Beam Switch with a Liquid Crystal Variable Retarder; Feedback Augmented Sub-Ranging (FASR) Quantizer; Real-Time Distributed Embedded Oscillator Operating Frequency Monitoring; Software Modules for the Proximity-1 Space Link Interleaved Time Synchronization (PITS) Protocol; Description and User Instructions for the Quaternion to Orbit v3 Software; AdapChem; Mars Relay Lander and Orbiter Overflight Profile Estimation; Extended Testability Analysis Tool; Interactive 3D Mars Visualization; Rapid Diagnostics of Onboard Sequences; MER Telemetry Processor; pyam: Python Implementation of YaM; Process for Patterning Indium for Bump Bonding; Archway for Radiation and Micrometeorite Occurrence Resistance; 4D Light Field Imaging System Using Programmable Aperture; Device and Container for Reheating and Sterilization; Radio Frequency Plasma Discharge Lamps for Use as Stable Calibration Light Sources; Membrane Shell Reflector Segment Antenna; High-Speed Transport of Fluid Drops and Solid Particles via Surface Acoustic Waves; Compact Autonomous Hemispheric Vision System; A Distributive, Non-Destructive, Real-Time Approach to Snowpack Monitoring; Wideband Single-Crystal Transducer for Bone Characterization; Numerical Simulation of Rocket Exhaust Interaction With Lunar Soil; Motion Imagery and Robotics Application (MIRA): Standards-Based Robotics; Particle Filtering for Model-Based Anomaly Detection in Sensor Networks; Ka-band Digitally Beamformed Airborne Radar Using SweepSAR Technique; Composite With In Situ Plenums; Multi-Beam Approach for Accelerating Alignment and Calibration of HyspIRI-Like Imaging Spectrometers; JWST Lifting System; Next-Generation Tumbleweed Rover; Pneumatic System for Concentration of Micrometer-Size Lunar Soil.

Source record↗

Spot size measurement of a deuterium–tritium dense plasma focus using neutron radiography

Neutron radiography is a technique uniquely suited to applications in nuclear diagnostics, non-destructive testing, and subcritical experiments. The spatial resolution of neutron radiographs is degraded by optical blur in the imaging system and the neutron source size, where the ideal source is point-like to optimize the point-spread function. A potential neutron source for radiography is the dense plasma focus (DPF), a coaxial Z-pinch that produces thermonuclear and beam-target neutrons. To assess if the source size is suitable for radiography, a neutron imaging system was used to measure the source size of the 4 MA Sodium DPF at the Nevada National Security Site operating with deuterium–tritium gas-fill. The source size was measured using the edge-spread function of tungsten objects, each having a rolled (convex) edge. The spot size was found to be 7–12 mm full-width at half-max (FWHM) assuming a Gaussian source, though comparison is presented for Lorentzian and Bennett distributions. The average FWHM was found to be 8.6 ± 1.2 mm vertically and 10.8 ± 1.2 mm horizontally with respect to the image plane, averaging over varied edges and alignments. The results were sensitive to source alignment and edge metrology, which introduced notable uncertainties. These results are consistent with separate experimental measurements as well as magnetohydrodynamics simulations of this DPF, which suggest that neutron production can originate from pinches ∼5–7 mm off-axis. These results suggest that the DPF should be used for radiography at low magnification (M < 1) where spot size does not dominate spatial blur.

47 OTHER INSTRUMENTATION↗

Integrated filter and detector array for spectral imaging

A spectral imaging system having an integrated filter and photodetector array is disclosed. The filter has narrow transmission bands which vary in frequency along the photodetector array. The frequency variation of the transmission bands is matched to, and aligned with, the frequency variation of a received spectral image. The filter is deposited directly on the photodetector array by a low temperature deposition process. By depositing the filter directly on the photodetector array, permanent alignment is achieved for all temperatures, spectral crosstalk is substantially eliminated, and a high signal to noise ratio is achieved.

Labaw, Clayton C.↗

SU-F-T-258: Efficacy of Exit Fluence-Based Dose Calculation for Prostate Radiation Therapy

Purpose: To investigate the efficacy of exit-fluence-based dose computation for prostate radiotherapy by determining if it estimates true dose more accurately than the original planning dose. Methods: Virtual exit-fluencebased dose computation was performed for 19 patients, each with 9–12 repeat CT images. For each patient, a 78 Gy treatment plan was created utilizing 5 mm CTV-to-PTV and OAR-to-PRV margins. A Monte Carlo framework was used to compute dose and exit-fluence images for the planning image and for each repeat CT image based on boney-anatomyaligned and prostate-centroid-aligned CTs. Identical source particles were used for the MC dose-computations on the planning and repeat CTs to maximize correlation. The exit-fluence-based dose and image were computed by multiplying source particle weights by FC(x,y)=FP(x,y)/FT(x,y), where (x,y) are the source particle coordinates projected to the exit-fluence plane and we denote the dose/fluence from the plan by (DP,FP), from the repeat-CT as (DT,FT), and the exit-fluence computation by (DFC,FFC). DFC mimics exit-fluence backprojection through the planning image as FT=FFC. Dose estimates were intercompared to judge the efficacy of exit-fluence-based dose computation. Results: Boney- and prostate-centroid aligned results are combined as there is no statistical difference between them, yielding 420 dose comparisons per dose-volume metric. DFC is more accurate than DP for 46%, 33%, and 44% of cases in estimating CTV D98, D50, and D2 respectively. DFC improved rectum D50 and D2 estimates 54% and 49% respectively and bladder D50 and D2 47 and 49% respectively. While averaged over all patients and images DFC and DP were within 3.1% of DT, they differed from DT by as much as 22% for GTV D98, 71% for the Bladder D50, 17% for Bladder D2, 19% for Rectum D2. Conclusion: Exit-fluence based dose computations infrequently improve CTV or OAR dose estimates and should be used with caution. Research supported in part by Varian Medical Systems.

60 APPLIED LIFE SCIENCES↗

Spacecraft Alignment Determination and Control for Dual Spacecraft Precision Formation Flying

Many proposed formation flying missions seek to advance the state of the art in spacecraft science imaging by utilizing precision dual spacecraft formation flying to enable a virtual space telescope. Using precision dual spacecraft alignment, very long focal lengths can be achieved by locating the optics on one spacecraft and the detector on the other. Proposed science missions include astrophysics concepts with spacecraft separations from 1000 km to 25,000 km, such as the Milli-Arc-Second Structure Imager (MASSIM) and the New Worlds Observer, and Heliophysics concepts for solar coronagraphs and X-ray imaging with smaller separations (50m 500m). All of these proposed missions require advances in guidance, navigation, and control (GNC) for precision formation flying. In particular, very precise astrometric alignment control and estimation is required for precise inertial pointing of the virtual space telescope to enable science imaging orders of magnitude better than can be achieved with conventional single spacecraft instruments. This work develops design architectures, algorithms, and performance analysis of proposed GNC systems for precision dual spacecraft astrometric alignment. These systems employ a variety of GNC sensors and actuators, including laser-based alignment and ranging systems, optical imaging sensors (e.g. guide star telescope), inertial measurement units (IMU), as well as micro-thruster and precision stabilized platforms. A comprehensive GNC performance analysis is given for Heliophysics dual spacecraft PFF imaging mission concept.

Formation flying↗

Spacecraft Alignment Determination and Control for Dual Spacecraft Precision Formation Flying

Many proposed formation flying missions seek to advance the state of the art in spacecraft science imaging by utilizing precision dual spacecraft formation flying to enable a virtual space telescope. Using precision dual spacecraft alignment, very long focal lengths can be achieved by locating the optics on one spacecraft and the detector on the other. Proposed science missions include astrophysics concepts with spacecraft separations from 1000 km to 25,000 km, such as the Milli-Arc-Second Structure Imager (MASSIM) and the New Worlds Observer, and Heliophysics concepts for solar coronagraphs and X-ray imaging with smaller separations (50m-500m). All of these proposed missions require advances in guidance, navigation, and control (GNC) for precision formation flying. In particular, very precise astrometric alignment control and estimation is required for precise inertial pointing of the virtual space telescope to enable science imaging orders of magnitude better than can be achieved with conventional single spacecraft instruments. This work develops design architectures, algorithms, and performance analysis of proposed GNC systems for precision dual spacecraft astrometric alignment. These systems employ a variety of GNC sensors and actuators, including laser-based alignment and ranging systems, optical imaging sensors (e.g. guide star telescope), inertial measurement units (IMU), as well as microthruster and precision stabilized platforms. A comprehensive GNC performance analysis is given for Heliophysics dual spacecraft PFF imaging mission concept.

Virtual Telescope↗

Characterization of Distributed Phase Plates for use on Z-Beamlet

Distributed Phase Plates (DPP) are used in laser experiments to create homogenous intensity distributions of a distinct shape at the location of the laser focus. Such focal shaping helps with controlling the intensity that is impeding on the target. To efficiently use a DPP, the exact size and shape of the focal distribution is of critical importance. We recorded direct images of the focal distribution with ideal continuous-wave (CW) alignment lasers and with laser pulses delivered by the Z-Beamlet facility. As necessary to protect the imaging sensors, laser pulses will not be performed by full system shots, but rather with limited energy on so-called 'rod-shots', in which Z-Beamlet's main amplifiers do not engage. The images are subsequently analyzed for characteristic radii and shape. All characterizations were performed at the Pecos target area of Sandia with a lens of 3.2 m focal length.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Prediction and Evaluation of the Image of the WFIRST Coronagraph Pupil at the Shaped-Pupil Mask

To create a high contrast field of view with a shaped pupil coronagraph (SPC), the telescope pupil is imaged onto the shaped pupil mask, the shaped pupil mask is designed and fabricated through a design optimization based on a given pupil wavefront, and deformable mirrors (DM) in the coronagraph are modulated according to a nonlinear optimization procedure. Both the mask design optimization and the DM optimization require accurate knowledge of the image of the pupil at the shaped pupil plane for the calculation of Jacobians, and the evaluation of alignment tolerances. The shaped pupil coronagraphs demonstrated in the high contrast imaging testbed (HCIT) at JPL has heretofore assumed perfect imaging of the pupil onto the shaped pupil mask. Similarly, the design and performance modeling of the WFIRST CGI instrument makes the same assumption. In this paper we estimate and compare the image of the pupil mask at the shaped pupil plane in the case of the coronagraph testbed, and the image of the telescope pupil at the shaped pupil plane for the WFIRST CGI instrument. The estimated pupil images include field curvature and aberrations resulting from the layout of the parabolic mirror imaging system, which is optimized for the source image, not the image of the pupil. We also show the results of direct measurement of the image of the pupil mask at the shaped pupil plane in the coronagraph testbed.

Crowther, Blake↗

Imaging phased telescope array study

The problems encountered in obtaining a wide field-of-view with large, space-based direct imaging phased telescope arrays were considered. After defining some of the critical systems issues, previous relevant work in the literature was reviewed and summarized. An extensive list was made of potential error sources and the error sources were categorized in the form of an error budget tree including optical design errors, optical fabrication errors, assembly and alignment errors, and environmental errors. After choosing a top level image quality requirment as a goal, a preliminary tops-down error budget allocation was performed; then, based upon engineering experience, detailed analysis, or data from the literature, a bottoms-up error budget reallocation was performed in an attempt to achieve an equitable distribution of difficulty in satisfying the various allocations. This exercise provided a realistic allocation for residual off-axis optical design errors in the presence of state-of-the-art optical fabrication and alignment errors. Three different computational techniques were developed for computing the image degradation of phased telescope arrays due to aberrations of the individual telescopes. Parametric studies and sensitivity analyses were then performed for a variety of subaperture configurations and telescope design parameters in an attempt to determine how the off-axis performance of a phased telescope array varies as the telescopes are scaled up in size. The Air Force Weapons Laboratory (AFWL) multipurpose telescope testbed (MMTT) configuration was analyzed in detail with regard to image degradation due to field curvature and distortion of the individual telescopes as they are scaled up in size.

Harvey, James E.↗

(S)TEM/EDS study of native precipitates and irradiation induced Nb-rich platelets in high-burnup M5®

We have investigated microstructure and microchemistry of precipitates and dislocation loops in high-burnup M5® using (scanning) transmission electron microscopy ((S)TEM) equipped with energy dispersive X-ray spectroscopy (EDS). Two (S)TEM lamellae were made by cryo-FIB from the same cladding sample. The Nb-rich native precipitates were found in the metal, in the suboxide and in the oxide. Upon diffraction analysis, most of the Nb-rich native precipitates in the metal matrix remain as β-Nb phase, while no β-Nb native precipitates were found in the oxide. Nearby the oxide and metal (O/M) interface, the native precipitates in the oxide were already oxidized into t-NbO2 phase. At further distance away from the O/M interface, the Nb-rich native precipitates were gradually oxidized and became amorphous. Besides the native precipitates, Nb-rich irradiation induced precipitates (IIPs) were found in the metal matrix. Using g = <0002> vector for imaging, the length of the IIPs was aligned with dislocation loops. However, no Nb segregation to the dislocation loops themselves was observed. For the first time, we report that IIPs indeed exist in the oxide but only within about 1.5 µm away from O/M interface. However, the oxidation state of the IIPs in the oxide is still unclear. The presence of both native precipitates and IIPs in the oxide may indicate the Nb concentration in the oxide solid solution remain low nearby the O/M interface, which may explain the reduced corrosion kinetics of in-pile M5®. On the other hand, no IIPs were observed in the oxide at further distance and this may indicate that they have eventually dissolved back into the oxide. A few mechanisms related to IIPs stability in the oxide are presented.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Collimation of laser-produced plasmas using axial magnetic field

We investigated the expansion dynamics of laser-produced plasmas expanding into an axial magnetic field. Plasmas were generated by focusing 1.064 µm Nd:YAG laser pulses onto a planar tin target in vacuum and allowed to expand into a 0.5 T magnetic-filed where field lines were aligned along the plume expansion direction. Gated images employing intensified CCD showed focusing of the plasma plume, which were also compared with results obtained using particle-in-cell modelling methods. The estimated density and temperature of the plasma plumes employing emission spectroscopy revealed significant changes in the presence and absence of the 0.5T magnetic field. In the presence of the field, the electron temperature is increased with distance from the target, while the density showed opposite effects.

laser produced plasma↗

SINGLE: Atomic-resolution structure identification of nanocrystals by graphene liquid cell EM

Analysis of the three-dimensional (3D) structures of nanocrystals with solution-phase transmission electron microscopy is beginning to reveal their unique physiochemical properties. We developed a “one-particle Brownian 3D reconstruction method” based on imaging of ensembles of colloidal nanocrystals using graphene liquid cell electron microscopy. Projection images of differently rotated nanocrystals are acquired using a direct electron detector with high temporal (<2.5 ms) resolution and analyzed to obtain an ensemble of 3D reconstructions. Here, we introduce computational methods required for successful atomic-resolution 3D reconstruction: (i) tracking of the individual particles throughout the time series, (ii) subtraction of the interfering background of the graphene liquid cell, (iii) identification and rejection of low-quality images, and (iv) tailored strategies for 2D/3D alignment and averaging that differ from those used in biological cryo–electron microscopy. Our developments are made available through the open-source software package SINGLE.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

ALS/Milo: BL402 RSXD data analysis

Suite of tools designed to simply data collection, extraction, reduction, and plotting for resonant soft x-ray scattering experiments performed at ALS beamline 4.0.2; speeds up the process of converting data into meaningful information for users to publish experimental results. * Python software routines for processing CCD images, including reciprocal space maps, diffraction peak alignment, resonant spectral profiles, line-cut comparisons, coordinate transforms, etc. * Scan file generator, optimized for typical uses cases, reduces burden on users by handling complex operations behind the scenes of a simplified user interface * Deployed at beamline endstation computers; packaged and deployable as standardized PyPI package * Under version control (git) and hosted on LBL-sponsored repository (bitbucket)

Shafer, Padraic↗

Superpolishing and Precision Metrology on a Metal Mandrel and Replicated Segments for Constellation-X

We have superpolished a diamond-turned aluminum mandrel (coated with electroless Ni) to an axial roughness of 6.34 nm rms. The mandrel is made to the Astro-E secondary mirror design for the 81st shell. Precision metrology at 100 mm to submicron scales has established the power spectral density of the mandrel and ultralightweight gold coated replicated segments. Predicted image quality of a set of optimally aligned replicated segments of this and a matching primary is substantially improved as compared to the flight mirrors for Astro-E. This approach using metal mandrels, superpolishing, and replicated ultralightweight foil mirrors, may represent a cost-effective approach to meeting the 15 arcsec half-energy width and weight requirements for the Constellation-X mission. Descriptions of the polishing apparatus, the precision metrology instruments, and the surface data analysis are presented. The general methods described are applicable to precision optics for both normal incidence and grazing incidence optics.

Content, D.↗

Superpolishing and Precision Metrology on a Metal Mandrel and Replicated Segments for Constellation-X

We have superpolished a diamond-turned aluminum mandrel (coated with electroless Ni) to an axial roughness of 0.34 nm rms. The mandrel is made to the Astro-E secondary mirror design for the 81st shell. Precision metrology at 100 mm to submicron scales has established the power spectral density of the mandrel and ultralightweight gold coated replicated segments. Predicted image quality of a set of optimally aligned replicated segments of this and a matching primary is substantially improved as compared to the flight mirrors for Astro-E. This approach using metal mandrels, superpolishing, and replicated ultralightweight foil mirrors, may represent a cost-effective approach to meeting the 15 arcsec half-energy width and weight requirements for the Constellation-X mission. Descriptions of the polishing apparatus, the precision metrology instruments, and the surface data analysis are presented. The general methods described are applicable to precision optics for both normal incidence and grazing incidence optics.

Content, D.↗