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At least 433 records · Page 24
All sourcesNASA NTRSDOE OSTI
NASA NTRS1981

Photolysis of CH4-NH3 mixtures and PH3 as models for the photochemical transformations on the primitive earth and Jupiter

Methane, ammonia and phosphine are some of the possible constituents of the atmospheres of the Jovian planets and their satellites. Photolysis of NH3 in the presence of CH4 at 185 nm in the temperature range of 25 C to -100 C results in the decomposition of CH4. The reaction is inhibited by added H2 or SF6. These findings are consistent with the reaction of hot hydrogen atoms with CH4 to give the CH3 radical. P2H4 is the initial product formed by the photolysis of PH3 at 206 nm. Kinetic studies established that it is the intermediate in the formation of P4 from PH3. The potential significance of these reactions to the atmospheric photochemistry of the Jovian planets and moons is discussed.

Ferris, J. P.↗
NASA NTRS1981

Clay-mediated reactions of HCN oligomers - The effect of the oxidation state of the clay

Montmorillonite clays which contain Fe(III) inhibit the oligomerization of aqueous solutions of HCN. The inhibitory effect is due to the rapid oxidation of diaminomaleonitrile, a key intermediate in HCN oligomerization, by the Fe(III) incorporated into the aluminosilicate lattice of the clay. The Fe(III) oxidizes diaminomaleonitrile to diiminosuccinonitrile, a compound which is rapidly hydrolyzed to HCN and oxalic acid derivatives. Diaminomaleonitrile is not oxidized when Fe(III) in the montmorillonite is reduced with hydrazine. The oxidation state of the clay is an important variable in experiments designed to simulate clay catalysis on the primitive earth.

Ferris, J. P.↗
NASA NTRS1982

Altitude variations in stratospheric aerosols of a tropical region

To investigate the possibility that significant amounts of tropical tropospheric air may be convectively introduced into the stratosphere, aerosol samplings over Panama were made at various altitudes using a wire impactor collector. The percentage of particle sizes less than the mean mode decreases with height above the tropopause, suggesting depletion of small particles, possibly due to coagulation. Larger aerosols (greater than 0.3 micron in diam.) are more abundant farther above the tropopause, indicating growth, mainly by condensation. The total particle concentration decreases with increasing height above the tropopause, and also with increasing temperature. Aerosols containing smaller-size particles are thus found closer to the tropopause, and larger-size, more-evolved aerosols occur at higher altitudes. These data indicate that convective activity at the Intertropical Convergence Zone may be a source mechanism for stratospheric aerosols.

Goodman, J.↗
NASA NTRS1982

Chemical evolution. XL - Clay-mediated oxidation of diaminomaleonitrile

The inhibition of the oligomerization of HCN by montmorillonite clays is shown to be caused by oxidation of diaminomaleonitrile (DAMN) by ferric ion in the clay lattice, with ferrous ion and oxalic acid the reaction products. It is demonstrated that diiminosuccinonitrile is the initial reaction product and is rapidly hydrolized to oxalic acid and HCN. The same oxidative transformations are effected by ferric ion bound to Dowex 50, ferric ion in solution, and Ni(NH3)6(2+). The rate of reaction of DAMN indicates no catalytic role for the clay in the oxidation of DAMN, and little reaction of the latter was observed with montmorillonite in which the bulk of the iron was in the divalent state. The possible significance of these redox reactions to chemical evolution is discussed.

Ferris, J. P.↗
NASA NTRS1981

Force instrumentation for cryogenic wind tunnels using one-piece strain-gage balances

Materials and techniques for a transducer capable of obtaining accurate force measurements at cryogenic temperatures (down to 77 K) and high pressures (up to 9 atm) have been determined. Areas of high stress concentration are minimized by balance design, and model and sting attachment methods able to withstand cryogenic temperatures are used. Maraging 200 is the material used for the balances, due to its high impact strength and simple heat treatment procedure. Test results verify that the balances produce reliable, repeatable, and predictable data from 300 K to 110 K under steady state conditions. Techniques have been developed to reduce the temperature-induced bridge output, such as the use of bridges with two gages mounted transverse to the principal stress direction. Under these conditions, the results given by the balances should be equally good during transient temperatures on five of the six components. The work will be used at the National Transonic Facility (NTF) at NASA Langley.

Ferris, A. T.↗
NASA NTRS1982

Mount Saint Helens aerosol evolution

Stratospheric aerosol samples were collected using a wire impactor during the year following the eruption of Mt. St. Helens. Analysis of samples shows that aerosol volume increased for 6 months due to gas-to-particle conversion and then decreased to background levels in the following 6 months.

Oberbeck, V. R.↗
NASA NTRS1973

Wind-tunnel measurements of the chordwise pressure distribution and profile drag of a research airplane model incorporating a 17-percent-thick supercritical wing

The Langley 8-foot transonic pressure tunnel to determine the wing chordwise pressure distribution for a 0.09-scale model of a research airplane incorporating a 17-percent-thick supercritical wing. Airfoil profile drag was determined from wake pressure measurements at the 42-percent-semispan wing station. The investigation was conducted at Mach numbers from 0.30 to 0.80 over an angle-of-attack range sufficient to include buffet onset. The Reynolds number based on the mean geometric chord varied from 2 x 10 to the 6th power at Mach number 0.30 to 3.33 x 10 to the 6th power at Mach number 0.65 and was maintained at a constant value of 3.86 x 10 to the 6th power at Mach numbers from 0.70 to 0.80. Pressure coefficients for four wing semispan stations and wing-section normal-force and pitching-moment coefficients for two semispan stations are presented in tabular form over the Mach number range from 0.30 to 0.80. Plotted chordwise pressure distributions and wake profiles are given for a selected range of section normal-force coefficients over the same Mach number range.

Ferris, J. C.↗
NASA NTRS1972

Static aerodynamic characteristics of a model with a 17 percent thick supercritical wing

The statis stability and control characteristics and air loads on the wing and aileron of a 0.09 scale model of an airplane with a 17 percent thick supercritical wing were investigated. The longitudinal aerodynamic characteristics were determined over a lift coefficient range sufficiently high to induce buffet onset at Mach numbers from 0.30 to 0.80. In addition, the lateral aerodynamic characteristics were determined as a function of sideslip angle and angle of attack at selected Mach numbers.

Ferris, J. C.↗
NASA NTRS1975

Static longitudinal aerodynamic characteristics of a model with a modified 17 percent thick supercritical wing

The static longitudinal stability characteristics of a 0.09 scale model of an airplane with a modified 17 percent thick supercritical wing were investigated. Modifications were made to the wing to reduce a gradual buildup of boundary layer shock loss preceding drag divergence (drag creep) noted in an earlier investigation. The longitudinal aerodynamic characteristics were determined over a Mach number range from 0.30 to 0.76 at angles of attack that generally provided a lift coefficient range from 0 to buffet onset. Results indicate that the modifications to the airfoil essentially eliminated the drag creep associated with the airfoil that occurs between the critical Mach number and the drag divergence Mach number.

Ferris, J. C.↗
NASA NTRS1982

Time variations of aerosols in the stratosphere following Mount St. Helens eruptions

Samples of stratospheric aerosols collected with U-2 aircraft for several months following the first three major eruptions of Mount St. Helens were analyzed for ash and liquid acid content. Ash grain sizes and compositions vary depending on collection altitude, location within the drifting cloud, and days following their injection. s computers Size distributions of ash particles vary with altitude. Generally small particles are depleted more rapidly at low altitudes (12 km) than at higher altitudes (17-18 km). Although samples collected 1 day after the first eruption of May 18, 1980, were dry, flow marks on the aircraft indicated parts of the cloud contained heavy acid concentrations. Indeed, all other samples obtained within 1 to 4 days after later eruptions (May 25 and June 12, 1980) were covered with copious amounts of liquid acid. Proportions of liquid to ash varied considerably depending on sampling location and cloud age. Because the acid-coated ash globules were large, they rapidly fell from the stratosphere until, by late June 1980, only a residue of acid droplets remained. Size distributions and concentrations of these droplets varied considerably.

Farlow, N. H.↗
NASA NTRS1983

Strain gage balances and buffet gages

One-piece strain gage force balances were developed for use in the National Transonic Facility (NTF). This was accomplished by studying the effects of the cryogenic environment on materials, strain gages, cements, solders, and moisture proofing agents, and selecting those that minimized strain gage output changes due to temperature. In addition, because of the higher loads that may be imposed by the NTF, these balances are designed to carry a larger load for a given diameter than conventional balances. Full cryogenic calibrations were accomplished, and wind tunnel results that were obtained from the Langley 0-3-Meter Transonic Cryogenic Tunnel were used to verify laboratory test results.

Ferris, A. T.↗
NASA NTRS1983

Measurement of the linear viscoelastic behavior of antimisting kerosene

Measurements of dynamic viscoelastic properties in very small oscillating shear deformations was made on solutions of a jet fuel, Jet A, containing an antimisting polymeric additive, FM-9. A few measurements were also made on solutions of FM-9 in a mixed solvent of mineral oil, Tetralin, and 0-terphenyl. Two samples of FM-9 had approximate number-average molecular weights of 12,000,000 and 8,100,000 as deduced from analysis of the measurements. The ranges of variables were 2.42 to 4.03 g/1 in concentration (0.3 to 0.5% by weight), 1 to 35 in temperature, 1.3 to 9.4 cp in solvent viscosity, and 103 to 6100 Hz in frequency. Measurements in the Jet A solvent were made both with and without a modifying carrier. The results were compared with the Zimm theory and the viscoelastic behavior was found to resemble rather closely that of ordinary non-polar polymers in theta solvents. The relation of the results to the antithixotropic behavior of such solutions a high shear rates is discussed in terms of intramolecular and intermolecular interactions.

Ferry, J. D.↗
NASA NTRS1982

Photochemistry of NH3, CH4 and PH3 - Possible applications to the Jovian planets

It is found that the photolysis of NH4 at 185 nm in the presence of a two-fold excess of CH4 results in the loss of about 0.25 mole of CH4 per mole of NH3 decomposed. The loss is shown to arise from the abstraction of hydrogen atoms from CH4 by photolytically generated hot hydrogen atoms. It is concluded that NH3 photolysis in the H2-abundant atmosphere of Jupiter is not responsible for the presence of the carbon compounds observed there, such as ethane, acetylene, and hydrogen cyanide, but may have had a role in the early atmosphere of Titan. Also, it is found that the photolysis of PH3 with a 206 nm light source gives P2H4, which in turn is converted to a red-brown solid. The course of the photolysis is not changed appreciably when the temperature is lowered to 157 K except that the concentration of P2H4 increases, while the presence of H2 has no effect on the P2H4 yield. Photolysis of 9:1 NH3:PH3 is found to give a rate of decomposition of PH3 that is comparable with that observed by the direct photolysis of PH3 and comparable amounts of the red-brown solid and P2H4 are observed. In addition, the implications of these results for the structures of the compounds responsible for the wide array of colors observed in the atmosphere of Jupiter are examined.

Ferris, J. P.↗
NASA NTRS1983

Aerodynamic design for improved maneuverability by the use of three-dimensional transonic theory

This study has examined the level of transonic maneuver performance that can be achieved by the use of three-dimensional transonic theory. The FLO-27 code of Jameson and Caughey (1977) was used to lower maneuver drag by the reduction of shock strength on the wing upper surface. A design procedure was used to provide a set of guidelines for the iterative application of FLO-27 during the wing design process. The fighter configuration utilized had a leading-edge sweep of 45 deg and an aspect ratio of 3.28. Tests were conducted at Mach numbers from 0.60 to 0.95 and angles of attack from -5 to 18 deg. The accurate prediction of wing shock systems required the inclusion of fuselage effects in the theory. The FLO-27 code gave a reasonable estimate of the experimental wing pressure distributions at transonic maneuver conditions in the region of the wing where the flow was attached. For Mach numbers between 0.60 and 0.95 and lift coefficients near 0.9, a wing designed by the use of FLO-27 showed substantially lower drag than an empirically developed, supercritical maneuver wing and a maneuver wing designed primarily by two-dimensional transonic theory. For some maneuver conditions, the drag of the two-dimensional design was somewhat lower.

Mann, M. J.↗
NASA NTRS1983

Prebiotic synthesis and reactions of nucleosides and nucleotides

The potential of diiminosuccinonitrile (DISN) as a prebiotic phosphorylating agent is studied. This compound is formed readily by the oxidation of diaminomaleonitrile, a tetramer of HCN. DISN is shown to produce the cyclization of 3'-adenosine monophosphate to adenosine 2',3'-cyclic phosphate in up to 40 percent yield. The DISN-mediated phosphorylation of uridine to uridine monophosphate is determined not to proceed efficiently in aqueous solution. The reaction of DISN and BrCN with uridine-5'-phosphate and uridine is found to result in the formation of 2,2'-anhydronucleotides and 2,2'-anhydronucleosides, respectively, and other reaction products resulting from an initial reaction at the 2' and 3'-hydroxyl groups. Homoionic montmorillonites were employed to study the clay mineral catalysis of the cyclization of adenosine-3'-phosphate.

Ferris, J. P.↗
NASA NTRS1983

Aerodynamic force measurements with a strain-gage balance in a cryogenic wind tunnel

Aerodynamic force measurements on a generalized 75 deg delta wing model with sharp leading edges were made with a three component internal strain gage balance in a cryogenic wind tunnel at stagnation temperatures of 300 K, 200 K, and 110 K. The feasibility of using a strain gage balance without thermal control in a cryogenic environment as well as the use of electrical resistance heaters, an insulator between the model and the balance, and a convection shield on the balance was investigated. Force and moment data on the delta wing model as measured by the balance are compared at the different temperatures while holding constant either the Reynolds number or the tunnel stagnation pressure. Tests were made at Mach numbers of 0.3 and 0.5 and at angles of attack up to 29 deg. The results indicate that it is feasible to acquire accurate force and moment data while operating at steady state thermal conditions in a cryogenic wind tunnel, either with or without electrical heaters on the balance. Within the limits of the balance accuracy, there were no apparent Reynolds number effects on the aerodynamic results for the delta wind model.

Boyden, R. P.↗
NASA NTRS1984

Aerodynamic design for improved manueverability by use of three-dimensional transonic theory

Improvements in transonic maneuver performance by the use of three-dimensional transonic theory and a transonic design procedure were examined. The FLO-27 code of Jameson and Caughey was used to design a new wing for a fighter configuration with lower drag at transonic maneuver conditions. The wing airfoil sections were altered to reduce the upper-surface shock strength by means of a design procedure which is based on the iterative application of the FLO-27 code. The plan form of the fighter configuration was fixed and had a leading edge sweep of 45 deg and an aspect ratio of 3.28. Wind-tunnel tests were conducted on this configuration at Mach numbers from 0.60 to 0.95 and angles of attack from -2 deg to 17 deg. The transonic maneuver performance of this configuration was evaluated by comparison with a wing designed by empirical methods and a wing designed primarily by two-dimensional transonic theory. The configuration designed by the use of FLO-27 had the same or lower drag than the empirical wing and, for some conditions, lower drag than the two-dimensional design. From some maneuver conditions, the drag of the two-dimensional design was somewhat lower.

Mann, M. J.↗
NASA NTRS1984

Atlas of high resolution infrared spectra of carbon dioxide

An atlas of long-path room-temperature absorption spectra of carbon dioxide is presented for the spectral intervals 1830-2100 cm, 2395-2680 cm, and 3140-3235 cm. The spectral data were recorded at high signal to noise with the 0.01 cm resolution Fourier transform interferometer. The spectra were obtained with pressures between 1 and 10 Torr of CO2 and with total paths between 24 and 384 meters. A compilation of the measured line positions and the assignments derived from the analysis are presented. Of the 3336 lines in the atlas, 94 percent were identified as CO2 lines or as residual lines H2O and CO. Calculated positions are presented for the carbon dioxide lines; a total of 52 bands of C-12O2-16, C-13O2-16, C-12O-16O-18, C-12O-16O-17, and C-13O-16O18 were identified. The weakest carbon dioxide lines marked in the atlas have intensities of approximately 0.5 x 10 to the negative 26th power cm/molecule at room temperature.

Rinsland, C. P.↗