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At least 433 records · Page 24

Analysis of an astrometric Fizeau interferometer for GAIA

The concepts related to the operation and design of the global astrometric interferometer for astrophysics (GAIA) bring together solutions chosen for the astrometry satellite and interferometric techniques. Like the Hipparcos satellite, GAIA is a continuously scanning instrument for which the integration time on any observed object is limited by the field of view of the detector. If a final astrometric accuracy of 10 microarcsec is aimed at, a field of 1 deg in diameter is needed. A design is presented for the proposed 2.6 m baseline Fizeau interferometer with two 40 cm apertures and overall dimensions compatible with the size of the Ariane 5 payload shroud. It has a 0.9 deg diffraction limited field of view. The response of the optical system to small perturbations on each optical element is given in terms of the fringe visibility, which is shown to be dependent on the sub-aperture spot separation. The robustness of the design to thermal, mechanical and manufacturing errors is discussed. The unavoidable distortion present in wide field optical systems is analyzed in terms of displacement of the interference fringes.

Loiseau, Sacha↗

Micro-Optic Color Separation Technology for Efficient Projection Displays

Phase 1 of this project focused on development of an overall optical concept which incorporated a single liquid crystal spatial light modulator. The system achieved full color by utilizing an echelon grating, which diffracted the incident light into three orders with different color spectra, in combination with a microlens array, which spatially separated RGB bands and directed the light of the appropriate wavelength to the appropriate color dot. Preliminary echelon grating designs were provided by MIT/LL and reviewed by Rockwell. Additional Rockwell activities included the Identification of microlens designs, light sources (ILC), and projection optics to fulfill the overall design requirements. An Internal subcontract was established with Rockwell's Collins Avionics and Communications Division (CACD) which specified the liquid crystal SLM (Sharp Model No. LQ 46EO2) and built the projection display baseline projector. Full Color projected video images were produced and shown at the 1995 HDS meeting in Washington. Analysis of the luminance performance of the projector and detailed parameter trade studies helped define the dependence of overall display efficiency on lamp collimation, and indicated that a lamp with very small arc dimension is required for the optical concept to be viable.

Gunning, W. J.↗

The High Mosaicity Illusion: Revealing the True Physical Characteristics of Macromolecular Crystals

An experimental system and software have been developed for simultaneously measuring the diffraction resolution and mosaic spread of macromolecular crystals. Hundreds of reflection profiles over a wide resolution range were rapidly measured by using a charge coupled device (CCD) area detector in combination with superfine phi slicing data collection. The contributions of the X-ray beam to the reflection widths were minimized by using a highly-parallel, highly-monochromatic synchrotron source. These contributions and Lorentz effects were evaluated and deconvoluted from the recorded data. Data collection and processing is described. From one degree of superfine phi slice data collected on a crystal of manganese superoxide dismutase the mosaicity of 261 reflections were measured. The average mosaicity was 0.0101 degrees (0.0035) at the full-width-at-half-maximum (FWHM) and ranged from 0.0011 degrees to 0.0188 degrees. Each reflection profile was individually fit with two gaussian profiles with the first gaussian contributing 55% and the second contributing 35% of the reflection. On average, the mosaicity of the first gaussian was 0.0054 degrees (0.0015) and the second was 0.0061 degrees (0.0023). The mosaicity of the crystal was anisotropic with fh, f k, and fl values of 0.0068 degrees, 0.0140 degrees and 0.0046 degrees, respectively at the FWHM. The anisotropic mosaicity analysis indicates that the crystal is the most perfect in the I direction which corresponds to the favored growth direction of the crystal.

Bellamy, Henry↗

The high-pressure lithium-palladium and lithium-palladium-hydrogen systems

The lithium-palladium and lithium-palladium-hydrogen systems are investigated at high pressures at and above room temperature. Two novel lithium-palladium compounds are found below 18.7 GPa. An ambient temperature phase is tentatively assigned as $F\bar{4}3m$ Li 17 Pd 4 , with a = 17.661(1) Å at 8.64 GPa, isostructural with Li 17 Sn 4 . The other phase occurs at high-temperature and is $I\bar{4}3m$ Li 11 Pd 2 , a = 9.218(1) Å at 3.88 GPa and 200 °C, similar to Li 11 Pt 2 , which is also known at high pressure. The presence of hydrogen in the system results in an $I\bar{4}3m$ structure with a = 8.856(1) Å at 9.74 GPa. This persists up to 13.3 GPa, the highest pressure studied. Below 2 GPa an fcc phase with a large unit cell, a = 19.324(1) Å at 0.39 GPa, is also observed in the presence of hydrogen. On heating the hydrogen containing system at 4 GPa the $I\bar{4}3m$ phases persists to the melting point of lithium. In both systems melting the lithium results in the loss of crystalline diffraction from palladium containing phases. This is attributed to dissolution of the palladium in the molten lithium, and on cooling the palladium remains dispersed.

Frost, Mungo↗

The Segmented Aperture Interferometric Nulling Testbed (SAINT) I: Overview and Air-side System Description

This work presents an overview of the This work presents an overview of the Segmented Aperture Interferometric Nulling Testbed (SAINT), a project that will pair an actively-controlled macro-scale segmented mirror with the Visible Nulling Coronagraph (VNC). SAINT will incorporate the VNCs demonstrated wavefront sensing and control system to refine and quantify the end-to-end system performance for high-contrast starlight suppression. This pathfinder system will be used as a tool to study and refine approaches to mitigating instabilities and complex diffraction expected from future large segmented aperture telescopes., a project that will pair an actively-controlled macro-scale segmented mirror with the Visible Nulling Coronagraph (VNC). SAINT will incorporate the VNCs demonstrated wavefront sensing and control system to refine and quantify the end-to-end system performance for high-contrast starlight suppression. This pathfinder system will be used as a tool to study and refine approaches to mitigating instabilities and complex diffraction expected from future large segmented aperture telescopes.

wavefront sensing↗

Intense Reactivity in Sulfur–Hydrogen Mixtures at High Pressure under X-ray Irradiation

Superconductivity near room temperature in the sulfur–hydrogen system arises from a sequence of reactions at high pressures, with X-ray diffraction experiments playing a central role in understanding these chemical–structural transformations and the corresponding S:H stoichiometry. Here we document X-ray irradiation acting as both a probe and as a driver of chemical reaction in this dense hydride system. We observe a reaction between molecular hydrogen (H 2 ) and elemental sulfur (S 8 ) under high pressure, induced directly by X-ray illumination, at photon energies of 12 keV using a free electron laser. The rapid synthesis of hydrogen sulfide (H 2 S) at 0.3 GPa was confirmed by optical observations, spectroscopic measurements, and microstructural changes detected by X-ray diffraction. These results document X-ray induced chemical synthesis of superconductor-forming dense hydrides, revealing an alternative production strategy and confirming the disruptive nature of X-ray exposure in studies on high-pressure hydrogen chalcogenides, from water to high-temperature superconductors.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Magnetic structure of triangular lattice compound Tb2Ni0.90Si2.94

AlB 2 -type ternary intermetallic compound Tb 2 Ni 0.90 Si 2.94 (space group P 6=mmm, hP 3, No. 191) was reported to exhibit spin freezing behaviour of the ferromagnetic clusters present in the system below T f = 9:9 K, along with the presence of spatially limited antiferromagnetic phase. In this work, on the basis of variable temperature zero-field neutron diffraction measurements, we have shown that the antiferromagnetic phase transition occurs for the compound below T N ~13 K. Neutron diffraction study indicates ab-plane non-collinear sine-modulated antiferromagnetic ordering of the system with wave vectors of k 1 = [±1/6, ±1/6, 0] and k 2 = [±1/3, ±1/3, 0] down to 1.7 K. The weak and diffuse nature of the magnetic Bragg peaks along with limited coherence length further confirm the short-range nature of the antiferromagnetic phase in this compound.

36 MATERIALS SCIENCE↗

Magnetic properties of the quasi-one-dimensional S = 1 spin chain antiferromagnet BaNi Te 2 O 7

We report a quasi-one-dimensional S=1 spin chain compound BaNiTe 2 O 7 . This magnetic system has been investigated by magnetic susceptibility, specific heat, and neutron powder diffraction. These results indicate that BaNiTe 2 O 7 develops a short-range magnetic correlation around T ~ 22K. With further cooling, an antiferromagnetic phase transition is observed at T N ~ 5.4K. Neutron powder diffraction revealed antiferromagnetic noncollinear order with a commensurate propagation vector k = (1/2,1,0). The refined magnetic moment size of Ni 2+ at 1.5 K is 1.84 μB , and its noncollinear spin texture is confirmed by first-principles calculations. In conclusion, inelastic neutron-scattering results and density functional theory calculations confirmed the quasi-one-dimensional nature of the spin systems.

1-dimensional spin chains↗

Determining Catalytically Relevant Surfaces through Coverage-Dependent Lattice Gas Models: Carbon Adsorption on Fe(100)

Here, we have quantified the C–C lateral interactions on Fe(100) using a density functional theory (DFT)-parameterized lattice gas cluster expansion (LG CE) model trained using 265 unique configurations spanning a C coverage from 0 to 1 monolayer (ML). Our LG CE model shows high predictive accuracy with a leave-multiple-out cross-validation score of 10.2 and 16.6 meV/site for systems with and without the top two layers of Fe atoms fixed, respectively. Electronic ground-state structures identified from the lattice gas model (including the structures at 0 and 1 monolayers) were further used to generate ab initio phase diagrams under a range of temperatures and pressures. At low temperatures (<400 K), we found that the 1.0 monolayer structure is dominant, whereas at higher temperatures (>500 K), the 0.88 ML structure is most likely to form on the Fe surface. Interestingly, our model identified a c (2 × 2) ordered structure at 1/2 ML, which correlates well with previous DFT studies for carbon adsorption on iron surfaces and matches with the experimentally observed low-energy electron diffraction structure. Overall, the DFT-parameterized energies for the C/Fe system including effects of coverage and configurational space can further help in developing multiscale models for various heterogeneous reactions involving C–C and C–Fe interactions.

08 HYDROGEN↗

Feasibility investigation of integrated optics Fourier transform devices

The possibility of producing an integrated optics data processing device based upon Fourier transformations or other parallel processing techniques, and the ways in which such techniques may be used to upgrade the performance of present and projected NASA systems were investigated. Activities toward this goal include; (1) production of near-diffraction-limited geodesic lenses in glass waveguides; (2) development of grinding and polishing techniques for the production of geodesic lenses in LiNbO3 waveguides; (3) development of a characterization technique for waveguide lenses; and (4) development of a theory for corrected aspheric geodesic lenses. A holographic subtraction system was devised which should be capable of rapid on-board preprocessing of a large number of parallel data channels. The principle involved is validated in three demonstrations.

Verber, C. M.↗

Analysis of Measurements for Solid State Lidar Development

A Detector Characterization Facility (DCF), capable of measuring 2-micron detection devices and evaluating heterodyne receivers, was developed at the Marshall Space Flight Center. The DCF is capable of providing all the necessary detection parameters for design, development, and calibration of coherent and incoherent solid state laser radar (lidar) systems. The coherent lidars in particular require an accurate knowledge of detector heterodyne quantum efficient, nonlinearity properties, and voltage-current relationship as a function of applied optical power. At present, no detector manufacturer provides these qualities or adequately characterizes their detectors for heterodyne detection operation. In addition, the detector characterization facility measures the detectors DC and AC quantum efficiencies noise equivalent power and frequency response up to several GHz. The DCF is also capable of evaluating various heterodyne detection schemes such as balanced detectors and fiber optic interferometers. The design and analyses of measurements for the DCF were preformed over the previous year and a detailed description of its design and capabilities was provided in the NASA report NAS8-38609/DO77. It should also be noted that the DCF design was further improved to allow for the characterization of diffractive andholographical optical elements and other critical components of coherent lidar systems.

Amzajerdian, Farzin↗

Quasicrystalline phase and crystalline approximant in Ni–Mn–In Heusler alloy system

Intermetallic compounds and micro-structures in Ni–Mn–In alloy system were investigated with transmission electron microscopy, selected-area and nano-beam electron diffraction, and energy-dispersive x-ray spectroscopy. Together with two types of Heusler phases, a decagonal quasicrystalline phase and a structurally related crystallite were found in the Ni–Mn–In system. As is well-known, most of the decagonal quasicrystals are aluminum-based intermetallic phases. It is interesting to investigate the aluminum-free decagonal quasicrystalline phase as a new member of the quasicrystal family. Structural characterization was carried out on the decagonal quasicrystalline phase and the crystalline approximant in the Ni–Mn–In alloy system.

36 MATERIALS SCIENCE↗

Research Studies on Advanced Optical Module/Head Designs for Optical Data Storage

Preprints are presented from the recent 1992 Optical Data Storage meeting in San Jose. The papers are divided into the following topical areas: Magneto-optical media (Modeling/design and fabrication/characterization/testing); Optical heads (holographic optical elements); and Optical heads (integrated optics). Some representative titles are as follow: Diffraction analysis and evaluation of several focus and track error detection schemes for magneto-optical disk systems; Proposal for massively parallel data storage system; Transfer function characteristics of super resolving systems; Modeling and measurement of a micro-optic beam deflector; Oxidation processes in magneto-optic and related materials; and A modal analysis of lamellar diffraction gratings in conical mountings.

Source record↗

Stratified Volume Diffractive Optical Elements as Low-Mass Coherent Lidar Scanners

Transmissive scanning elements for coherent laser radar systems are typically optical wedges, or prisms, which deflect the lidar beam at a specified angle and are then rotated about the instrument optical axis to produce a scan pattern. The wedge is placed in the lidar optical system subsequent to a beam-expanding telescope, implying that it has the largest diameter of any element in the system. The combination of the wedge diameter and asymmetric profile result in the element having very large mass and, consequently, relatively large power consumption required for scanning. These two parameters, mass and power consumption, are among the instrument requirements which need to be minimized when designing a lidar for a space-borne platform. Reducing the scanner contributions in these areas will have a significant effect on the overall instrument specifications, Replacing the optical wedge with a diffraction grating on the surface of a thin substrate is a straight forward approach with potential to reduce the mass of the scanning element significantly. For example, the optical wedge that will be used for the SPAce Readiness Coherent Lidar Experiment (SPARCLE) is approximately 25 cm in diameter and is made from silicon with a wedge angle designed for 30 degree deflection of a beam operating at approx. 2 micrometer wavelength. The mass of this element could be reduced by a factor of four by instead using a fused silica substrate, 1 cm thick, with a grating fabricated on one of the surfaces. For a grating to deflect a beam with a 2 micrometer wavelength by 30 degrees, a period of approximately 4 micrometers is required. This is small enough that fabrication of appropriate high efficiency blazed or multi-phase level diffractive optical gratings is prohibitively difficult. Moreover, bulk or stratified volume holographic approaches appear impractical due to materials limitations at 2 micrometers and the need to maintain adequate wavefront quality. In order to avoid the difficulties encountered in these approaches, we have developed a new type of high-efficiency grating which we call a Stratified Volume Diffractive Optical Element (SVDOE). The features of the gratings in this approach can be easily fabricated using standard photolithography and etching techniques and the materials used in the grating can be chosen specifically for a given application, In this paper we will briefly discuss the SVDOE technique and will present an example design of a lidar scanner using this approach. We will also discuss performance predictions for the example design.

Chambers, Diana M.↗

Quasi-optical beam tracing module development for millimeter-wave high-wavenumber collective scattering on the NSTX-U and EAST tokamaks

A Python3-based beam tracing code utilizing Quasi-Optics has been developed to track both incident and receiving beams in high-k collective millimeter wave scattering systems within magnetic fusion plasmas. In contrast to existing ray tracing codes that solely consider refraction, this beam tracing code incorporates diffraction phenomena, providing a more comprehensive calculation. Here, this enhanced capability allows for a more accurate calculation of the scattering volume and spatial resolution in high-k collective scattering systems, crucial for evaluating system performance and facilitating data analysis. Unlike Geometrical Optics, Quasi-Optics employs the complex eikonal method, representing a Gaussian beam as a collection of coupled rays to accurately preserve diffraction characteristics. The developed code is intended for application in NSTX-Upgrade and EAST high-k beam tracing analyses, targeting frequencies of 693 GHz and 270 GHz, respectively. The high-k system's primary objective is the observation of electron-scale instabilities. Employing a symplectic integrator, the code ensures numerical accuracy, assessed through the conservation of the Hamiltonian. With its precision and efficiency, the code facilitates rapid inter-shot analyses.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

IBIS: An Interferometer-Based Imaging System for Detecting Extrasolar Planets with a Next Generation Space Telescope

The direct detection of extrasolar planetary systems is a challenging observational objective. The observing system must be able to detect faint planetary signals against the background of diffracted and scattered starlight, zodiacal light, and in the IR, mirror thermal radiation. As part of a JPL study, we concluded that the best long-term approach is a 10-20 m filled-aperture telescope operating in the thermal IR (10-15 microns). At these wavelengths, the star/planet flux ratio is on the order of 10(exp 6)-10(exp 8). Our study supports the work of Angel et al., who proposed a cooled 16-m IR telescope and a special apodization mask to suppress the stellar light within a limited angular region around the star. Our scheme differs in that it is capable of stellar suppression over a much broader field-of- view, enabling more efficient planet searches. To do this, certain key optical signal-processing components are needed, including a coronagraph to apodize the stellar diffraction pattern, an infrared interferometer to provide further starlight suppression, a complementary visible-wavelength interferometer to sense figure errors in the telescope optics, and a deformable mirror to adaptively compensate for these errors. Because of the central role of interferometry we have designated this concept the Interferometer-Based Imaging System (IBIS). IBIS incorporates techniques originally suggested by Ken Knight for extrasolar planet detection at visible wavelengths. The type of telescope discussed at this workshop is well suited to implementation of the IBIS concept.

Diner, David J.↗

Equilibria bearing on the behavior of titanate phases during crystallization of iron silicate melts under strongly reducing conditions

Titanate phase relations at liquidus temperatures are determined for the CaAl2Si2O8-Fe2TiO4-FeTi2O5 system in contact with metallic iron by reflected- and transmitted-light microscopy, electron microprobe, and X-ray diffraction analyses. Results of critical equilibration runs are presented, various primary phase areas and liquidus isotherms are illustrated, and the geometry of the system is described. Three piercing points are determined, and it is noted that the compositional interrelations among coexisting crystalline and liquid phases as well as the sequence of the various titanate phases are indicative of the significant effects of the various cations on the relative stability of these phases. It is found that Al2O3 exerts a strong stabilizing effect on the phase assemblage of ulvospinel plus ferropseudobrookite relative to ilemite.

Lipin, B. R.↗