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At least 415 records · Page 23

Robotic Sample Manipulator for Handling Astromaterials Inside the Geolab Microgravity Glovebox

Future human and robotic sample return missions will require isolation containment systems with strict protocols and procedures for reducing inorganic and organic contamination. Robotic handling and manipulation of astromaterials may be required for preliminary examination inside such an isolation containment system. In addition, examination of astromaterials in microgravity will require constant contact to secure samples during manipulation. The National Space Grant Foundation exploration habitat (XHab) academic innovative challenge 2012 administered through the NASA advanced exploration systems (AES) deep space habitat (DSH) project awarded funding to the University of Bridgeport team to develop an engineering design for tools to facilitate holding and handling geological samples for analysis in a microgravity glovebox environment. The Bridgeport XHab team developed a robotic arm system with a three-finger gripper that could manipulate geologic samples within the existing GeoLab glovebox integrated into NASA's DSH called the GeoLab Robotic Sample Manipulator (see fig. 1 and 2). This hardware was deployed and tested during the 2012 DSH mission operations tests [1].

Bell, Mary S.↗

Explosion Welding for Hermetic Containerization

A container designed for storing samples of hazardous material features a double wall, part of which is sacrificed during an explosion-welding process in which the container is sealed and transferred to a clean environment. The major advantage of this container sealing process is that once the samples have been sealed inside, the outer wall of what remains of the container is a clean surface that has not come into contact with the environment from which the samples were taken. Thus, there is no need to devise a decontamination process capable of mitigating all hazards that might be posed by unanticipated radioactive, chemical, and/or biological contamination of the outside of the container. The container sealing method was originally intended to be used to return samples from Mars to Earth, but it could also be used to store samples of hazardous materials, without the need to decontaminate its outer surface. The process stages are shown. In its initial double-wall form, the volume between the walls is isolated from the environment; in other words, the outer wall (which is later sacrificed) initially serves to protect the inner container from contamination. The sample is placed inside the container through an opening at one end, then the container is placed into a transfer dock/lid. The surfaces that will be welded together under the explosive have been coated with a soft metallic sacrificial layer. During the explosion, the sacrificial layer is ejected, and the container walls are welded together, creating a strong metallic seal. The inner container is released during the same event and enters the clean environment.

Dolgin, Benjamin↗

Chemical weathering and diagenesis of a cold desert soil from Wright Valley, Antarctica - An analog of Martian weathering processes

Weathering, diagenesis, and chemical alteration of a soil profile from the Dry Valleys of Antarctica are investigated as an analog to soil development within the Martian regolith. Soil samples from a soil pit one meter deep on Prospect Mesa, Wright Valley, are examined for their major element concentrations, water-soluble cations and anions, carbon, sulfur, and water concentrations, and related petrographic characteristics of weathering in a cold, dry environment. A petrographic study of the samples suggests that most silicate mineral and lithic fragments exhibit some degree of alteration. Chemical alteration occurs both in samples above and within the permanently frozen zone. The concentrations of water-soluble cations, for example, Na(+), K(+), Ca(2+), and anions, Cl(-), SO4(2-), NO3(-), are found to decrease significantly from the surface to the permanently frozen zone, suggesting a major movement of water-soluble species. It is also found that enrichments in secondary mineral abundances correlate with the water soluble ion concentrations. The formation of zeolites is seen throughout the soil column; these, it is thought, may be reservoirs for volatile storage within the regolith.

Gibson, E. K.↗

Storage of solid propellants in space

A test program is described which determines the extent of physical property changes that result from extended space exposure. Primary emphasis was placed on determining the effects of space vacuum. Solid propellants were stored and their physical properties tested in a vacuum and in a dry environment. The storage caused significantly greater increases in the propellants' modulus and maximum tensile strength than occurred in parallel ambient stored samples. The data indicate that the loss of trace amounts of residual moisture from cured propellant is the apparent cause of the observed propellant property changes. Therefore, initial screening tests were carried out under dry storage conditions. Upon completion of the dry storage tests, appropriate propellant samples are exposed to an actual space environment using the Long Duration Exposure Facility (LDEF).

Udlock, D. E.↗

Comet nucleus and asteroid sample return missions

Three Advanced Design Projects have been completed this academic year at Penn State. At the beginning of the fall semester the students were organized into eight groups and given their choice of either a comet nucleus or an asteroid sample return mission. Once a mission had been chosen, the students developed conceptual designs. These were evaluated at the end of the fall semester and combined into three separate mission plans, including a comet nucleus same return (CNSR), a single asteroid sample return (SASR), and a multiple asteroid sample return (MASR). To facilitate the work required for each mission, the class was reorganized in the spring semester by combining groups to form three mission teams. An integration team consisting of two members from each group was formed for each mission so that communication and information exchange would be easier among the groups. The types of projects designed by the students evolved from numerous discussions with Penn State faculty and mission planners at the Johnson Space Center Human/Robotic Spacecraft Office. Robotic sample return missions are widely considered valuable precursors to manned missions in that they can provide details about a site's environment and scientific value. For example, a sample return from an asteroid might reveal valuable resources that, once mined, could be utilized for propulsion. These missions are also more adaptable when considering the risk to humans visiting unknown and potentially dangerous locations, such as a comet nucleus.

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Enabling Planetary In-Situ and Sample Return Missions: NASA Developed 3-D Woven Thermal Protection / Heatshield Technology for Extreme Entry Environment

Heatshield for Extreme Entry Environment Technology (HEEET) and 3-D Mid-Density Carbon-Phenolic (3MDCP) are two variants of 3-D Woven. TPS funded by STMD and SMD. HEEET was matured to TRL 6 in 2019, and SMD offered it as incentivized technology. Mars Sample Return Earth Entry System has baselined a seamless 3MDCP heatshield, and it will reach TRL 6 by 2025. HEEET and 3MDCP have been tested to withstand entry peak heat-flux ~ 4500 W/sq.cm, pressure ~ 6.5 atm, and shear ~ 4000 Pa. Bally Ribbon Mills and T.E.A.M. Inc developed looms and demonstrated their capability to weave HEEET and 3MDCP respectively. F.M.I. has demonstrated capability to form and resin infuse the preforms, and machine the TPS for final assembly. Expertise to integrate the parts reside at NASA, and NASA can transfer the knowhow to interested parties via technology transfer.

Ethiraj Venkatapathy↗

The record of solar and galactic radiations in the ancient lunar regolith and their implications for the early history of the sun and moon

The paper reviews research into the nature and history of the lunar environment, as recorded in rocks and core samples, performed by studying effects produced by the energetic nuclear particles constituting the solar wind, solar flares, and galactic cosmic rays. Results obtained with lunar rocks are discussed which suggest a remarkable constancy of the lunar environment at least over the last several million years. Analyses of lunar core samples are examined which indicate an apparent secular change in the N-15/N-14 ratio with time in solar-wind-related nitrogen, possibly due to greatly enhanced solar flare activity in the past. Lunar and meteoritic breccias are proposed as obvious candidates for extending the radiation record much further back in time, perhaps even close to the beginning of the solar system.

Grozaz, G.↗

MSFC Analysis of Thermal Control Materials on MISSE

Many different passive thermal control materials were flown as part of the Materials on International Space Station Experiment, including coatings, anodizes, and multi-layer insulation materials. Engineers and scientists at the Marshall Space Flight Center have analyzed a number of these materials, including: Zinc oxide/potassium silicate coating, Zinc orthotitanate/potassium silicate coating, Sulfuric acid anodized aluminum, Various coatings for part marking, automated rendezvous and capture, and astronaut visual aids, FEP Teflon with silver/Inconel backing, and Beta cloth with and without aluminization. These and other material samples were exposed to the low Earth orbital environment of atomic oxygen, ultraviolet radiation, thermal cycling, and hard vacuum, though atomic oxygen exposure was very limited for some samples. Solar absorptance, infrared emittance, and mass measurements indicate the durability of these materials to withstand the space environment. The effect of contamination from an active space station on the performance of white thermal control coatings is discussed.

Finckenor, Miria↗

Analysis of Thermal Control Coatings on MISSE for Aerospace Applications

Many different passive thermal control materials were flown as part of the Materials on International Space Station Experiment. Engineers and scientists at the Marshall Space Flight Center have analyzed a number of these materials, including: Zinc oxide/potassium silicate coating, Zinc oxide/potassium silicate/silicone coating, Zinc orthotitanate/potassium silicate coating, Electrically conductive thermal control coatings and Various coatings for part marking, automated rendezvous and capture, and astronaut visual aids These and other material samples were exposed to the low Earth orbital environment of atormc oxygen, ultraviolet radiation, thermal cycling, and hard vacuum, though atomic oxygen exposure was very limited for some samples. Solar absorptance, infrared emittance, and mass measurements indicate the durability of these materials to withstand the space environment. The effect of contamination from an active space station on the performance of white thermal control coatings is discussed.

Finckenor, Miria↗

Moisture diffusion parameter characteristics for epoxy composites and neat resins

The moisture absorption characteristics of two graphite/epoxy composites and their corresponding cured neat resins were studied in high humidity and water immersion environments at elevated temperatures. Moisture absorption parameters, such as equilibrium moisture content and diffusion coefficient derived from data taken on samples exposed to high humidity and water soak environments, were compared. Composite swelling in a water immersion environment was measured. Tensile strengths of cured neat resin were measured as a function of their equilibrium moisture content after exposure to different moisture environments. The effects of intermittent moderate tensile loads on the moisture absorption parameters of composite and cured neat resin samples were determined.

Long, E. R., Jr.↗

Fluid Lensing and Applications to Remote Sensing of Aquatic Environments

The use of fluid lensing technology on UAVs is presented as a novel means for 3D imaging of aquatic ecosystems from above the water's surface at the centimeter scale. Preliminary results are presented from airborne fluid lensing campaigns conducted over the coral reefs of Ofu Island, American Samoa (2013) and the stromatolite reefs of Shark Bay, Western Australia (2014), covering a combined area of 15km2. These reef ecosystems were revealed with centimetre-scale 2D resolution, and an accompanying 3D bathymetry model was derived using fluid lensing, Structure from Motion and UAV position data. Data products were validated from in-situ survey methods including underwater calibration targets, depth measurements and millimetre-scale high-dynamic range gigapixel photogrammetry. Fluid lensing is an experimental technology that uses water transmitting wavelengths to passively image underwater objects at high-resolution by exploiting time-varying optical lensing events caused by surface waves. Fluid lensing data are captured from low-altitude, cost-effective electric UAVs to achieve multispectral imagery and bathymetry models at the centimetre scale over regional areas. As a passive system, fluid lensing is presently limited by signal-to-noise ratio and water column inherent optical properties to approximately 10 m depth over visible wavelengths in clear waters. The datasets derived from fluid lensing present the first centimetre-scale images of a reef acquired from above the ocean surface, without wave distortion. The 3D multispectral data distinguish coral, fish and invertebrates in American Samoa, and reveal previously undocumented, morphologically distinct, stromatolite structures in Shark Bay. These findings suggest fluid lensing and multirotor electric drones represent a promising advance in the remote sensing of aquatic environments at the centimetre scale, or 'reef scale' relevant to the conservation of reef ecosystems. Pending further development and validation of fluid lensing methods, these technologies present a solution for large-scale 3D surveys of shallow aquatic habitats with centimetre-scale spatial resolution and hourly temporal sampling.

Aquatic↗

Debris Flux Comparisons From The Goldstone Radar, Haystack Radar, and Hax Radar Prior, During, and After the Last Solar Maximum

The continual monitoring of low Earth orbit (LEO) debris environment using highly sensitive radars is essential for an accurate characterization of these dynamic populations. Debris populations are continually evolving since there are new debris sources, previously unrecognized debris sources, and debris loss mechanisms that are dependent on the dynamic space environment. Such radar data are used to supplement, update, and validate existing orbital debris models. NASA has been utilizing radar observations of the debris environment for over a decade from three complementary radars: the NASA JPL Goldstone radar, the MIT Lincoln Laboratory (MIT/LL) Long Range Imaging Radar (known as the Haystack radar), and the MIT/LL Haystack Auxiliary radar (HAX). All of these systems are highly sensitive radars that operate in a fixed staring mode to statistically sample orbital debris in the LEO environment. Each of these radars is ideally suited to measure debris within a specific size region. The Goldstone radar generally observes objects with sizes from 2 mm to 1 cm. The Haystack radar generally measures from 5 mm to several meters. The HAX radar generally measures from 2 cm to several meters. These overlapping size regions allow a continuous measurement of cumulative debris flux versus diameter from 2 mm to several meters for a given altitude window. This is demonstrated for all three radars by comparing the debris flux versus diameter over 200 km altitude windows for 3 nonconsecutive years from 1998 through 2003. These years correspond to periods before, during, and after the peak of the last solar cycle. Comparing the year to year flux from Haystack for each of these altitude regions indicate statistically significant changes in subsets of the debris populations. Potential causes of these changes are discussed. These analysis results include error bars that represent statistical sampling errors, and are detailed in this paper.

Stokely, C. L.↗

Current Status of Martian Moons eXploration (MMX) Contamination Control and Curation Activity

Martian Moons eXploration (MMX) is a sample return mission from the Martian moon Phobos. The MMX spacecraft is scheduled to launch in 2026 and return to Earth in 2031. The main science goals of MMX are “to reveal the origin of the Martian moons and make progress in the understanding of planetary system formation and material transport in the solar system, and to observe processes that impact the circumplanetary and surface environments of Mars”. MMX has two sampling systems: coring (C)-sampler and pneumatic (P)-sampler and plans to bring back >10 g of Phobos sample. The retuned sample in the sample capsule will be transferred to the curation facility in ISAS/JAXA for sample curation and subsequent sample analysis. Contamination control of the sample return mission requires special care to prevent terrestrial contamination to the spacecraft, which would ruin the scientific value of the returned sample. Retaining the pristineness of the retuned sample is an important task of the MMX Curation and Sampler Science teams. The basis of the contamination control is (1) to minimize and understand the nature and amount of contaminants, (2) to perform contamination assessment and evaluate the effect of contaminants in the spacecraft on the retuned sample, (3) to employ a contamination knowledge (CK) material coupon in the spacecraft to identify the contaminants in the returned samples. In the MMX contamination control plan, the allowable contamination level for each contaminant is carefully defined. They are mostly set to be 1/1000 of the expected amount of each material in the returned sample and are divided into two main categories: organic and inorganic. The allowable atmospheric leakage rate to the sample container is also defined. The allowable contamination level of the organic materials is based on the composition of carbonaceous chondrites. The target contaminants are amino acids, aliphatic and aromatic hydrocarbons, carboxylic acids, etc. In case of the inorganic materials, the target contaminants are important elements to permit distinguishing the origin of the Martian moon by nucleosynthetic isotope anomalies (Cr, Ti, and Mo) and to reveal the evolution of the Martian moon by chronology (Hf, W, U, Pb, Rb, Sr, Sm, and Nd). The key instrument of contamination control in the sample return mission is the sampler system. The C-sampler has been developed by JAXA and the P-sampler was provided by Honeybee/NASA. In MMX, materials used in the two samplers (C- and P- sampler) were carefully selected to avoid potential contamination from the design stage of the system. The individual parts of the C-sampler FM (Flight Model) were thoroughly cleaned at the curation facility in ISAS/JAXA by the full-course cleaning procedure, which is an ultrasonic cleaning with organic solvents and ultrapure water in several steps. The equivalent level of cleaning was also carried out on the P-Samper FM as well by Honeybee Robotics in the USA. Now, MMX is in the critical phase for contamination control called ATLO: Assembly, Test, and Launch Operations. During the ATLO phase, sampler FM is constantly purged with nitrogen gas and maintained at positive pressure to prevent environmental contamination. The surrounding environments of the sampler FM are also simultaneously monitored using the CK Monitoring Coupon Set, which consists of several witness materials such as a glass petri dish, sapphire glass disk, and carbon adhesive tape (Figure 1). The detailed environmental assessment of each clean room used for the assembly and test of the sampler FM has also been conducted. This assessment includes microbial analysis, which was performed for OSIRIS-REx. Regarding the sample recovery and sample curation, we have started the designing of Sample Container Disassembling Instrument for the sample recovery from the sample container and the MMX curation chamber for sample curation. The curation protocol for the Phobos returned sample has also been discussed by the MMX Sample Analysis Working Team (SAWT). The MMX curation protocol consists of three phases: (1) quick analysis, (2) pre-basic characterization, and (3) basic characterization. (1) is extraction of the sample gas from the sample container and analysis by mass spectrometry, (2) is observation in bulk level, and (3) is observation in grain level and allocation of the sample aliquots. In parallel with the curation protocol, the returned sample undergoes preliminary examination for scientific investigations to achieve science goals. In addition, the CK witness plates made of sapphire glass are on board the sampler system. The CK witness plates will be recovered from the sampler system and analyzed by SAWT for the assessment of in-flight contamination.

Haruna Sugahara↗

Assessment of holographic microscopy for quantifying marine particle size and concentration

Holographic microscopy has emerged as a tool for in situ imaging of microscopic organisms and other particles in the marine environment: appealing because of the relatively larger sampling volume and simpler optical configuration compared to other imaging systems. However, its quantitative capabilities have so far remained uncertain, in part because hologram reconstruction and image recognition have required manual operation. Here, we assess the quantitative skill of our automated hologram processing pipeline (CCV Pipeline), to evaluate the size and concentration measurements of environmental and cultured assemblages of marine plankton particles, and microspheres. Over 1 million particles, ranging from 10 to 200 μm in equivalent spherical diameter, imaged by the 4‐Deep HoloSea digital inline holographic microscope (DIHM) are analyzed. These measurements were collected in parallel with a FlowCam (FC), Imaging FlowCytobot (IFCB), and manual microscope identification. Once corrections for particle location and nonuniform illumination were developed and applied, the DIHM showed an underestimate in ESD of about 3% to 10%, but successfully reproduced the size spectral slope from environmental samples, and the size distribution of cultures (Dunaliella tertiolecta, Heterosigma akashiwo, and Prorocentrum micans) and microspheres. DIHM concentrations (order 1 to 1000 particles ml(exp −1)) showed a linear agreement (r(exp 2) = 0.73) with the other instruments, but individual comparisons at times had large uncertainty. Overall, we found the DIHM and the CCV Pipeline required extensive manual correction, but once corrected, provided concentration and size estimates comparable to the other imaging systems assessed in this study. Holographic cameras are mechanically simple, autonomous, can operate at very high pressures, and provide a larger sampling volume than comparable lens‐based tools. Thus, we anticipate that these characterization efforts will be rewarded with novel discovery in new oceanic environments.

Noah L. Walcutt↗

Trace Oxygen Measurements of Asteroid Sample Storage Desiccators

The Astromaterials Curation facility at the NASA Johnson Space Center is currently curating more than 120 g of carbonaceous asteroid Bennu material as well as over 500 mg of asteroid Ryugu [1 and 2]. These astromaterials are stored in isolating desiccators and gloveboxes under a continuous purge of pure (<1 ppm O 2 ) gaseous nitrogen. The oxygen and moisture concentrations in our OSIRIS-REx sample processing gloveboxes are continuously monitored via integrated sensors; however, our sample storage desiccators lack integrated oxygen and humidity sensors. In previous studies, we used PreSens Fibox 4 trace oxygen meters and optochemical PSt9 spot sensors to measure the oxygen concentrations in candidate asteroid sample containers that had been sealed in nitrogen; we determined that Eagle stainless steel containers inhibit the ingress of external oxygen for several weeks [3]. This optochemical sensor technology allowed us to take precise, contactless measurements within a trace range of 0 to 200 ppmv O 2 . The effectiveness of the trace oxygen sensors in our container experiments inspired us to utilize them to assess the performance of our desiccators that previously lacked trace oxygen monitoring. In this study, our goal was to determine the quality of the nitrogen purge in the isolating desiccator under normal operating conditions by measuring the trace oxygen content. Utilizing optochemical sensor technology, we determined how long the oxygen concentration takes to reach an equilibrium in the desiccator; that is, determine the rate at which the oxygen diffusion into the desiccator equals the rate at which oxygen diffuses out of the desiccator via N2 purge. Additionally, we wanted to determine the oxygen concentration at this equilibrium, the state in which our desiccators are in during normal operating conditions. We tested a custom three chamber desiccator manufactured by Germfree using a PSt9 trace oxygen sensor spot that was mounted into a ¼” National Pipe Tapered (NPT) metal flow-through cell and attached it to the desiccator exhaust. The desiccator consists of top, middle, and bottom isolating chambers. The top chamber door was opened for several minutes to simulate a sample exchange, it was sealed, and then purged ~15 Standard Cubic Feet per Hour (SCFH). Oxygen measurements were automatically recorded via the Fibox 4 trace oxygen meter in 5-minute intervals over the course of a 24-hour period. Our results indicate the desiccator reached an equilibrium value of 10-15 ppm O 2 after ~5 hours (Fig. 1). This data allows us to explore standards for purging and exchange protocols that can be applied to similar types of desiccators in Hayabusa2, OSIRIS-REx, and for sample return collections. The assessment of the internal gaseous compositions of desiccators also allows us to share with the community the N 2 environment in which many of our asteroid samples and hardware are securely curated. Future measurements will include other nitrogen flow rates and measuring the trace oxygen concentration as a function of time for the levels of the previous commercial desiccator in which the Hayabusa2 sample collection was stored. We will also analyze how long the desiccators hold N2 after being disconnected from their N2 source, an extended measurement for sample security reassurance.

Curation↗

Geopolymer Lunar Concrete under Reduced-Pressure Curing and Vacuum Exposure

Geopolymer concrete has emerged as a promising material for constructing habitats, roads, landing pads, and other necessary infrastructure on the lunar surface. Proper in-situ resource utilization (ISRU) is an important aspect of any candidate lunar construction material. Geopolymer concrete is effective at ISRU, as the lunar regolith can be used in the “as found” condition and mixed with an alkaline solution, such as sodium silicate and sodium hydroxide, which could also be mostly produced in-situ. It is envisioned that any concrete material on the lunar surface would be deposited with additive manufacturing techniques and would require a temporary environmental enclosure to mitigate the harsh lunar environment during construction and curing, such as pressure and temperature. Data are needed to set a benchmark for the conditions to be achieved within the deployable environmental enclosure during printing, as well as the resultant material properties after the enclosure is removed. This novel study investigated the influence of reduced atmospheric pressures during the initial curing period on the compressive strength of geopolymer lunar concrete created with two types of lunar regolith simulant. The simulants used in the study represent the regolith for the lunar mare (OPRL2N) and lunar highlands (OPRH2N) regions. Results show a noticeable decline in strength with a reduction in pressure and visible degradation. After the deployable environmental enclosure is removed from the printed segment of infrastructure on the lunar surface, it would then be exposed to the harsh vacuum environment. To understand the importance of curing time required within the deployable enclosure before it is removed, samples were cast and cured for different lengths of time and then exposed to a vacuum chamber capable of achieving 100 mTorr. Control samples were also cast at the same time but left in a standard laboratory environment after curing. The weight change and compressive strength as a function of time in the vacuum chamber were monitored for up to 56 days. The results showed that exposure to the vacuum limits further reaction and strength gain in comparison to control samples left in the laboratory environment. This research is in strong alignment with the 2020 NASA Technology Taxonomy materials area (12.1) and the in-situ resource utilization area (7.1), as it provides necessary data on the geopolymer lunar concrete material to support safe and sustainable options for maintaining a human presence on the Moon.

Moon to Mars Planetary Autonomous Construction Tec↗

Acoustic levitation and manipulation for space applications

A wide spectrum of experiments to be performed in space in a microgravity environment require levitation and manipulation of liquid or molten samples. A novel acoustic method has been developed at JPL for controlling liquid samples without physical contacts. This method utilizes the static pressure generated by three orthogonal acoustic standing waves excited within an enclosure. Furthermore, this method will allow the sample to be rotated and/or oscillated by modifying the phase angles and/or the amplitude of the acoustic field. This technique has been proven both in our laboratory and in a microgravity environment provided by KC-135 flights. Samples placed within our chamber driven at (1,0,0), (0,1,0), and (0,0,1), modes were indeed levitated, rotated, and oscillated.

Wang, T. G.↗

Low fluxes of X-rays

Analytic and experimental investigations of the interactions of high-energy protons with spacecraft materials and light nucleus atoms were conducted. Irradiation of typical materials for scintillation detectors using accelerator-produced energetic protons and associated theoretical calculations indicate activity within detectors produced by this mechanism is significant to detection of low-level cosmic gamma radiation. Samples of several materials were flown aboard Skylab to obtain measures of the neutron and proton flux environment. Extremely weak activity was produced in the samples. Calculations of interactions of intermediate-energy protons with light nuclei were performed and a more complete theoretical model programmed for digital computation. Preliminary results appear promising for calculating products of such interactions.

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