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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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All sourcesNASA NTRSDOE OSTI
NASA NTRS2012

Collisional Histories of Comets and Trojan Asteroids: Diopside, Magnesite, and Fayalite Impact Studies

Comets and asteroids have weathered dynamic histories, as evidenced by their rough surfaces. The Nice model describes a violent reshuffling of small bodies during the Late Heavy Bombardment, with collisions acting to grind these planetesimals away. This creates an additional source of impact material that can re-work the surfaces of the larger bodies over the lifetime of the solar system. Here, we investigate the possibility that signatures due to impacts (e.g. from micrometeoroids or meteoroids) could be detected in their spectra, and how that can be explained by the physical manifestation of shock in the crystalline structure of minerals. All impact experiments were conducted in the Johnson Space Center Experimental Impact Laboratory using the vertical gun. Impact speeds ranged from approx.2.0 km/s to approx.2.8 km/s. All experiments were conducted at room temperature. Minerals found in comets and asteroids were chosen as targets, including diopside (MgCaSi2O6, monoclinic pyroxene), magnesite (MgCO3, carbonate), and fayalite (FeSiO4, olivine). Impacted samples were analyzed using a Fourier Transform Infrared Spectrometer (FTIR) and a Transmission Electron Microscope (TEM). Absorbance features in the 8-13 m spectral region demonstrate relative amplitude changes as well as wavelength shifts. Corresponding TEM images exhibit planar shock dislocations in the crystalline structure, attributed to deformation at high strain and low temperatures. Elongating or shortening the axes of the crystalline structure of forsterite (Mg2SiO4, olivine) using a discrete dipole approximation model (Lindsay et al., submitted) yields changes in spectral features similar to those observed in our impacted laboratory minerals.

Lederer, S. M.↗
NASA NTRS2012

Portable Fourier Transform Spectroscopy for Analysis of Surface Contamination and Quality Control

Progress has been made into adapting and enhancing a commercially available infrared spectrometer for the development of a handheld device for in-field measurements of the chemical composition of various samples of materials. The intent is to duplicate the functionality of a benchtop Fourier transform infrared spectrometer (FTIR) within the compactness of a handheld instrument with significantly improved spectral responsivity. Existing commercial technology, like the deuterated L-alanine triglycine sulfide detectors (DLATGS), is capable of sensitive in-field chemical analysis. This proposed approach compares several subsystem elements of the FTIR inside of the commercial, non-benchtop system to the commercial benchtop systems. These subsystem elements are the detector, the preamplifier and associated electronics of the detector, the interferometer, associated readout parameters, and cooling. This effort will examine these different detector subsystem elements to look for limitations in each. These limitations will be explored collaboratively with the commercial provider, and will be prioritized to meet the deliverable objectives. The tool design will be that of a handheld gun containing the IR filament source and associated optics. It will operate in a point-and-shoot manner, pointing the source and optics at the sample under test and capturing the reflected response of the material in the same handheld gun. Data will be captured via the gun and ported to a laptop.

Pugel, Diane↗
DOE OSTI2024

An affordable platform for automated synthesis and electrochemical characterization

In recent years, self-driving laboratories (SDLs) have emerged as a powerful tool to expedite various areas of chemical research. For optimal functionality, these laboratories must be adaptable, readily modifying configurations to meet researchers' specific needs. Despite these advances, much of chemistry still depends on proprietary equipment from specialized vendors, which can be restrictive and difficult to customize for diverse lab setups. Moreover, ensuring reproducibility requires full disclosure of equipment details. In this work, we introduce an automated system featuring a cost-effective, self-designed potentiostat and a straightforward synthesis platform. We provide complete transparency by disclosing the electronic schematics of the potentiostat and the software used in the system. Our aim is to reduce the barriers to entry for SDLs and promote the principles of open science.

Pablo-García, Sergio↗
DOE OSTI2023

High-Performance Accelerator Modeling: Toward Improving Controls and Diagnostics for High-Brightness Beams in Experiment

One of the main charges of beam physics is to improve the overall beam quality delivered to experiments and applications, which is generally quantified by the beam brightness. High brightness beams have numerous applications, including x-ray free electron lasers and ultrafast electron diffraction (UED). To these ends, this thesis details efforts to use high-performance models --- high-fidelity models that execute quickly --- for controls and diagnostics. To demonstrate the generality of these techniques, this thesis focuses on three of the most successful photoinjector designs currently used worldwide: the UCLA/SLAC/BNL-type high-gradient S-band gun, the continuous-wave high-repetition rate VHF APEX gun and the L-band DESY-PITZ-type gun. Work will be shown from Pegasus (UCLA), HiRES (LBNL) and FAST (FNAL).Specifically, data-driven models for online virtual diagnostics are presented, in this case, in the context of UED at HiRES, leading to a temporal resolution improvement. Methods for improving the fidelity of physics-based models are discussed, with examples at HiRES, Pegasus and FAST. Markov-chain Monte Carlo analysis is applied to match simulations, in the context of photocathode studies at HiRES and Pegasus. Lastly, the augmentation of online model-based predictions with model-independent optimization is explored in a fluctuating environment at Pegasus and HiRES. A central theme of this dissertation is working with parameter fluctuations when modeling an accelerator beamline. Long-term drifts and shot-to-shot jitter exist in every accelerator to a varying degree and therefore play an important role in every chapter of this dissertation. This thesis attempts to address the issues associated with these fluctuations when trying to develop faithful model representations of the system.

43 PARTICLE ACCELERATORS↗
NASA NTRS1972

Study of a splat cooled Cu-Zr-noncrystalline phase.

By rapid quenching from the melt, using the splat forming gun technique, a noncrystalline phase has been obtained in a Cu-Zr alloy containing 60 at. % Cu. Upon heating, rapid crystallization of the samples takes place at 477 C with a heat release of about 700 cal per mol. The variation of the electrical resistivity of the samples with temperature confirms the transformation. Very high resolution electron microscopy studies of the structural changes of the samples upon heating are presented and show the gradual crystallization of the amorphous structure.

Revcolevschi, A.↗
DOE OSTI2020

Laser-free GHz stroboscopic transmission electron microscope: Components, system integration, and practical considerations for pump–probe measurements

In this work a 300 keV transmission electron microscope was modified to produce broadband pulsed beams that can be, in principle, between 40 MHz and 12 GHz, corresponding to temporal resolution in the nanosecond to picosecond range without an excitation laser. The key enabling technology is a pair of phase-matched modulating and de-modulating traveling wave metallic comb striplines (pulsers). An initial temporal resolution of 30 ps was achieved with a strobe frequency of 6.0 GHz. The placement of the pulsers, mounted immediately below the gun, allows for preservation of all optical configurations, otherwise available to the unmodified instrument, and therefore makes such a post-modified instrument for dual-use, i.e., both pulsed-beam mode (i.e., stroboscopic time-resolved) and conventional continuous waveform mode. In this article, we describe the elements inserted into the beam path, challenges encountered during integration with an in-service microscope, and early results from an electric-field-driven pump–probe experiment. We conclude with ideas for making this class of instruments broadly applicable for examining cyclical and repeatable phenomena.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1979

Design of high-perveance confined-flow guns for periodic-permanent-magnet-focused tubes

An approach to the design of high perveance, low compression guns is described in which confinement is used to stabilize the beam for subsequent periodic-permanent-magnet focusing. The computed results for two cases are presented. A magnetic boundary value problem was solved for the scalar potential from which the axial magnetic field was computed. A solution was found by iterating between Poisson's equation and the electron trajectory calculations. Magnetic field values were varied in magnitude until a laminar beam with minimum scalloping was produced.

Stankiewicz, N.↗
NASA NTRS1988

ELF electric turbulence near an electron beam-emitting rocket in the auroral ionosphere - Echo 6

Orthogonal double-probes on the Echo 6 free-lying plasma diagnostic payload were used to study ELF turbulent electric fields during 36-keV beam injections. The observed characteristics of the ELF fields can best be explained by the current systems set up around the entire system rather than by a direct beam-plasma interaction. Frequency-power spectra were calculated for two different polarizations as a function of the probe-gun payload distance, and measurements were obtained of the lower hybrid waves near 8.5 kHz and whistler mode waves near 125 kHz. The dispersion of a current instability was calculated in order to investigate the generation mechanism of the observed ELF electric turbulence.

Abe, Y.↗
DOE OSTI2020

Experimental characterization of a section of a spherically imploding plasma liner formed by merging hypersonic plasma jets

In this work, we report experimental results on merging of hypersonic plasma jets, which is the fundamental building block for forming spherically imploding plasma liners as a potential standoff compression driver for magneto-inertial fusion. Jets are formed and launched by contoured-gap coaxial plasma guns mounted at the six vertices and the center of a hexagon covering approximately one-tenth of the surface area of a 9-ft-diameter spherical chamber. First, from experiments with two and three merging jets of four different species (N, Ar, Kr, and Xe), we show that (1) density spatial non-uniformities can be large (with electron-density jumps ranging from 2.9 for N to 6.6 for Xe) when shocks form upon jet merging, but smaller (density jumps <2) when shocks do not form; (2) jet impurities (20% Ti in these experiments) can increase the level of density spatial non-uniformity by increasing the collisionality of jet merging, leading to shock formation rather than potentially more desirable shockless jet merging; and (3) the liner Mach number can remain high (≳10), as required for plasma liners to be an effective compression driver. Secondly, from experiments with six and seven merging jets using Ar, we present results with improved jet-to-jet mass balance of <2% across jets, including (1) evidence of substantially increased balance in the jet merging and symmetry of the liner structure and (2) potentially favorable changes in the jet-merging morphology with the addition of the seventh jet. Ultimately, for both experiments, we present comparisons between experimental and synthetic data from three-dimensional hydrodynamic codes.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS2013

Insights into Collisional between Small Bodies: Comparison of Impacted Magnesium-rich Minerals

Impacts are sustained by comets and asteroids throughout their lives, especially early in the Solar system's history, as described by the Nice model. Identifying observable properties that may be altered due to impacts can lead to a better understanding their collisional histories. Here, we investigate spectral effects and physical shock features observed in infrared spectra and Transmission Electron Microscope (TEM) images, respectively, of magnesium-rich minerals subjected to shock through impact experiments. Samples of magnesium-rich forsterite (Mg2SiO4, olivine), orthoenstatite (Mg2SiO3, pyroxene), diopside (MgCaSi2O6, monoclinic pyroxene), and magnesite (MgCO3, carbonate) were impacted at speeds of 2.4 km/s, 2.6 km/s and 2.8 km/s. Impact experiments were conducted in the Johnson Space Center Experimental Impact Laboratory using the vertical gun. Clear signatures are observed in both the mid-IR spectra (shift in wavelengths of the spectral peaks and relative amplitude changes) of all minerals except magnesite, and in TEM images (planar dislocations) of both the forsterite and orthoenstatite samples. Further discussion on forsterite and enstatite analyses can be found in Jensen et al., this meeting.

Lederer, Susan M.↗
DOE OSTI2025

MAIA: A new detector concept for a 10 TeV muon collider

Muon colliders offer a compelling opportunity to explore the TeV scale and conduct precision tests of the Standard Model, all within a relatively compact geographical footprint. This paper introduces a new detector concept, MAIA (Muon Accelerator Instrumented Apparatus), optimized for $\sqrt{s}=10$ TeV $\mu\mu$ collisions. The detector features an all-silicon tracker immersed in a 5T solenoid field. High-granularity silicon-tungsten and iron-scintillator calorimeters surrounding the solenoid capture high-energy electronic and hadronic showers, respectively, and support particle-flow reconstruction. The outermost subsystem comprises an air-gap muon spectrometer, which enables standalone track reconstruction for high-momentum muons. The performance of the MAIA detector is evaluated in terms of differential particle reconstruction efficiencies and resolutions. Beam-induced background (BIB) simulations generated in FLUKA are overlaid with single particle gun samples to assess detector reconstruction capabilities under realistic experimental conditions. Even with BIB, reconstruction efficiencies exceed 95% for energetic tracks, photons, and neutrons in the central region of the detector. This paper outlines promising avenues of future work, including forward region optimization and opportunities for enhanced flavor/boosted object tagging, and addresses the technological assumptions needed to achieve the desired detector performance.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2020

Direct Observations of Sub-micropulse Electron-beam Effects from Short-range Wakefields in TESLA-type Superconducting RF Cavities

The preservation of the low emittance of electron beams during transport in the accelerating structures of large facilities is an ongoing challenge. In the cases of the TESLA-type superconducting rf cavities currently used in the European X-ray Free-electron Laser (FEL) and the under construction Linac Coherent Light Source upgrade (LCLS-II), off-axis beam transport may result in emittance dilution due to transverse long-range and short-range wakefields (SRW)*. To investigate such effects, experiments were performed at the Fermilab Accelerator Science and Technology (FAST) facility with its unique two-cavity configuration after the photocathode rf gun. We used optical transition radiation (OTR) imaging with a UV-visible synchroscan streak camera to display sub-micropulse y-t effects in the 41-MeV beam. The head-tail transverse kicks within the 11-ps-long micropulses were observed at the 100-micron level for steering off-axis in one cavity and several 100 microns for two cavities. Since the SRW kick angles go inversely with energy, these results may inform the commissioning plans of the LCLS-II injector where beam will be injected at ~1 MeV into a cryomodule.

43 PARTICLE ACCELERATORS↗
NASA NTRS2008

Outcome of Recent Satellite Impact Experiments

This paper summarizes three satellite impact tests completed in early 2007 through collaboration between Kyushu University and the NASA Orbital Debris Program Office. The previous experiments completed in late 2005 aimed to compare low- and hyper-velocity impacts on identical target satellites, whereas the new tests used larger satellites as targets and aimed to investigate the effects of impact directions. Three identical micro satellites equipped with fully-functional electronic devices were prepared as targets. Their dimensions were 20 cm by 20 cm by 20 cm, and the mass of each was approximately 1.3 kilograms. Aluminum alloy solid spheres, with diameters of 3 cm and masses of 39 grams were prepared as projectiles. The impact velocity was approximately 1.7 km/s. The impact tests were carried out at the two-stage light gas gun facility at the Kyushu Institute of Technology. All three target satellites were completely fragmented, but there were noticeable differences among the three sets of fragments due to the different impact directions. More than 1000 fragments from each test were collected, measured, photographed, and documented with material descriptions. The analysis of the fragments is currently in progress. Preliminary results of the new data and comparisons with previous data will be included in the paper.

Hanada, Toshiya↗
NASA NTRS1988

Ion beam and plasma methods of producing diamondlike carbon films

A variety of plasma and ion beam techniques was employed to generate diamondlike carbon films. These methods included the use of RF sputtering, dc glow discharge, vacuum arc, plasma gun, ion beam sputtering, and both single and dual ion beam deposition. Since films were generated using a wide variety of techniques, the physico-chemical properties of these films varied considerably. In general, these films had characteristics that were desirable in a number of applications. For example, the films generated using both single and dual ion beam systems were evaluated for applications including power electronics as insulated gates and protective coatings on transmitting windows. These films were impervious to reagents which dissolve graphitic and polymeric carbon structures. Nuclear reaction and combustion analysis indicated hydrogen to carbon ratios to be 1.00, which allowed the films to have good transmittance not only in the infrared, but also in the visible. Other evaluated properties of these films include band gap, resistivity, adherence, density, microhardness, and intrinsic stress. The results of these studies and those of the other techniques for depositing diamondlike carbon films are presented.

Swec, Diane M.↗
DOE OSTI2024

CEBAF Injector for K Long Beam Conditions

The Continuous Electron Beam Accelerator Facility (CEBAF) at Jefferson Lab concurrently operates four experimental Halls with distinct bunch charge specifications and repetition rates. Numerous critical beam parameters within CEBAF are configured in the injector, some remaining unchanged throughout the accelerator. Consequently, the injector plays a crucial role in determining final beam characteristics, including bunch structure, beam sizes, bunch lengths, energy spread, and beam transmission. The Jefferson Lab KL experiment is scheduled to take place at CEBAF in Hall D, featuring a much lower bunch repetition rate of 7.80 MHz or 15.59 MHz, below the nominal values of 249.5 MHz or 499 MHz. Although the proposed average current of 5 ?A or 10 ?A is low compared to the maximum CEBAF cur- rent of approximately 180 ?A, the corresponding bunch charge is unusually high for CEBAF injector operation. This study focuses on the behavior of low-repetition-rate, high-bunch- charge (0.32 to 0.64 pC) beams in the CEBAF injector. We investigated the evolution and transmission of low-charge beams to space-charge dominated high-charge beams in the front end of the CEBAF injector for two configurations: the pre-existing CEBAF Phase 1 injector upgrade, operated at 130 kV, and the existing CEBAF Phase 2 injector upgrade, operated at 140 kV, 180 kV, and to be operated at 200 kV. The electron beam through the CEBAF injector is characterized using beam dynamics simulations and comparisons with the available measurements performed at 130 kV. Multi-objective genetic optimizations of the CEBAF injector were performed to determine the operating magnetic elements and RF settings for the evolution and transmission of low, moderate, and high charge beams in the CEBAF injector at 180 kV and 200 kV DC gun voltages. Subsequently, simulations at the same voltages were conducted to obtain the beam characteristics at the front end of the CEBAF injector. The laser spot size and laser pulse length at the cathode were varied to observe their effects on beam transmission in the injector at different voltages (130 kV, 180 kV, and 200 kV). Experimental studies at 130 kV, 140 kV, and 180 kV validate the simulations. Beam study measurements are carried out using EPICS tools, while optimizations and simulations are facilitated by General Particle Tracer. Based on the findings, optimal parameters for the upcoming Jefferson Lab KL experiment are proposed, utilizing a lower repetition rate and higher bunch charge

Pokharel, Sunil↗
DOE OSTI2021

Optimization of a High Bunch Charge ERL Injection Merger for PERLE

Delivery of high charge electron bunches into the main loop of an ERL (energy recovery linac) while preserving the emittance is challenging. This is because at the typical injection momentum, space charge forces still have a significant effect on the beam dynamics. In this work we consider the design of the merger for PERLE, an ERL test facility to be based at IJCLab in France. Previous simulations have shown that the baseline DC gun based injector can achieve the required emittance at the booster linac exit. The quality of the 500 pC bunches must then be preserved with space charge through the merger at total beam energy of 7 MeV keeping the emittance below 6 mm mrad. The beam dynamics in the merger were simulated using the code OPAL and optimised using a genetic algorithm. Three possible merger schemes were investigated. The goal of the optimisation was to minimise the emittance growth while also achieving the required Twiss parameters to match onto the spreader at the main linac exit. A three dipole solution is then examined in more detail.

Hounsell, B.↗
NASA NTRS2001

The Combined Detection of Morphological and Molecular Biomarkers: Implications for Astrobiology

Experience gathered by previous researchers during their hunt for evidence of early Earth life has shown the complexity in interpreting observations of possible microfossils and to establish the evidence to be positive. Similarly, the stillsimmering controversy on the nature of the nano-structures in Martian meteorite ALH84001 described by McKay et al. (1996) emphasizes the difficulties of conclusively identifying those structures as (a) fossilized bacterial cells and (b) establish their indigeneity. A better understanding of biological signatures in rocks is needed in order to identify traces of microbial life, which include morphological, mineralogical and chemical traces. It is thus considered crucial to tackle the problems emerging in the search for evidence of early life on Earth and in exopaleontological research with a multidisciplinary approach. With this is mind we applied surface sensitive Time of Flight-Secondary Ion Mass Spectroscopy (ToF-SIMS) to a previously described 25 m.y. old fossil bacterial biofilm. This technique allows in situ analysis with high mass resolution as well as molecular imaging of micron sized structures. As no extraction or derivatisation of the sample is required for ToF-SIMS analysis, electron microscopical investigation of the same samples subsequent to analysis is possible, thus allowing the combination of molecular and morphological biomarkers. The analysed fossil bacterial biofilms were associated with macrofossils from volcanoclastic lacustrine sediments from the Upper Oligocene Enspel formation (Germany). Preliminary scanning electron microscopy (SEM) studies have shown that a fossil structure interpreted as a coprolite purely consisted of fossilized bacterial biofilm. For ToF-SIMS investigation small particles were taken from the fossil biofilm and mounted onto Au-coated In-foil and analysed in a Phi Evans T-2000 TRIFT system. The ToF-SIMS analysed samples were Au/Pd-sputter coated and imaged using a Philips XL40 Field Emission Gun SEM (FEG-SEM). ToF-SIMS analysis of the organic rich fossil biofilm (TOC 29%) in the 0-100 Dalton (Da) range showed significant amounts of inorganic species, confirming the results obtained previously by EDX analysis, clearly showing the bacterial fossils to be mineralised. ToF-SIMS furthermore revealed the presence of a variety of low- and high-mass organic molecules and fragments thereof. These include peaks indicative of alkenes and alkanes, aromatic organic species and the polycyclic aromatic hydrocarbon naphthalene. More tentatively, peaks indicative of alkyl pyrroles and pyridyl-CH2 were identified. Other peaks of interest include peaks indicative of C(n)H(2n)O2 and C(n)H(2n-2)O2, which according to their general formula would suggest the presence of both saturated and unsaturated fatty acids although further in situ derivatisation experiments and GC-MS (Gas Chromatography MS) need to be applied to verify this beyond doubt. Furthermore, peaks at m/z 370, 384, 398, 412, 426, 440, 454 and 468 were identified, which indicate the potential presence of bacterial hopanes, a class of biomarkers indicative of bacteria. The main diagnostic peak for this group of chemicals is the fragment at m/z 191.18. Our studies conducted on purified hopane standards have shown that in the high-mass resolution mode differentiation of this diagnostic hopane peak and polyethylene at m/z 191.05 is possible. However, the spectra discussed here were collected in the lower resolution mapping mode, therefore this differentiation was not possible. The centroids of the possible hopane peaks obtained on the fossil biofilms are well within the range associated with bacterial hopanes. There is a strong possibility therefore that hopanoids may be associated with the fossil bacterial cells. Due to the non-destructive nature of ToF-SIMS, analysed samples can be studied using SEM, thus allowing the combination of morphological and molecular biomarkers. Subsequent SEM analysis of the ToF-SIMS analysed samples confirmed that the analysed material purely consists of fossil bacterial cells. This is thus the first successful effort to demonstrate the combination of spectral and morphological biomarkers. The advantages of highly sensitive non-destructive in situ analysis techniques for biomarker detection are invaluable, particularly with respect to envisaged Mars sample return missions, as it may allow us to identify remains and traces of former microbial life in both ancient terrestrial and extraterrestrial materials. This technique may prove particularly useful in the quest for extraterrestrial life with respect to precious extraterrestrial materials, as minute quantities are sufficient to conduct analysis.

Toporski, J.↗
DOE OSTI2021

Investigations of Long-Range Wakefield Effects in a TESLA-type Cryomodule at FAST

The preservation of low emittance of electron beams during transport in the accelerating structures of large facilities is an ongoing challenge. In the cases of the TESLA-type superconducting rf cavities currently used in the European X-ray Free-electron Laser (XFEL) and the under-construction Linac Coherent Light Source upgrade (LCLS-II), off-axis beam transport may result in emittance dilution due to transverse long-range wakefields (LRWs) and short-range wakefields (SRW)***. To investigate such effects, experiments were performed at the Fermilab Accelerator Science and Technology (FAST) facility with its unique configuration of two TESLA-type cavities after the photocathode rf gun followed by an 8-cavity cryomodule CM). We generated beam trajectory changes with the H/V125 corrector set located 4 m upstream of the cryomodule. At 125 pC/bunch, 50 bunches, 25-MeV input, and 100-MeV exit energy, we observed for the first time submacropulse position slews of up to 500 microns at locations ~3 m after the CM and a centroid oscillation at a difference frequency of 240 kHz further downstream. Both are emittance-dilution effects which we mitigated with selective upstream beam steering.

43 PARTICLE ACCELERATORS↗