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At least 415 records · Page 23
All sourcesNASA NTRSDOE OSTI
NASA NTRS1986

Toughening mechanisms in elastomer-modified epoxies. I - Mechanical studies. II - Microscopy studies

Tensile dilatometry at constant displacement rates is presently used to ascertain whether voiding, crazing or shear banding are the deformation mechanisms at work in the toughening of brittle epoxies through the addition of an elastomeric phase. The results obtained for epoxies toughened by various levels of several types of carbonyl-terminated butadiene nitrile liquid rubber indicate that, at low strain rates, the rubber particles simply enhance shear deformation; at sufficiently high strain rates, the particles cavitate and promote further shear deformation. Examinations of these materials are conducted by means of SEM, TEM, and optical microscopy in the second part of this study. Toughening is hypothesized to involve cavitation's relieving of triaxial tension at the crack tip, as well as shear band formation, which creates a plastic zone.

Yee, A. F.↗
DOE OSTI2026

Molecular origin of anisotropic shear elastoplasticity in chitin

Chitin nano- and mesoscale structures present in the exoskeleton of crustaceans exhibit exceptional longitudinal stiffness and toughness, rivaling or even exceeding that of many synthetic polymer architectures. Here, we reveal the origin of the asymmetric shear response in chitin multiscale architectures, marked by pronounced anisotropy in deformation. Under shear aligned with the molecular axis, chitin accommodates strain through coherent atomic rearrangements that enable elastic recovery. In contrast, shear applied perpendicular to this axis induces liquid-like plasticity via localized sliding. These results demonstrate the intrinsic mechanical anisotropy of chitin, underpinning a dual function in resisting repetitive loading while dissipating internal stress during high-strain events. Our findings establish the molecular basis of shear elastoplasticity in multiscale chitin structures, wherein axial elasticity supports energy storage in load-bearing regions, whereas transverse plasticity enables controlled energy dissipation. These atomic-scale insights lay a foundation for the predictive design of chitin-based materials with tunable strength-toughness profiles.

Wan, Zhangmin [University of British Columbia, Van↗
DOE OSTI2021

In-situ TEM observation of shear induced microstructure evolution in Cu-Nb alloy

Phase boundaries in multiphase alloys govern defect interaction and chemical intermixing across different phases during plastic deformation. Dynamic interaction of defects with phase boundaries in multiphase alloys, especially for immiscible alloys, has been topic of significant research interest in recent years. In this work, we describe a novel approach for carrying out in-situ TEM shear deformation to directly observe interfacial microstructural evolution of a Cu-Nb alloy. A unique double shear specimen geometry is microfabricated by a focused ion beam technique to apply shear deformation upon push loading inside the TEM. From the real-time observation, we discover that the phase boundary with a zigzag morphology effectively blocks stacking faults nucleated in a Cu grain from slipping into a Nb grain. Meanwhile, the Cu phase bears the most plastic deformation through slip or twinning mechanisms. This work sheds light on understanding the shear deformation and the behavior of phase boundaries in multiphase alloys during shear deformation.

36 MATERIALS SCIENCE↗
DOE OSTI2025

Temperature-Dependent Mechanical Properties of Ni-Based Concentrated Alloys: Insights from First-Principles Calculations

The present work focuses on predicting temperature-dependent mechanical properties of Ni-based concentrated alloys Ni 18 Cr 10 Co 10 Fe 6 M 4 (abbreviated by X 44 M 4 , with M = Al, V, Mn, Fe, Nb, Mo, and W) using density functional theory (DFT). These predictions are based on shear (plastic) and elastic deformations, utilizing the special quasirandom structure (SQS), the phonon-based quasiharmonic approach (QHA), and the quasistatic approach. The resulting properties include coefficient of thermal expansion via QHA, ideal shear strength (τ IS ), and stable and unstable stacking fault energies (γ SF and γ US ) through pure alias shear deformation, and elastic constants (c ij ), bulk modulus (B 0 ), and shear modules (G 0 ) via elastic deformation. Notably, predicting accurate γ SF is challenging due to uncertainties that can exceed the γ SF values. τ IS and γ US exhibit a strong linear relationship, enabling the accurate prediction of γ US based on the precisely determined τ IS . All mechanical properties of X 44 M 4 decrease with increasing temperature, except for some γ SF cases such as X 44 M 4 with M = V, Mn, Fe, Mo, and W. Among the X 44 M 4 alloys, X 44 Nb 4 exhibits the lowest τ IS , γ US , and G 0 values, and the highest B 0 /G 0 ratio, while X 44 Mn 4 has the lowest B 0 and B 0 /G 0 ratio. We found that volume is a crucial descriptor for understanding and modeling mechanical properties (except B0 and maybe also γ SF ) affected by alloying elements and temperature. Ni-based dilute alloys (e.g., Ni 11 M 1 and Ni 31 M 1 ) and concentrated alloys (e.g., X 44 M 4 ) show similar trends in mechanical properties influenced by alloying elements and temperature, simplifying the analysis and design of Ni-based alloys.

Elastic properties↗
NASA NTRS1980

Stress analysis of bonded plates and joints

The paper presents a general numerical method of solution to the transverse normal stress and longitudinal shear stress distributions in the adhesive layers of bonded stiffener plates, double lap joints, and strap joints, all of dissimilar orthotropic adherends. The bending deformations and the transverse shear deformations are included in the analytical model. The present influence of bending deformations of adherends on both the normal and shear stresses in adhesive layers is discussed in detail for practical cases.

Yuceoglu, U.↗
NASA NTRS1985

Shear strain anomalies in composite beam specimens by moire interferometry

Experimental analyses were performed for determination of in-plane deformations and shear strains in unidirectional and quasi-isotropic graphite-epoxy beams. Forty-eight-ply beams were subjected to five-point and three-point flexure. Whole-field measurements were recorded at load levels from about 20 percent to more than 90 percent of failure loads. Contour maps of U and W displacement fields were obtained by moire interferometry, using reference gratings of 2400 lines/mm. Clearly defined fringes with fringe orders exceeding 1000 were obtained. Whole-field contour maps of shear strains were obtained. Various anomalous effects were detected in the displacement fields. Their analysis indicated excess shear strains in resin-rich zones in regions of shear tractions; free-edge shear strains in quasi-isotropic specimens in regions of normal stresses, and shear stresses associated with cyclic shear compliances of quasi-isotropic laminates in regions of shear tractions. Their contributions could occur independently or in superposition. Qualitative analyses addressed questions of the effect of specimen overhang, nonlinearity, and characteristics of five-point and three-point flexure tests.

Post, D.↗
NASA NTRS1977

Characterization of crack growth under combined loading

Room-temperature static and cyclic tests were made on 21 aluminum plates in the shape of a 91.4x91.4-cm Maltese cross with 45 deg flaws to develop crack growth and fracture toughness data under mixed-mode conditions. During cyclic testing, it was impossible to maintain a high proportion of shear-mode deformation on the crack tips. Cracks either branched or turned. Under static loading, cracks remained straight if shear stress intensity exceeded normal stress intensity. Mixed-mode crack growth rate data compared reasonably well with published single-mode data, and measured crack displacements agreed with the straight and branched crack analyses. Values of critical strain energy release rate at fracture for pure shear were approximately 50% higher than for pure normal opening, and there was a large reduction in normal stress intensity at fracture in the presence of high shear stress intensity. Net section stresses were well into the inelastic range when fracture occurred under high shear on the cracks.

Feldman, A.↗
DOE OSTI2020

The role of irradiation on deformation-induced martensitic phase transformations in face-centered cubic alloys

Localized deformation, including that by the deformation-induced shearing martensitic phase transformation, is responsible for hardening and embrittlement in irradiated face-centered cubic alloys. These localized deformation processes can have profound consequences on the mechanical integrity of common structural metals used in extreme radiation environments such as nuclear reactors. This article aims to review and understand exactly how irradiation affects the martensitic phase transformation in face-centered cubic alloys, with an emphasis on austenitic stainless steel, given its ubiquity in the archival literature. The influence of irradiation on stacking fault energy and subsequent implications on the phase transformation are discussed. Mechanisms by which irradiation-induced microstructures enhance the phase transformation are also described, including the surface energy contribution of irradiation-induced cavities (i.e., voids and bubbles) toward the critical martensite nucleation energy, and partial dislocation–cavity interactions. In conclusion, a deformation mechanism map illustrates how irradiation-induced cavities can modulate the martensitic transformation pathway.

36 MATERIALS SCIENCE↗
NASA NTRS1988

A study on the thermal and moisture influences on the free-edge delamination of laminated composites

A simple delamination analysis method is presented here. It is based on a shear-type deformation theory and includes hygrothermal effects. These environmental conditions are applied to the strain energy release rate and interlaminar shear stresses. The method is applied to mixed mode edge delamination specimens made of T300/5208 graphite/epoxy material. Residual thermal and moisture stresses significantly influenced the strain energy release rate and interlaminar stresses. Both experienced large increases when thermal conditions were added to the mechanical strains. These effects were alleviated when moisture stresses were included. Thermal effects on the interlaminar shear stress and total energy release rate were totally alleviated for the same specific moisture content. Moreover, the value of the moisture content was not significantly affected by the stacking sequence for the laminates considered.

Mahler, Mary A.↗
NASA NTRS2001

Rheology of Diabase: Implications for Tectonics on Venus and Mars

Two important goals of our experimental investigation of the rheological behavior of diabase rocks were: (1) to determine flow laws describing their creep behavior over wide ranges of temperature, stress and strain rate and (2) to develop an understanding of the physical mechanisms by which these rocks flow under laboratory conditions. With this basis, a primary objective then was to construct constitutive equations that can be used to extrapolate from laboratory to planetary conditions. We specifically studied the rheological properties of both natural rock samples and synthetic aggregates. The former provided constraints for geologic systems, while the latter defined the relative contributions of the constituent mineral phases and avoided the influence of glass/melt found in natural samples. In addition, partially molten samples of crustal rock composition were deformed in shear to large strains (greater than 200%) important in crustal environments. The results of this research yielded essential rheological properties essential for models of crustal deformation on terrestrial planets, specifically Venus and Mars, as well as on the geodynamical evolution of these planets. Over the past three years, we also completed our investigation of the creep behavior of water ice with applications to the glaciers, ice sheets and icy satellites. Constitutive equations were determined that describe flow over a wide ranged of stress, strain rate, grain size and temperature. In the case of ice, three creep regimes were delineate. Extrapolation demonstrates that dislocation glide and grain boundary sliding processes dominate flow in ice I under planetary conditions and that diffusion creep is not an important deformation mechanism either in the laboratory or on icy satellites. These results have already been incorporated by other investigators into models describing, for example, the thickness and stability of the ice shell on Europa and to unravel long-standing discrepancies between field observations on glaciers and laboratory results.

Kohlstedt, David L.↗
NASA NTRS1984

Deformation measurements of composite multi-span beam shear specimens by Moire interferometry

Experimental analyses were performed for determination of in plane deformations and shear strains in unidirectional and quasi-isotropic graphite-epoxy beams. Forty-eight ply beams were subjected to 5 point and 3 point flexure. Whole field measurements were recorded at load levels from about 20% to more than 90% of failure loads. Contour maps of U and W displacement fields were obtained by moire interferometry, using reference gratings of 2400 lines/mm. Clearly defined fringes with fringe orders exceeding 1000 were obtained. Whole field contour maps of shear strains were obtained by a method developed for these tests. Various anomalous effects were detected in the displacement fields. Their analysis indicated excess shear strains in resin rich zones in regions of shear tractions; free edge shear strains in quasi-isotropic specimens in regions of normal stresses; and shear stresses associated with cyclic shear compliances of quasi-isotropic plies in regions of shear tractions. Their contributions could occur independently or in superposition. Qualitative analyses addressed questions of relaxation; influence of contact stress distribution; specimen failure; effect of specimen overhang; nonlinearity; and qualities of 5 and 3 point flexure tests.

Post, D.↗
NASA NTRS2005

Prediction of Mechanical Properties of Polymers With Various Force Fields

The effect of force field type on the predicted elastic properties of a polyimide is examined using a multiscale modeling technique. Molecular Dynamics simulations are used to predict the atomic structure and elastic properties of the polymer by subjecting a representative volume element of the material to bulk and shear finite deformations. The elastic properties of the polyimide are determined using three force fields: AMBER, OPLS-AA, and MM3. The predicted values of Young s modulus and shear modulus of the polyimide are compared with experimental values. The results indicate that the mechanical properties of the polyimide predicted with the OPLS-AA force field most closely matched those from experiment. The results also indicate that while the complexity of the force field does not have a significant effect on the accuracy of predicted properties, small differences in the force constants and the functional form of individual terms in the force fields determine the accuracy of the force field in predicting the elastic properties of the polyimide.

Odegard, Gregory M.↗
NASA NTRSDate not supplied

Understanding the Vertical Slope of Mesoscale Snow Band Reflectivity Signatures

Mesoscale snow bands are frequently responsible for dumping large amounts of snow over a relatively small region and pose a considerable forecasting challenge. The ongoing NASA Investigation of Microphysics and Precipitation for Atlantic Coast-Threatening Snowstorms (IMPACTS) field campaign observed several instances of mesoscale snow bands during January and February of 2020 and 2022. These snow bands were sampled by a combination of airborne (NASA ER-2 and P-3) and ground-based remote sensing and in-situ instruments. Along-band cross sections of these snow bands reveal that many of them are vertically sloped. Our preliminary analysis into one of these snow bands suggests that the vertical slope is not maintained by isentropic lift and does not appear to be tied to horizontal deformation. A combined analysis of the reflectivity and wind retrievals from the ER-2 radars raises the possibility that these features could be produced by vertical wind shear layers deforming fall streaks into bands that extend hundreds of kilometers. The present study will focus on extending our preliminary analysis to additional cases and understanding the mechanisms that support these features using a combination of radar data, in-situ aircraft measurements, and numerical modeling.

Charles Helms↗
NASA NTRS1987

Composite box beam analysis - Theory and experiments

Beam theory is widely used as a first approximation in numerous structural applications. When applied to composite beams, the accuracy of beam theory becomes questionable because (1) the shearing and warping deformations become significant, as the shearing stiffness of composite laminates is often very low, and (2) several elastic couplings can occur that strongly influence the behavior of composite beams. The torsional behavior of thin-walled composite beams has important implications for aeronautical structures and is deeply modified by the above nonclassical effects. This paper presents two comprehensive analysis methodologies for composite beams and describes experimental results obtained from a thin-walled, rectangular cross-sectional beam. The theoretical predictions are found in good agreement with the observed twist and strain distributions. Out-of-plane torsional warping of the cross-section is found to be the key factor for an accurate modeling of the torsional behavior of such structures.

Bauchau, O. A.↗
NASA NTRS1988

Residual thermal and moisture influences on the free-edge delamination of laminated composites

A simple delamination analysis method is developed. It is based on a shear-type deformation theory and includes hygrothermal effects. The method is applied to mixed-mode edge delamination specimens made of T300/5208 graphite/epoxy. It is found that residual thermal influences were alleviated when moisture stresses were included. Thermal effects on the interlaminar shear stress and total energy release rate were totally alleviated for the same specific moisture content. Moreover, this value of moisture content was not significantly affected by the stacking sequence for the laminates considered.

Armanios, Erian A.↗
DOE OSTI2022

Characterization and Modeling of Deformation Induced Damage in Titanium Alloys

Over the lifetime of their DOE support, and specifically during the past funding cycle, the PIs have primarily focused on ambient temperature studies of the mechanisms of heterogeneous deformation and shear transfer at GBs. The PIs have developed and applied a broad array of experimental approaches complemented by advanced computational methods and simulations to enable new understanding of GB shear transfer, and a new approach for modeling this behavior at the mechanistic level has been established. The PIs have examined how slip behavior differs on the surface and interior of polycrystals using a variety of approaches. Some of the associated data has been used to generate 3-D models of experimentally-characterized microstructures that both support interpretation of deformation mechanisms as well as reveal where modeling needs to be improved to more closely agree with what is experimentally observed. The PIs progress in constitutive modeling of crystal plasticity has introduced explicit GB resistance to shear that depends on the mutual geometry of active slip systems. This past work places the PIs in a good position to take on the challenges associated with mechanistically understanding the interplay between GBS and slip interactions.

42 ENGINEERING↗
DOE OSTI2021

Amorphization in extreme deformation of the CrMnFeCoNi high-entropy alloy

Ever-harsher service conditions in the future will call for materials with increasing ability to undergo deformation without sustaining damage while retaining high strength. Prime candidates for these conditions are certain high-entropy alloys (HEAs), which have extraordinary work-hardening ability and toughness. By subjecting the equiatomic CrMnFeCoNi HEA to severe plastic deformation through swaging followed by either quasi-static compression or dynamic deformation in shear, we observe a dense structure comprising stacking faults, twins, transformation from the face-centered cubic to the hexagonal close-packed structure, and, of particular note, amorphization. The coordinated propagation of stacking faults and twins along {111} planes generates high-deformation regions, which can reorganize into hexagonal packets; when the defect density in these regions reaches a critical level, they generate islands of amorphous material. These regions can have outstanding mechanical properties, which provide additional strengthening and/or toughening mechanisms to enhance the capability of these alloys to withstand extreme loading conditions.

36 MATERIALS SCIENCE↗