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At least 397 records · Page 22

Progress of simulations for reacting shear layers

An attempt was made to develop a high speed, chemically reactive shear layer test rig. The purpose of the experiment was to study the mixing of oxidizer and fuel streams in reacting shear layers for various density, velocity, and Mach number. The primary goal was to understand the effects of the compressibility upon mixing and combustion in a fundamental way. Therefore, a two-dimensional shear layer is highly desirable for its simplicity to quantify the compressibility effects. The RPLUS 2D code is used to calculate the flow fields of different sections of the test rig. The emphasis was on the supersonic nozzle design, the vitiation process for the hot air stream and the overall thermodynamic conditions of the test matrix. The k-epsilon turbulence model with wall function was successfully implemented in the RPLUS code. The k and epsilon equations are solved simultaneously and the LU scheme is used to make it compatible with the flow solver.

Yu, Sheng-Tao↗

Local Heat Flux Measurements with Single Element Coaxial Injectors

To support the mission for the NASA Vision for Space Exploration, the NASA Marshall Space Flight Center conducted a program in 2005 to improve the capability to predict local thermal compatibility and heat transfer in liquid propellant rocket engine combustion devices. The ultimate objective was to predict and hence reduce the local peak heat flux due to injector design, resulting in a significant improvement in overall engine reliability and durability. Such analyses are applicable to combustion devices in booster, upper stage, and in-space engines, as well as for small thrusters with few elements in the injector. In this program, single element and three-element injectors were hot-fire tested with liquid oxygen and ambient temperature gaseous hydrogen propellants at The Pennsylvania State University Cryogenic Combustor Laboratory from May to August 2005. Local heat fluxes were measured in a 1-inch internal diameter heat sink combustion chamber using Medtherm coaxial thermocouples and Gardon heat flux gauges. Injectors were tested with shear coaxial and swirl coaxial elements, including recessed, flush and scarfed oxidizer post configurations, and concentric and non-concentric fuel annuli. This paper includes general descriptions of the experimental hardware, instrumentation, and results of the hot-fire testing for three of the single element injectors - recessed-post shear coaxial with concentric fuel, flush-post swirl coaxial with concentric fuel, and scarfed-post swirl coaxial with concentric fuel. Detailed geometry and test results will be published elsewhere to provide well-defined data sets for injector development and model validatation.

Jones, Gregg↗

Novel Preprocessing Techniques for Enhancing Flowability of Miscanthus

Purpose-grown energy crops possess significant potential as promising feedstocks for biofuel and biochemical production. However, similar to other biomass feedstocks, their utilization has been hindered by handling and feeding challenges such as clogging and segregation, which prevent biorefineries from operating at full capacity. These challenges arise primarily due to particle attributes including irregular shape, high flexibility, and high compressibility, leading to interlocking, high compaction, and significant friction under stress consolidation. To enhance operational reliability, it is crucial to focus on preprocessing techniques to address these issues, alongside accurately characterizing the mechanical and physical properties and flow performance of these feedstocks. This study investigates novel preprocessing techniques, including pelletization and torrefaction, to fundamentally alter these particle attributes and improve flowability. Miscanthus, an herbaceous energy crop, was the primary focus of this study. Samples were processed using a Forest Concepts Crumbler rotary shear system and an oscillating multi-stack screen bed to achieve two nominal (baseline) particle sizes: 6mm and 2mm. The study evaluated the efficiency and energy consumption of size reduction, revealing that while 2mm particles required more energy, they exhibited better flowability and higher yield strength compared to 6mm particles. Shear and compression tests assessed the material's shear strength, internal friction, and elastic modulus, while wedge-shaped hopper tests measured the critical arching distance and mass flow rate. The results provide valuable insights into the mechanical properties and processing efficiency of Miscanthus, contributing to the development of a preprocessing framework that enhances energy efficiency and material flowability in bioenergy production. However, further preprocessing and development are required to optimize this framework fully.

09 - BIOMASS FUELS↗

Toward Interpreting Failure in Sintered-Silver Interconnection Systems

The mechanical strength and subsequent reliability of a sintered-silver interconnection system is a function of numerous independent parameters. That system is still undergoing process development. Most of those parameters (e.g., choice of plating) are arguably and unfortunately taken for granted and are independent of the silver s cohesive strength. To explore such effects, shear strength testing and failure analyses were completed on a simple, mock sintered-silver interconnection system consisting of bonding two DBC ceramic substrates. Silver and gold platings were part of the test matrix, as was pre-drying strategies, and the consideration of stencil-printing vs. screen-printing. Shear strength of sintered-silver interconnect systems was found to be was insensitive to the choice of plating, drying practice, and printing method provided careful and consistent processing of the sintered-silver are practiced. But if the service stress in sintered silver interconnect systems is anticipated to exceed ~ 60 MPa, then the system will likely fail.

Wereszczak, Andrew A↗

Fabrication of Titanium Bonded Joint Specimens for High Temperature Testing

Four sets of adhesively bonded, titanium lap-shear coupon specimens were fabricated for ultimate strength testing according to the ASTM D1002 and D3165 standards. Important features of the fabrication methods, processing details, and lap-shear test results are presented for specimens fabricated using a modified bismaleimide adhesive, EA 9673, on titanium. Surface treatment of the titanium was performed using surface abrasion followed by one of two separate chemical etching processes. Although cure cycle requirements are different among most adhesives, a single surface preparation method was sought as the preferred method for conditioning the titanium specimens prior to bonding and curing. A fabrication process using a combination of low-pressure grit-blasting of the titanium surface followed by anodization with a sodium hydroxide solution applied to the D1002 specimen geometry provided the highest lapshear strengths in the study. Additionally, difficulties documented during the fabrication process of the D3165 specimens along with features of the D3165 geometry were identified as factors that contributed to lower lap-shear strength results for the D3165 specimens as compared to the results for the D1002 specimens.

Smeltzer, Stanley S., III↗

Mechanical Properties of Continuous Fiber Reinforced Zirconium Diboride Matrix Composites

Continuous fiber reinforced zirconium diboride matrix composites, SCS-9a-(RBSiCZrB2)matrix, are being developed for leading edge, rocket nozzle and turbine engine applications. Recently, the composite materials have been characterized for tensile properties to 1250 C, the highest temperature tested. The tensile properties are fiber dominated as the matrix is microcracked on fabrication, but favorable failure characteristic are observed. Compression and shear mechanical testing results will be reported if completed. The effects of fiber volume fraction and matrix density on mechanical properties will be discussed. The target applications of the materials will be discussed. Specific testing being performed towards qualification for these applications will be included.

Stuffle, Kevin↗

Rheological Behaviour, Mechanical Properties and Processability of Biodegradable Polymer Systems for Film Blowing

Films for agricultural or packaging applications are typically made of low density polyethylene (LDPE). They are produced through the film blowing process, which requires the use of polymers with suitable rheological properties. Furthermore, the short shelf-life which is often related to many packed products leads to huge amounts of plastic-based wastes. This suggests the use of biodegradable and/or compostable polymers in replacement for traditional ones. To this regard, only few data exist on the rheological properties of biodegradable polymers undergoing film blowing processing. In this work, a detailed investigation on the rheological, mechanical and processability behaviour of some biodegradable polymers (originating from MaterBi{sup ®} and Bioflex{sup ®} commercial groups) was carried out, in order to assess their suitability to industrial-scale film blowing by direct comparison with a traditional non-biodegradable polymer (LDPE). Rheological tests under shear and non-isothermal elongational flow allowed to find out the two most suitable polymer grades. The film blowing production operations at different draw and blow-up ratios (from 2.5 to 3.5) showed that the two samples are suitable for industrial scale operations. Results from tensile and impact tests indicated that the two selected polymers exhibit significantly different mechanical properties (up to 10–15%).

36 MATERIALS SCIENCE↗

Shear rupture of a directionally solidified eutectic gamma/gamma prime - alpha (Mo) alloy

Directionally solidified Mo alloys are evaluated to determine the shear rupture strength and to possibly improve it by microstructural and heat treatment variations. Bars of the alloy containing nominally 5.7% Al and 33.5% Mo by weight with balance Ni were directionally solidified at rates between 10 and 100 mm per hour in furnaces with thermal gradients at the liquid-solid interface of 250 or 100 C per cm. A limited number of longitudinal shear rupture tests were conducted at 760 C and 207 MPa in the as - solidified and in several heat treated conditions. It is shown that shear rupture failures are partly transgranular and that resistance to failure is prompted by good fiber alignment and a matrix structure consisting mainly of gamma prime. Well aligned as - solidified specimens sustained the shear stress for an average of 81 hours. A simulated coating heat treatment appeared to increase the transformation of gamma to gamma prime and raised the average shear life of aligned specimens to 111 hours. However, heat treatments at 1245 C and especially at 1190 C appeared to be detrimental by causing partial solutioning of the gamma prime, and reducing lives to 47 and 10 hours, respectively.

Harf, F. H.↗

Brazing of Martensitic Stainless Steel to Copper Using Electroplated Copper and Silver Coatings

Brazing of 3 mm thick sheets of low-carbon martensitic stainless steel and Cu-Cr-Zr-Ti alloy was attempted using electroplated coatings of Cu and Ag. Ni coating of 5 µm thick was provided on the MSS base metal to enhance the wettability. Brazing experiments were carried out at 985 °C for a holding of 15 min. Detailed microstructural studies, hardness, lap-shear, tensile, and pressure tests were carried out on the brazed joints. The reaction between the Cu and Ag coatings lead to the formation of in situ braze metal. The microstructure of the braze metal was found to consist of Cu-rich primary alpha (α{sub P}) and Ag-rich eutectic mixture (β + α{sub E}). In lap-shear tests, the brazed joints produced with an overlap of 9 and 6 mm were found to fail in copper base metal, while the joints produced with an overlap of 3 mm failed in the braze metal exhibiting a lap-shear strength of 147 MPa. In tensile tests, the butt brazed joints were found to fail in copper base metal as well with an average tensile strength of 213 MPa. The braze metal hardness was found to be higher than the hardness of the copper base metal. In pressure tests, the brazed panels were found to survive a pressure of 750 bar without undergoing any damage. These results show that electroplated coatings of Cu and Ag can be advantageously utilized for brazing of large, complex-shaped parts such as thrust chambers in space industry.

36 MATERIALS SCIENCE↗

Development of procedures for calculating stiffness and damping of elastomers in engineering applications. Part 5: Elastomer performance limits and the design and test of an elastomer damper

Tests were performed on elastomer specimens of the material polybutadiene to determine the performance limitations imposed by strain, temperature, and frequency. Three specimens were tested: a shear specimen, a compression specimen, and a second compression specimen in which thermocouples were embedded in the elastomer buttons. Stiffness and damping were determined from all tests, and internal temperatures were recorded for the instrumented compression specimen. Measured results are presented together with comparisons between predictions of a thermo-viscoelastic analysis and the measured results. Dampers of polybutadiene and Viton were designed, built, and tested. Vibration measurements were made and sensitivity of vibration to change in unbalance was also determined. Values for log decrement were extracted from the synchronous response curves. Comparisons were made between measured sensitivity to unbalance and log decrement and predicted values for these quantities.

Tecza, J. A.↗

Shear rupture of a directionally solidified eutectic gamma/gamma-prime - alpha /Mo/ alloy

Directionally solidified gamma/gamma-prime - alpha (Mo) eutectic alloys are being evaluated for application as advanced aircraft engine turbine blades. Their excellent high-temperature strength is partly due to their directionally aligned microstructure. However, alloys with such directional structures may display low shear strength at 760 C, the operating temperature of advanced blade roots. The objective of this investigation was to determine the shear rupture strength of the gamma/gamma-prime - alpha eutectic alloy and possibly to improve it by microstructural and heat-treatment variations. Bars of gamma/gamma-prime - alpha alloy containing nominally 5.7% Al and 33.5% Mo by weight with balance Ni were directionally solidified at rates between 10 and 100 mm per hour. Materials were solidified in furnaces with thermal gradients at the liquid-solid interface of 250 or 100 C per cm. A limited number of longitudinal shear rupture tests were conducted at 760 C and 207 MPa in the as-solidified and in several heat-treated conditions. It was found that the shear rupture failures are partly transgranular and that resistance to failure is promoted by good fiber alignment and a matrix structure consisting mainly of gamma-prime. Well-aligned as-solidified specimens sustained the shear stress for an average of 81 hours, while cellular material failed in one hour or less.

Harf, F. H.↗

Ca(2+) regulates fluid shear-induced cytoskeletal reorganization and gene expression in osteoblasts

Osteoblasts subjected to fluid shear increase the expression of the early response gene, c-fos, and the inducible isoform of cyclooxygenase, COX-2, two proteins linked to the anabolic response of bone to mechanical stimulation, in vivo. These increases in gene expression are dependent on shear-induced actin stress fiber formation. Here, we demonstrate that MC3T3-E1 osteoblast-like cells respond to shear with a rapid increase in intracellular Ca(2+) concentration ([Ca(2+)](i)) that we postulate is important to subsequent cellular responses to shear. To test this hypothesis, MC3T3-E1 cells were grown on glass slides coated with fibronectin and subjected to laminar fluid flow (12 dyn/cm(2)). Before application of shear, cells were treated with two Ca(2+) channel inhibitors or various blockers of intracellular Ca(2+) release for 0. 5-1 h. Although gadolinium, a mechanosensitive channel blocker, significantly reduced the [Ca(2+)](i) response, neither gadolinium nor nifedipine, an L-type channel Ca(2+) channel blocker, were able to block shear-induced stress fiber formation and increase in c-fos and COX-2 in MC3T3-E1 cells. However, 1, 2-bis(2-aminophenoxy)ethane-N,N,N',N'-tetraacetic acid-AM, an intracellular Ca(2+) chelator, or thapsigargin, which empties intracellular Ca(2+) stores, completely inhibited stress fiber formation and c-fos/COX-2 production in sheared osteoblasts. Neomycin or U-73122 inhibition of phospholipase C, which mediates D-myo-inositol 1,4,5-trisphosphate (IP(3))-induced intracellular Ca(2+) release, also completely suppressed actin reorganization and c-fos/COX-2 production. Pretreatment of MC3T3-E1 cells with U-73343, the inactive isoform of U-73122, did not inhibit these shear-induced responses. These results suggest that IP(3)-mediated intracellular Ca(2+) release is required for modulating flow-induced responses in MC3T3-E1 cells.

Non-NASA Center↗

SDU6 Interior Liner Testing & Evaluation

Two liner materials (Marseal® M-3500 and REMA Chemoline® 4CN) proposed for use as a liner inside the Saltstone Disposal Unit 6 (SDU6) were subjected to specific ASTM tests (tensile and lap-shear) after immersion in 50% and 100% simulant solutions for 1000 hours at the Savannah River Ecology Laboratory. Both liner materials exhibited good resistance to the simulant chemistry, at least based on the tests performed and the test duration/conditions imposed. In lap-shear tests, both materials failed in the base material rather than peeling apart, confirming good adhesion. The REMA 4CN bromobutyl elastomer showed superior bonding characteristics and absence of warping or delamination at the conditions tested. The Marseal M-3500 material (PVC/EVA blend with polyester reinforcement) exhibited deformation and debonding in some locations. The cause of the deformation and delamination observed in the Marseal M-3500 material is not fully known, but possibly attributed to thermomechanical stress at immersion temperatures, and the thermoplastic nature of the material. The immersion temperature (68 °C) is slightly greater than the maximum use temperature limit quoted for the Marseal M- 3500 liner (65 °C), though the basis for the service limit is unknown. The testing performed was limited in scope and only for these two liner materials. These tests were primarily performed to screen for severe incompatibility or short-term degradation in Saltstone bleedwater simulants at bounding solution temperatures. Additional testing is recommended to assess long-term performance and the overall service life of the liner.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Non-destructive Evaluation of Bonds Between Fiberglass Composite and Metal

To assess the integrity and reliability of an adhesive joint in an automotive composite component, several non-destructive evaluation (NDE) methodologies are correlated to lap shear bond strengths. A glass-fabric-reinforced composite structure was bonded to a metallic structure with a two-part epoxy adhesive. Samples were subsequently cut and tested in shear, and flaws were found in some areas. This study aims to develop a reliable and portable NDE system for service-level adhesive inspection in the automotive industry. The results of the experimental investigation using several NDE methods are presented and discussed. Fiberglass-to-metal bonding is the ideal configuration for NDE via thermography using excitation with induction heating, due to the conductive metal and non-conductive glass-fiber-reinforced composites. Excitation can be either by a research-grade induction heater of highly defined frequency and intensity, or by a service-level heater, such as would be used for sealing windshields in a body shop. The thermographs thus produced can be captured via a high-resolution infrared camera, with principal component analysis and 2D spatial Laplacian processing. Alternatively, the thermographs can be captured by low resolution thermochromic microencapsulated liquid crystal film imaging, which needs no post-processing and can be very inexpensive. These samples were also examined with phased-array ultrasound. The NDE methods are compared to the lap shear values and to each other for approximate cost, accuracy, and time and level of expertise needed.

Zhao, Selina↗

The production of turbulent stress in a shear flow by irrotational fluctuations

Attention is given to the way in which external turbulence affects an initially turbulence-free region in which there is a mean velocity gradient. External turbulence induces irrotational fluctuations in the sheared region which interact with the shear to produce rotational velocity fluctuations and mean Reynolds stresses. Since the actual front between the initial external turbulence and the shear flow is a randomly contorted surface, the turbulence near the front is intermittent, and is presently included in the form of a simple statistical model. In wind tunnel tests, turbulent shear stress was found to grow from zero to significant values in the interaction region. Observed stress magnitude and extent agrees with predictions, and it is concluded that turbulent stresses can be produced by irrotational fluctuations in a region of mean shear.

Gartshore, I. S.↗

Composite materials: Testing and design

The present conference discusses topics in the analysis of composite structures, composite materials' impact and compression behavior, composite materials characterization methods, composite failure mechanisms, NDE methods for composites, and filament-wound and woven composite materials' fabrication. Attention is given to the automated design of a composite plate for damage tolerance, the effects of adhesive layers on composite laminate impact damage, instability-related delamination growth in thermoset and thermoplastic composites, a simple shear fatigue test for unidirectional E-glass epoxy, the growth of elliptic delaminations in laminates under cyclic transverse shear, and the mechanical behavior of braided composite materials.

Whitcomb, John D.↗

Advanced beaded and tubular structural panels.

A review is presented of an NASA program to develop light-weight beaded and tubular structural panels which can be applied where beaded external surfaces are acceptable aerodynamically or where primary structure is protected by heat shields. The design shapes were obtained with an optimization computer code which iterates geometric parameters to satisfy strength, stability and weight constraints. Methods of fabricating these new configurations are discussed. Nondestructive testing produced extensive combined compression, shear and bending test data on local buckling specimens and large panels. The optimized design concepts offer 25 to 40% weight savings compared to conventional stiffened sheet construction.

Musgrove, M. D.↗