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At least 397 records · Page 22

Fracture of single crystals of the nickel-base superalloy PWA 1480E in helium at 22 C

The fracture behavior and deformation of He-charged (at 22 C) single crystals of PWA 1480E Ni-base superalloy were investigated using SEM and TEM techniques to observe the behavior of tensile fractures in notched single crystals with seven different crystal growth orientations: 100-line, 110-line, 111-line, 013-line, 112-line, 123-line, and 223-line. To identify the cleavage plane orientation, a stereoscopic technique, combined with the use of planar gamma-prime morphologies, was applied. It was found that gamma-prime particles were orderly and closely aligned with edges along the 100-line, 010-line, and 001-line-oriented directions of the gamma matrix. Different crystal growth orientations were found not to affect the morphology of gamma-prime particles. The accumulation of dislocations around gamma/gamma-prime interfaces formed strong barriers to subsequent dislocation movement and was the primary strengthening mechanism at room temperature.

Chen, P. S.↗

The long term stability of VLBI earth orientation measurements

Tectonic motions will, in general, change the orientation as well as the length of baselines used in Very Long Baseline Interferometry (VLBI), and will thus cause slow divergences between earth orientation results obtained with different VLBI networks, as well as between VLBI results and those obtained by satellite laser ranging and lunar laser ranging. Such drifts (on the order of a milliarcsecond/year) are inherently interesting as well as being significant in combinations of orientation results from different sources. The geodetic study of tectonic motions is also closely connected to research into the nature and causes of systematic errors in data from the modern techniques of space geodesy. Both a special coordinate system found to be of use in the analysis of VLBI data and tectonic motion estimates for a VLBI baseline stretching from California to Australia are described.

Eubanks, T. M.↗

Investigation of ZnSe-coated silicon substrates for GaAs solar cells

Studies are being carried out to determine the feasibility of using ZnSe as a buffer layer for GaAs solar cells grown on silicon. This study was motivated by reports in the literature indicating ZnSe films had been grown by metallorganic chemical vapor deposition (MOCVD) onto silicon with EPD values of 2 x 10(exp 5) cm(sup -2), even though the lattice mismatch between silicon and ZnSe is 4.16 percent. These results combined with the fact that ZnSe and GaAs are lattice matched to within 0.24 percent suggest that the prospects for growing high efficiency GaAs solar cells onto ZnSe-coated silicon are very good. Work to date has emphasized development of procedures for MOCVD growth of (100) ZnSe onto (100) silicon wafers, and subsequent growth of GaAs films on ZnSe/Si substrates. In order to grow high quality single crystal GaAs with a (100) orientation, which is desirable for solar cells, one must grow single crystal (100) ZnSe onto silicon substrates. A process for growth of (100) ZnSe was developed involving a two-step growth procedure at 450 C. Single crystal, (100) GaAs films were grown onto the (100) ZnSe/Si substrates at 610 C that are adherent and specular. Minority carrier diffusion lengths for the GaAs films grown on ZnSe/Si substrates were determined from photoresponse properties of Al/GaAs Schottky barriers. Diffusion lengths for n-type GaAs films are currently on the order of 0.3 microns compared to 2.0 microns for films grown simultaneously by homoepitaxy.

Huber, Daniel A.↗

Detection of uncompensated magnetization at the interface of an epitaxial antiferromagnetic insulator

We have probed directly the temperature and magnetic field dependence of pinned uncompensated magnetization at the interface of antiferromagnetic FeF 2 with Cu, using FeF 2 -Cu-Co spin valves. Electrons polarized by the Co layer are scattered by the pinned uncompensated moments at the FeF 2 -Cu interface giving rise to giant magnetoresistance. We determined the direction and magnitude of the pinned uncompensated magnetization at different magnetic fields and temperatures using the angular dependencies of resistance. The strong FeF 2 anisotropy pins the uncompensated magnetization along the easy axis independent of the cooling field orientation. Most interestingly, magnetic fields as high as 90 kOe cannot break the pinning at the FeF 2 -Cu interface. This proves that the pinned interfacial magnetization is strongly coupled to the antiferromagnetic order inside the bulk FeF 2 layer. Studies as a function of FeF2 crystalline orientation show that uncompensated spins are only detected in a spin valve with (110) crystal orientation, but not in valves containing FeF 2 (100) and FeF 2 (001). This observation is in agreement with symmetry-related considerations which predict the equilibrium boundary magnetization for the FeF 2 (110) layer.

36 MATERIALS SCIENCE↗

Leaf-shape effects in electromagnetic wave scattering from vegetation

A vegetation medium is modeled as a half-space of randomly distributed and oriented leaves of arbitrary shape. In accordance with the first-order radiative transfer theory, the backscattering coefficient for such a half-space is expressed in terms of the scattering amplitudes. For disc- or needle-shaped leaves, the generalized Rayleigh-Gans approximation is used to calculate the scattering amplitudes. This approach is valid for leaf dimensions up to the size of the incident wavelength. To examine the leaf-shape effect, elliptic discs are used to model deciduous leaves, and needles are used to model coniferous leaves. The differences between the scattering characteristics of leaves of different shapes are illustrated numerically for various orientations, frequencies, and incidence angles. It is found that the scattering characteristics of elliptic disc-shaped leaves are sensitive to the three angles of orientation and disc ellipticity. In general, both like and cross polarizations may be needed to differentiate the difference in scattering due to the shapes of the leaves.

Karam, Mostafa A.↗

Radiation of an acoustic source near the trailing edge of a wing in forward motion

The acoustic sources simulating engine or jet noise are located near the trailing edge. During landing or take-off operations the flap angle is not small. Solutions for the scattering of the acoustic sources, monopoles, dipoles or quadrupoles, by the wing with the flap at finite angle are constructed for the case that the acoustic wave length is much larger than the length of the flap but may be of the same order as the chord. For each given geometry of the flap and the position of the singularities, critical orientations of the dipoles and the quadrupoles are defined along which the noise becomes 'suppressed', i.e., the far field pressure becomes one order smaller.

Ting, L.↗

A statistical approach to the brittle fracture of a multi-phase solid

A stochastic damage model is proposed to quantify the inherent statistical distribution of the fracture toughness of a brittle, multi-phase solid. The model, based on the macrocrack-microcrack interaction, incorporates uncertainties in locations and orientations of microcracks. Due to the high concentration of microcracks near the macro-tip, a higher order analysis based on traction boundary integral equations is formulated first for an arbitrary array of cracks. The effects of uncertainties in locations and orientations of microcracks at a macro-tip are analyzed quantitatively by using the boundary integral equations method in conjunction with the computer simulation of the random microcrack array. The short range interactions resulting from surrounding microcracks closet to the main crack tip are investigated. The effects of microcrack density parameter are also explored in the present study. The validity of the present model is demonstrated by comparing its statistical output with the Neville distribution function, which gives correct fits to sets of experimental data from multi-phase solids.

Liu, W. K.↗

Development of a heterogeneous nanostructure through abnormal recrystallization of a nanotwinned Ni superalloy

This work explores the development of a heterogeneous nanostructured material through leveraging abnormal recrystallization, which is a prominent phenomenon in coarse-grained Ni-based superalloys. Additionally, through synthesis of a sputtered Inconel 725 film with a heterogeneous distribution of stored energy and subsequent aging treatments at 730°C, a unique combination of grain sizes and morphologies was observed throughout the thickness of the material. Three distinct domains are formed in the aged microstructure, where abnormally large grains are observed in-between a nanocrystalline and a nanotwinned region. In order to investigate the transitions towards a heterogeneous structure, crystallographic orientation and elemental mapping at interval aging times up to 8 h revealed the microstructural evolution and precipitation behavior. From the experimental observations and the detailed analysis of this study, the current methodology can be utilized to further expand the design space of current heterogeneous nanostructured materials.

36 MATERIALS SCIENCE↗

Grain incompatibility determines the local structure of amorphous grain boundary complexions

Amorphous grain boundary complexions lack long-range crystalline order but are not featureless, as distinct gradients in structural short-range order have been reported through their thickness. In this work, we test the hypothesis that the distribution of short-range order is determined by the confining crystals using atomistic simulations of both Cu-Zr bicrystals and a random polycrystal. Voronoi polyhedra with structures similar to that of perfect face-centered cubic serve as signatures of high structural order and are only found at the amorphous-crystalline transition regions. The density of the ordered structural motifs within a specific amorphous-crystalline transition region is found to not be directly determined by the orientation and symmetry of the grain which touches it, but rather by the incompatibility between the two confining grains. Further, ordered polyhedra density is found to be inversely related to grain incompatibility, meaning that large incompatibilities between the confining crystals lead to less order in the amorphous-crystalline transition region. The finding that the entire grain-film-grain system must be considered to understand local structure unequivocally demonstrates that amorphous complexions are not simply a collection of independent phases which happen to nucleate at a grain boundary. Rather, an amorphous grain boundary complexion is a single entity that finds a local equilibrium configuration.

36 MATERIALS SCIENCE↗

A molecular dynamics survey study of impact-induced amorphization in yttria nanoparticles

The impact of a single yttria (Y 2 O 3 ) nanoparticle onto a yttria substrate was studied as a function of particle velocity (300–1200 m/s) and diameter (5–12 nm) for three particle orientations and two substrate orientations using molecular dynamics simulations. Impacts resulted in minimal dislocation motion but extensive disordering of the crystal lattice without approaching the melting temperature. The resulting amorphous microstructure was both precisely coincident with plastic strain and retained until the end of the simulation, suggesting a deformation mechanism of amorphization-facilitated viscous flow. Further analysis revealed that the degree of amorphization depended primarily on the impact velocity and secondarily on the orientations of the particle and substrate, with significant second-order effects from variable interactions.

74 ATOMIC AND MOLECULAR PHYSICS↗

Facile alignment estimation in carbon nanotube films using image processing

Whether a macroscopic assembly of carbon nanotubes can exhibit the one-dimensional properties expected from individual nanotubes critically depends on how well the nanotubes are aligned inside the assembly. Therefore, a simple and accurate method for assessing the degree of alignment is desired for the rapid characterization of carbon nanotube films and fibers. Here, we present an end-to-end solution for determining the global and local spatial orientation of carbon nanotubes in films within a short amount of time using a fast, precise, and economical approach based on an image processing method applied to scanning electron microscopy images. Further, we first use Laplacian edge enhancement filtering for improving the appearance of edge regions, which is followed by image partitioning into multiple blocks to capture the nanoscale orientation characteristics and total variation-based image decomposition of these image blocks. We then perform a 2D-fast Fourier transform on the image decomposed textural components of these edge-enhanced image blocks to determine the orientation distribution, which is utilized to estimate the 2D nematic order parameter. To show the effectiveness of our method, we corroborated our results against results obtained with other state-of-the-art image processing and experimental techniques.

2D-FFT↗

Tuning Electronic Properties of 2D Materials Using Metal Adsorbates: Cu at WTe 2 Edges

Two-dimensional materials exhibit properties promising for novel applications. Topologically protected states at their edges can be harnessed for use in quantum devices. We use ab initio simulations to examine properties of edges in 1T'-WTe 2 monolayers, known to exhibit topological order, and their interactions with Cu atoms. Comparison of (010)-oriented edges that have the same composition but different terminations shows that, as the number of Cu atoms increases, their thermodynamically-preferred arrangement depends on the details of the edge structure. Cu atoms aggregate into a cluster at the most stable edge; while the cluster is non-magnetic, it spin-polarizes the W atoms along the edge, which removes the topological protection. At the metastable edge, Cu atoms form a chain incorporated into the WTe 2 lattice; the topological state is preserved in spite of the dramatic edge restructuring. This suggests that exploiting interactions of metal species with metastable edge terminations can provide a path towards non-invasive interfaces.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Modeling intrinsic galaxy alignment in the MICE simulation

The intrinsic alignment (IA) of galaxies is potentially a major limitation in deriving cosmological constraints from weak lensing surveys. In order to investigate this effect, we assign intrinsic shapes and orientations to galaxies in the light-cone output of the MICE simulation, spanning ~ 5000 deg 2 and reaching redshift Z = 1.4. This assignment is based on a semianalytic IA model that uses photometric properties of galaxies as well as the spin and shape of their host halos. Advancing on previous work, we include more realistic distributions of galaxy shapes and a luminosity-dependent galaxy-halo alignment. The IA model parameters are calibrated against COSMOS and BOSS LOWZ observations. The null detection of IA in observations of blue galaxies is accounted for by setting random orientations for these objects. We compare the two-point alignment statistics measured in the simulation against predictions from the analytical IA models NLA and TATT over a wide range of scales, redshifts, and luminosities for red and blue galaxies separately. We find that both models fit the measurements well at scales above 8h -1 Mpc, while TATT outperforms NLA at smaller scales. The IA parameters derived from our fits are in broad agreement with various observational constraints from red galaxies. Finally, we build a realistic source sample, mimicking DES Year 3 observations and use it to predict the IA contamination to the observed shear statistics. We find this prediction to be within the measurement uncertainty, which might be a consequence of the random alignment of blue galaxies in the simulation.

79 ASTRONOMY AND ASTROPHYSICS↗

Aerodynamic lift effect on satellite orbits

Numerical quadrature is employed to obtain orbit perturbation results from the general perturbation equations. Both aerodynamic lift and drag forces are included in the analysis of the satellite orbit. An exponential atmosphere with and without atmospheric rotation is used. A comparison is made of the perturbations which are caused by atmospheric rotation with those caused by satellite aerodynamic effects. Results indicate that aerodynamic lift effects on the semi-major axis and orbit inclination can be of the same order as the effects of atmosphere rotation depending upon the orientation of the lift vector. The results reveal the importance of including aerodynamic lift effects in orbit perturbation analysis.

Karr, G. R.↗

The P/POD project: Programmable/Pilot Oriented Display

A pilot orientated display system was developed for general aviation aircraft in order to reduce cockpit workloads. Emphasis was placed on the optimization of flight procedural aspects (i.e., interpretation of Loran data). Low cost hardware/software were utilized in the system to reduce developmental costs. Parallel development and testing were conducted on the ground (simulator) and in the air using the same hardware.

Littlefield, J. A.↗

Development of three-dimensional spatial displays using a geographically based information system

Procedures necessary for the development of a generalized three-dimensional perspective software capability in support of graphic, topographic, and color mapping of Landsat data are reviewed. The NASA Earth Resources Laboratory developed the procedures in order to facilitate the processing and analysis of disparate, geographically oriented base maps from aircraft and satellite sensors. Perspective displays are obtained through a translation of the space-viewed object to a vantage point coordinate system, followed by a rotation through two angles for alignment along the vantage line of sight, and finally a perspective transformation to yield two-dimensional displays with no hidden lines. Matrix equations for the transformations are reviewed, including scaling, and block diagrams are provided of the data and perspective software systems. The classification data plane may be mapped onto a topographic elevation data plane.

Junkin, B. G.↗

Multiple scattering of electromagnetic waves by rain

As the operating frequencies of communications systems move higher into the millimeter wave region, the effects of multiple scattering in precipitation media become more significant. In this paper, general formulations are presented for single, first-order multiple, and complete multiple scattering. Included specifically are distributions of particle size, shape, and orientation angle, as well as variation in the medium density along the direction of wave propagation. Calculations are performed for rain. It is shown that the effects of higher-order scattering are not noticeable in either attenuation or channel isolation on a dual-polarized system until frequencies of about 30 GHz are reached. The complete multiple-scattering formulation presented gives accurate results at high millimeter wave frequencies as well as including realistic medium parameter distributions. Furthermore, it is numerically efficient.

Tsolakis, A.↗

Investigations of the Mars Cratered Terrain: Smooth Plains Boundary in the Eastern Equatorial Region

As part of an ongoing study to place geologic constraints on, and to interpret the origin of the ancient cratered terrain - smooth plains boundary on Mars, structural features in the eastern hemisphere were mapped, looking at wide-scale variations in aereal percentage of crater vocer and distinctive landforms. Maps and a digitized data set for graben, scarps, ridges and elongate plateaus in the eastern hemisphere were completed for 30 deg N to 30 deg. In the equatorial region, results indicate a marked change from the N oriented ridges north of the boundary to the NW orientations of those in the inter and intracrater plains south of the boundary. The WNW orientation of the boundary itself is matched by similar orientations of graben and scraps in the southern terrain. In order to determine whether outlying plateaus and isolated knobby hills found north of the boundary are formed from material of the ancient cratered terrain, the Viking 2 approach color data were used to discriminate surface materials in the eastern hemisphere. In the southern half of the Amenthes quadrange (MC-14), several correlations exist among surficial spectral reflectance and observed geologic units. Old terrain on the eastern rim of the Isidis basin is much redder than the smooth volcanic plains on either side of the rim, even though the plains unit east of the rim is located several kilometers higher than the plains on the floor of Isidis. Based on statistics derived from the color data, the plains within Isidis were found to differ from those north of the boundary zone.

Maxwell, T. A.↗