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At least 397 records · Page 22
All sourcesNASA NTRSDOE OSTI
NASA NTRSDate not supplied

Influence of Airfoil Angle of Attack on Ice Accretion Roughness

The influence of airfoil angle attack on roughness evolution and spatial variation was investigated in the Icing Research Tunnel (IRT) at the NASA Glenn Research Center. Two airfoil models were used for the study: a 53.34-cm (21-in.) NACA 0012 model and a 152.4-cm (60-in.) HAARP-II model. For the NACA 0012, the angle of attack was varied from 0° to 3°, and the ice accretion roughness was characterized while keeping the other icing parameters such as freestream velocity, freestream stagnation temperature, accumulation parameter, and median volumetric diameter (MVD) constant. For the HAARP-II, the angle of attack was varied from -1.9°, which is the non-lifting angle of attack for the airfoil, to 3°. A series of accumulation time progression cases for the HAARP-II at 2.3° angle of attack was also performed in Appendix C and Appendix O conditions and compared to the measurements presented by McClain et al. (2018) for the non-lifting angle of attack condition. The results demonstrate the strong influence of the changing local static pressure along the surface influencing the roughness characteristics. A correlation approach for the maximum equivalent sand-grain roughness along the surface of an airfoil is presented and considers the scaled accumulation time, the stagnation point freezing fraction, and the surface pressure relative to the static and stagnation pressures of the flow. Finally, an attempt to relate the maximum roughness quantities to local pressure coefficients and local icing quantities is presented and discussed.

Icing↗
DOE OSTI2020

The diurnally-averaged aerosol direct radiative effect and the use of the daytime-mean and insolation-weighted-mean solar zenith angles

Here, this study examines the application of the daytime-mean and insolation-weighted-mean solar zenith angles to calculate the diurnally-averaged aerosol direct radiative effect (DRE), DRE DA , for observed clear-sky conditions at the Atmospheric Radiation Measurement Program (ARM) Southern Great Plains (SGP) and Tropical Western Pacific (TWP) sites. As compared with the reference calculation, the DRE DA are too strong (i.e., more negative) using daytime-mean solar zenith angles (DTMSZA) and are too weak (i.e., less negative) using insolation-weighted-mean solar zenith angles (IWMSZA). The biases in the DRE DA for DTMSZA (IWMSZA) are about -0.8 (0.7) W m -2 at the TOA and about -1.5 (0.9) W m -2 at the surface. Noting the mean TOA DRE DA of -2.85 W m -2 and the surface DRE DA of -7.09 W m -2 at SGP, the relative biases for DTMSZA (IWMSZA) are 26% (-24%) for the TOA DRE DA , and 17% (-11%) for the surface DRE DA . At TWP, the mean TOA DRE DA is -2.81 W m -2 and the surface DRE DA is -11.84 W m -2 which corresponds to relative biases for DTMSZA (IWMSZA) of 29% (-27%) for the TOA DRE DA and 15% (-9%) for the surface DRE DA . By introducing an adjusted insolation-weighted-mean solar zenith angle, the mean biases in the DRE DA at the TOA becomes -0.09 W m -2 and the biases in the DRE DA at the surface are about -0.41 W m -2 . Also presented are the effects of using the mean solar zenith angles on the shortwave (SW) upward fluxes at the TOA and SW downward fluxes at the surface in both clear-sky and pristine-clear-sky (i.e., gases only) conditions.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2025

Nonmonotonic Band Flattening near the Magic Angle of Twisted Bilayer MoTe 2

Twisted bilayer MoTe 2 (tMoTe 2 ) is an emergent platform for exploring exotic quantum phases driven by the interplay between nontrivial band topology and strong electron correlations. Direct experimental access to its momentum-resolved electronic structure is essential for uncovering the microscopic origins of the correlated topological phases therein. Here, we report angle-resolved photoemission spectroscopy measurements of tMoTe 2 , revealing pronounced twist-angle-dependent band reconstruction shaped by orbital character, interlayer coupling, and moiré potential modulation. Density functional theory captures the qualitative evolution, yet underestimates key energy scales across twist angles, highlighting the importance of electronic correlations. Notably, the hole effective mass at the 𝐾 point exhibits a nonmonotonic dependence on twist angle, peaking near 2°, consistent with band flattening at the magic angle predicted by continuum models. Via electrostatic gating and surface dosing, we further visualize the evolution of electronic structure versus doping, enabling direct observation of the conduction band minimum and confirm tMoTe 2 as a direct band gap semiconductor. These results establish a spectroscopic foundation for modeling and engineering emergent quantum phases in this moiré platform.

2D materials↗
DOE OSTI2025

Quantifying Twist Angles in Cuprate Heterostructures with Anisotropic Raman Signatures

Artificially engineered twisted van der Waals (vdW) heterostructures have unlocked new pathways for exploring emergent quantum phenomena and strongly correlated electronic states. Many of these phenomena are highly sensitive to the twist angle, which can be deliberately tuned to tailor the interlayer interactions. This makes the twist angle a critical tunable parameter, emphasizing the need for precise control and accurate characterization during device fabrication. In particular, twisted cuprate heterostructures based on Bi 2 Sr 2 CaCu 2 O 8 + x (BSCCO) have demonstrated angle-dependent superconducting properties, positioning the twist angle as a key tunable parameter. However, the twisted interface is highly unstable under ambient conditions and vulnerable to damage from conventional characterization tools such as electron microscopy or scanning probe techniques. In this work, a fully non-invasive, polarization-resolved Raman spectroscopy approach is introduced for determining twist angles in artificially stacked BSCCO heterostructures. By analyzing twist-dependent anisotropic vibrational Raman modes, particularly utilizing the out-of-plane A 1g vibrational mode of Bi/Sr at ≈116 cm −1 , clear optical fingerprints of the rotational misalignment between cuprate layers are identified. The high-resolution confocal Raman setup, equipped with polarization control and RayShield filtering down to 10 cm −1 , allows for reliable and reproducible measurements without compromising the material's structural integrity.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

Automated contact angle estimation for three-dimensional X-ray microtomography data

Multiphase flow in capillary regimes is a fundamental process in a number of geoscience applications. The ability to accurately define wetting characteristics of porous media can have a large impact on numerical models. In this paper, a newly developed automated three-dimensional contact angle algorithm is described and applied to high-resolution X-ray microtomography data from multiphase bead pack experiments with varying wettability characteristics. The algorithm calculates the contact angle by finding the angle between planes fit to each solid/fluid and fluid/fluid interface in the region surrounding each solid/fluid/fluid contact point. Results show that the algorithm is able to reliably compute contact angles using the experimental data. The in situ contact angles are typically larger than flat surface laboratory measurements using the same material. Furthermore, wetting characteristics in mixed-wet systems also change significantly after displacement cycles.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2020

A new flow pattern map for flow boiling of R410A in horizontal micro-fin tubes considering the effect of the helix angle

This paper presents an improved flow pattern map for flow boiling in horizontal micro-fin tubes considering the effect of helix angle. The proposed map is modified from the one developed for horizontal smooth tubes by Wojtan et al. (2005) and takes the early transition to annular flow due to micro-fin geometry into account. Visualization of R410A flow boiling is carried out through the transparent smooth and micro-fin tubes with 0°, 10° and 18° helix angle and plotted on the proposed map for comparison. The result shows that the flow pattern map for micro-fin tube with 0° helix angle is generally similar to that for the smooth tube. For the tube with 10° and 18° helix angle, the annular flow occurs at lower vapor quality and lower mass flux. The proposed map shows good agreements when compared with the visualization and reflects the downward shift (to lower mass flux and vapor quality conditions) of the SW-WA transition with the increase of the helix angle. In order to further validate the proposed model, the flow pattern transitions calculated from the equations are also compared with the experimental data of the micro-fin tube in literature. The results show that the modified map increase the prediction accuracy of the flow patterns in the micro-fin tube.

42 ENGINEERING↗
DOE OSTI2015

Anomalous small-angle X-ray scattering of nanoporous two-phase atomistic models for amorphous silicon–germanium alloys

The present work deals with a detailed analysis of the anomalous small-angle X-ray scattering in amorphous silicon–germanium alloy using the simulation technique. We envisage the nanoporous two-phase alloy model consisting in a mixture of Ge-rich and Ge-poor domains and voids at the nanoscale. By substituting Ge atoms for Si atoms in nanoporous amorphous silicon network, compositionally heterogeneous alloys are generated with various composition-contrasts between the two phases. After relaxing the as-generated structure, we compute its radial distribution function, and then we deduce by the Fourier transform technique its anomalous X-ray scattering pattern. Using a smoothing procedure, the computed X-ray scattering patterns are corrected for the termination errors due to the finite size of the model, allowing so a rigorous quantitative analysis of the anomalous small-angle scattering. Our simulation shows that, as expected, the anomalous small-angle X-ray scattering technique is a tool of choice for characterizing compositional heterogeneities coexisting with structural inhomogeneities in an amorphous alloy. Furthermore, the sizes of the compositional nanoheterogeneities, as measured by anomalous small-angle X-ray scattering technique, are X-ray energy independent. A quantitative analysis of the separated reduced anomalous small-angle X-ray scattering, as defined in this work, provided a good estimate of their size.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Pressure Drop with Moving Contact Lines and Dynamic Contact Angles in a Hydrophobic Round Minichannel: Visualization via Synchrotron X-ray Imaging and Verification of Experimental Correlations

In hydrophobic mini- and microchannels, slug flow with moving contact lines is typically generated under various two-phase flow conditions. There is a significant pressure drop in this flow pattern with moving contact lines, which is closely related to the dynamic contact angles. Researchers have investigated dynamic contact angles experimentally for decades, but due to the limitations of visualization techniques, these experiments have typically been conducted in low Weber number regions (We < 10 –3 ). In this study, we clearly visualized the dynamic contact angles of a liquid slug in high Weber number regions (10 –3 < We <1) via synchrotron X-ray imaging with high temporal (~1000 fps) and spatial (~ 2 μm/pixel) resolutions. We precisely measured the pressure drop with moving contact lines in a hydrophobic minichannel (inner diameter = 1.018 mm). On the basis of our experimental data, we verified previous correlations for dynamic contact angles and explored the relationship between pressure drop with moving contact lines and dynamic contact angles.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2015

Illumination angle and layer thickness influence on the photo current generation in organic solar cells: A combined simulative and experimental study

In most future organic photovoltaic applications, such as fixed roof installations, facade or clothing integration, the solar cells will face the sun under varying angles. By a combined simulative and experimental study, we investigate the mutual interdependencies of the angle of light incidence, the absorber layer thickness and the photon harvesting efficiency within a typical organic photovoltaic device. For thin absorber layers, we find a steady decrease of the effective photocurrent towards increasing angles. For 90-140 nm thick absorber layers, however, we observe an effective photocurrent enhancement, exhibiting a maximum yield at angles of incidence of about 50°. Both effects mainly originate from the angle-dependent spatial broadening of the optical interference pattern inside the solar cell and a shift of the absorption maximum away from the metal electrode.

14 SOLAR ENERGY↗
DOE OSTI2015

SU-E-T-494: Influence of Proton Track-Cell Nucleus Incidence Angle On Relative Biological Effectiveness

Purpose: To explain a Monte Carlo (MC) simulation artifact whereby differences in relative biological effectiveness (RBE) in the induction of initial double strand breaks are observed as a function of the proton track incidence angles in a geometric cell nucleus model. Secondly, to offer an alternative isotropic irradiation procedure to mitigate this effect. Methods: MC tracks of 1 MeV protons were generated in an event-by-event mode. They were overlaid on a cylindrical model of a cell nucleus containing 6×109 nucleotide base pairs. The tracks incidence angle θ with respect to the cell nucleus’s axis was varied in 10 degrees intervals, each time generating one hundred fractions of ∼2 Gy. Strand breaks were scored in the modeled DNA sugar-phosphate groups and further sub-classified into single or double strand breaks (ssbs or dsbs). For each angle, an RBE for the induction of initial dsbs with reference to Co-60 was calculated. Results: Our results show significant angular dependencies of RBE, with maximum values for incidence angles parallel to the nucleus central axis. Further examination shows that the higher cross-sections for the creation of dsbs is due to the preferential alignment of tracks with geometrical sub-parts of the cell nucleus model, especially the nucleosomes containing the sugar-phosphate groups. To alleviate the impact of this simulation artifact, an average RBE was calculated with a procedure based on a weighted sampling of the angular data. Conclusion: This work demonstrates a possible numerical artifact in estimated RBE if the influence of the particle incidence angle is not correctly taken into account. A correction procedure is presented to better conform the simulations to real-life experimental conditions. We would like to acknowledge support from the Fonds de recherche du Quebec Sante (FRQS), from the CREATE Medical Physics Research Training Network grant (number 432290) of NSERC, support from NSERC under grants RGPIN 397711-11 and RGPIN-2014-06475 and support from the CIHR under grants MOP-114910, MOP-136774 and MOP-102550.

60 APPLIED LIFE SCIENCES↗
NASA NTRS1994

(abstract) Observation by Clementine of a Hugh Opposition Surge on the Moon at Very Small Solar Phase Angles

The Clementine mission enabled the first quantative observations of the Moon at very small solar phase angles. It is well established from Earth-based observations that the Moon exhibits a non-linear increase in brightness as its face becomes fully illuminated to a terrestrial observer. Because the models of the opposition effect are sensitive indicators of surfical compaction state and particle size, observations at small solar phase angles are important to obtain. A recent model for optical coherent backscatter seeks to explain a narrow opposition spike at very small phase angles (< 1 degree) seen on several icy satellites , including Europa, Icarus 90, and Oberon . Over 90 images of the Moon's surface at phase angles less than 0.5(deg) (the minimum phase angle observable from Earth due to the Moon's angular size) were obtained by the Clementine spacecraft. Our analysis of these images shows the moon exhibits a surge in brightness of approximately 20% below 0.25(deg), comparable to the values observed on icy satellites. No color dependence was detected in the lunar phase curve below 2 degrees.

partical size icy satellites Europa Icarus 90 Ober↗
NASA NTRS2016

Banded Structures in Electron Pitch Angle Diffusion Coefficients from Resonant Wave Particle Interactions

Electron pitch angle (D (alpha)) and momentum (D(pp)) diffusion coefficients have been calculated due to resonant interactions with electrostatic electron cyclotron harmonic (ECH) and whistler mode chorus waves. Calculations have been performed at two spatial locations L = 4.6 and 6.8 for electron energies 10 keV. Landau (n = 0) resonance and cyclotron harmonic resonances n = +/-1, +/-2,...+/-5 have been included in the calculations. It is found that diffusion coefficient versus pitch angle (alpha) profiles show large dips and oscillations or banded structures. The structures are more pronounced for ECH and lower band chorus (LBC) and particularly at location 4.6. Calculations of diffusion coefficients have also been performed for individual resonances. It is noticed that the main contribution of ECH waves in pitch angle diffusion coefficient is due to resonances n = +1 and n = +2. A major contribution to momentum diffusion coefficients appears from n = +2. However, the banded structures in D alpha and Dpp coefficients appear only in the profile of diffusion coefficients for n = +2. The contribution of other resonances to diffusion coefficients is found to be, in general, quite small or even negligible. For LBC and upper band chorus waves, the banded structures appear only in Landau resonance. The Dpp diffusion coefficient for ECH waves is one to two orders smaller than D alpha coefficients. For chorus waves, Dpp coefficients are about an order of magnitude smaller than D alpha coefficients for the case n does not = 0. In case of Landau resonance, the values of Dpp coefficient are generally larger than the values of D alpha coefficients particularly at lower energies. As an aid to the interpretation of results, we have also determined the resonant frequencies. For ECH waves, resonant frequencies have been estimated for wave normal angle 89 deg and harmonic resonances n = +1, +2, and +3, whereas for whistler mode waves, the frequencies have been calculated for angle 10 deg and Landau resonance. Further, in ECH waves, the banded structures appear for electron energies (is) greater than1 keV, and for whistler mode chorus waves, structures appear for energies greater than 2 keV at L = 4.6 and above 200 eV for L = 6.8. The results obtained in the present work will be helpful in the study of diffusion curves and will have important consequences for diffuse aurora and pancake distributions.

diffusion↗
NASA NTRS2021

TLSLEAF: Automatic Leaf Angle Estimates From Single-Scan Terrestrial Laser Scanning

Leaf angle distribution (LAD) in forest canopies affects estimates of leaf area, light interception, and global-scale photosynthesis, but is often simplified to a single theoretical value. Here, we present TLSLeAF (Terrestrial Laser Scanning Leaf Angle Function), an automated open-source method of deriving LADs from terrestrial laser scanning. TLSLeAF produces canopy-scale leaf angle and LADs by relying on gridded laser scanning data. The approach increases processing speed, improves angle estimates, and requires minimal user input. Key features are automation, leaf–wood classification, beta parameter output, and implementation in R to increase accessibility for the ecology community. TLSLeAF precisely estimates leaf angle with minimal distance effects on angular estimates while rapidly producing LADs on a consumer-grade machine. We challenge the popular spherical LAD assumption, showing sensitivity to ecosystem type in plant area index and foliage profile estimates that translate to c. 25% and c. 11% increases in canopy net photosynthesis (c. 25%) and solar-induced chlorophyll fluorescence (c. 11%). TLSLeAF can now be applied to the vast catalog of laser scanning data already available from ecosystems around the globe. The ease of use will enable widespread adoption of the method outside of remote-sensing experts, allowing greater accessibility for addressing ecological hypotheses and large-scale ecosystem modeling efforts.

3D↗
NASA NTRSDate not supplied

Advancements in Force and Angle Measurement by the NFMTC

The National Force Measurement Technology Capability (NFMTC) is a nationwide partnership established in 2008 and sponsored by NASA’s Aeronautics Evaluation and Test Capabilities (AETC) project to maintain and further develop force and angle measurement capabilities primarily for NASA’s ground test facilities. One of the NFMTC’s primary objectives is to develop new force and angle measurement capabilities to meet the needs of researchers testing in NASA’s ground test facilities. This work will highlight several new capabilities that are either at or near operational readiness. A new six-component flow-through balance was designed and fabricated to support an upcoming retropropulsion test campaign at the NASA Langley Unitary Plan Wind Tunnel. The balance employs membranes in place of bellows, which have historically been used, and passes the flow through load bearing parts of the balance. Flow through the balance is optimized via the addition of flow guides, which are manufactured as separate parts, and attached to the balance. Calibration of this new flow-through balance demonstrates that it can suitably characterize the load and pressure ranges it was designed for, which provides aero researchers a new tool to directly measure retropropulsion performance of powered descent vehicles. Balances used in NASA’s ground test facilities are typically either single-piece balances or floating-frame balances. Historically, these two types of balances have generally used different front-end (model) attachments. Single-piece balances generally have a cylindrical front end that is forward of any measuring sections and at a reduced diameter relative to the balance outer diameter. Floating-frame balances generally have front end fits that extend over one or more measuring sections and that engage at the balance outer diameter. Recently, the NFMTC fabricated a single-piece balance with a front end fit that is compatible with the hardware used to calibrate floating-frame balances. Calibration results evaluating this front end fit will be presented. From a recent survey of angle measurement needs, the development of smaller angle measurement packages was identified as one area of improvement. Micro-electromechanical systems (MEMS) are continually being refined to provide high performance accelerometers that are a fraction of the volume of the quartz flexure based accelerometers that are standard in wind tunnels. A survey of commercial off-the-shelf MEMS accelerometers was conducted, and it identified the Safran Colibrys MS lines to be of adequate performance. Single-axis test boards and tri-axis rigid-flex production boards were designed and fabricated with a volume of approximately .18 cubic inches. The boards were designed to provide all the necessary conditioning for the MEMS accelerometers at levels to meet or exceed all requirements for the MS line sensors. Preliminary testing of these assembled sensor packages has demonstrated acceptable performance for wind-tunnel angle measurement. Several new rotating balances are at various stages of completion for NASA Glenn Research Center’s fan drive rigs. These balances provide direct measurement of thrust and torque of a driven fan or fan section to provide an estimate of fan efficiency and net thrust. Three two-component balances have been recently completed, and one six-component balance is in active development. A custom rotating telemetry system has been developed to support testing with these balances, and the telemetry system is integrated into the forward end of each one. The telemetry system is designed to remove mechanical sliprings by using an optical ethernet-based slipring for data transmission.

Force measurement↗
DOE OSTI2020

From boundary data to bound states. Part II. Scattering angle to dynamical invariants (with twist)

We recently introduced in [9] a boundary-to-bound dictionary between gravitational scattering data and observables for bound states of non-spinning bodies. In this paper, we elaborate further on this holographic map. We start by deriving the following — remarkably simple — formula relating the periastron advance to the scattering angle: $ΔΦ(J,ε)=χ(J,ε)+χ(-J,ε)$, via analytic continuation in angular momentum and binding energy. Using explicit expressions from [9], we confirm its validity to all orders in the Post-Minkowskian (PM) expansion. Furthermore, we reconstruct the radial action for the bound state directly from the knowledge of the scattering angle. The radial action enables us to write compact expressions for dynamical invariants in terms of the deflection angle to all PM orders, which can also be written as a function of the PM-expanded amplitude. As an example, we reproduce our result in [9] for the periastron advance, and compute the radial and azimuthal frequencies and redshift variable to two-loops. Agreement is found in the overlap between PM and Post-Newtonian (PN) schemes. Last but not least, we initiate the study of our dictionary including spin. We demonstrate that the same relation between deflection angle and periastron advance applies for aligned-spin contributions, with J the (canonical) total angular momentum. Explicit checks are performed to display perfect agreement using state-of-the-art PN results in the literature. Using the map between test- and two-body dynamics, we also compute the periastron advance up to quadratic order in spin, to one-loop and to all orders in velocity. We conclude with a discussion on the generalized ‘impetus formula’ for spinning bodies and black holes as ‘elementary particles’. Our findings here and in [9] imply that the deflection angle already encodes vast amount of physical information for bound orbits, encouraging independent derivations using numerical and/or self-force methodologies.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2020

Calculating the angle between jet axes

We study the angle between i) the standard jet axis, ii) the axis of a jet which has been groomed using soft drop, with reduced sensitivity to soft radiation, iii) the jet axis obtained with the winner-take-all recombination scheme, which is insensitive to soft radiation at leading power. We calculate the distributions for these angles at next- to-leading logarithmic accuracy, including non-global logarithms. The angle between the standard and groomed jet axis directly probes soft wide-angle radiation, leading to a novel factorization formula. This angle is also very sensitive to nonperturbative physics, which is directly connected to nonperturbative contribution to the rapidity anomalous dimension for transverse momentum distributions. Comparing our predictions to Pythia we find good agreement, and we foresee applications to jet substructure in proton-proton and heavy ion collisions.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2020

On the statistical treatment of the Cabibbo angle anomaly

We point out that testing the equality of the Cabibbo angle as extracted from $\Gamma(K\rightarrow \pi l\nu)$, the ratio $\Gamma(K\rightarrow l\nu)/\Gamma(\pi\rightarrow l\nu)$ and nuclear $\beta$ decays is not identical to a test of first row unitarity of the Cabibbo-Kobayashi-Maskawa (CKM) matrix. The reason is that a CKM unitarity test involves only two parameters, while the degrees of freedom for the assessment of the goodness-of-fit of the universality of the Cabibbo angle entailed by the Standard Model (SM) is equal to the number of measurements minus one. Beyond the SM all different processes could in principle give different Cabibbo angles. Consequently, the difference between the two tests becomes relevant starting from three observables giving results for the Cabibbo angle that are in tension with each other. With current data, depending on the treatment of the nuclear $\beta$ decays, we find that New Physics is favored over the SM at $5.1\,\sigma$ or $3.6\,\sigma$ while CKM unitarity is rejected at $4.8\sigma$ or $3.0\sigma$, respectively. We argue that the best method to test the SM is to test the equality of the Cabibbo angle, because CKM unitarity is only one aspect of the SM.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2019

Through-Thickness Strain Gradient in a Hot-Rolled Al-Mg Alloy Obtained by Nanoindentation and Glancing Angle X-Ray Diffraction

Combined nanoindentation and glancing angle X-ray diffraction (GAXD) methods were used to study the mechanical properties of near-surface microstructures (NSMs) of a hot-rolled 5xxx aluminum alloy. Nanoindentations with a sharp indenter were carried out with penetration depth ranging from 250 nm to 4500 nm at the near-surface regions as well as the bulk of the hot-rolled alloy. The primary indentation parameter presented here was the hardness, given that plastic strain obtained from GAXD experiment could be correlated with the hardness value. Analysis of nanoindentation hardness results proved that NSMs of this alloy on average were harder than the bulk due to the presence of different surface features discussed here. The GAXD experiments were performed between a minimum incident angle 0.025°, equivalent to 765 nm penetration depth, and a maximum angle 1°, equivalent to 3000 nm penetration depth. The strain-induced broadening in the diffraction peaks was calculated by the Williamson–Hall technique. Both indentation hardness and glancing angle diffraction results confirmed strain gradient as a function of depth in the NSMs of the alloy. Both techniques also showed that the thickness of the subsurface layer (i.e., several micrometers below the surface) of hot-rolled sample was approximately 2.44 μm at the tested areas. Additionally, reported results provided evidence for the ability to use glancing angle X-ray diffraction as a nondestructive tool for the measurement of subsurface layers' thickness as well as microstrain (non-uniform or plastic strain) as a function of depth.

36 MATERIALS SCIENCE↗