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Alumina-containing coatings based on molybdenum (Mo), silicon (Si), and boron (B) ("MoSiB coatings") that form protective, oxidation-resistant scales on ceramic substrate at high temperatures are provided. The protective scales comprise an aluminoborosilicate glass, and may additionally contain molybdenum. Two-stage deposition methods for forming the coatings are also provided.
The Mid-Infrared Instrument (MIRI) is a 5 to 28 micron imager and spectrometer that is slated to fly aboard the JWST in 2013. Each of the flight arrays is a 1024x1024 pixel Si:As impurity band conductor detector array, developed by Raytheon Vision Systems. JPL, in conjunction with the MIRI science team, has selected the three flight arrays along with their spares. We briefly summarize the development of these devices, then describe the measured performance of the flight arrays along with supplemental data from sister flight-like parts.
The high-resolution capabilities of the Interface Region Imaging Spectrometer (IRIS) mission have allowed the exploration of the finer details of the solar magnetic structure from the chromosphere to the lower corona that have previously been unresolved. Of particular interest to us are the relatively short-lived, low-lying magnetic loops that have foot points in neighboring moss regions. These inter-moss loops have also appeared in several AIA pass bands, which are generally associated with temperatures that are at least an order of magnitude higher than that of the Si IV emission seen in the 1400 angstrom pass band of IRIS. While the emission lines seen in these pass bands can be associated with a range of temperatures, the simultaneous appearance of these loops in IRIS 1400 and AIA 171, 193, and 211 suggest that they are not in ionization equilibrium. To study these structures in detail, we have developed a series of algorithms to automatically detect signal brightening or events on a pixel-by-pixel basis and group them together as structures for each of the above data sets. These algorithms have successfully picked out all activity fitting certain adjustable criteria. The resulting groups of events are then statistically analyzed to determine which characteristics can be used to distinguish the inter-moss loops from all other structures. While a few characteristic histograms reveal that manually selected inter-moss loops lie outside the norm, a combination of several characteristics will need to be used to determine the statistical likelihood that a group of events be categorized automatically as a loop of interest. The goal of this project is to be able to automatically pick out inter-moss loops from an entire data set and calculate the characteristics that have previously been determined manually, such as length, intensity, and lifetime. We will discuss the algorithms, preliminary results, and current progress of automatic characterization.
Chemical and mineralogical analyses of several samples from Murray Formation mudstones and Stimson Formation sandstones by the Mars Science Laboratory (MSL) revealed the presence of Si-rich amorphous or poorly ordered materials. It is possible to identify the presence of high-SiO2 vs. lower SiO2 amorphous materials (e.g., basaltic glasses), based on the position of the resulting wide diffraction features in XRD patterns from the Chemistry and Mineralogy (CheMin) instrument, but it is not possible to distinguish between several candidate high-SiO2 amorphous materials such as opal-A or rhyolitic glass. In the Buckskin (BS) sample from the upper Murray Formation, and the Big Sky (BY) and Greenhorn (GH) samples from the Stimson Formation, analyses by the Sample Analysis at Mars (SAM) instrument showed very broad H2O evolutions during sample heating at temperatures >450-500degC which had not been observed from previous samples. BS also had a significant broad evolution <450-500degC. We have undertaken a laboratory study targeted at understanding if the data from SAM can be used to place constraints on the nature of the amorphous phases. SAM-like evolved gas analyses have been performed on several opal and rhyolitic glass samples. Opal-A samples exhibited wide <500degC H2O evolutions, with lesser H2O evolved above ~500degC. H2O evolution traces from rhyolitic glasses varied, having either two broad H2O peaks, <300degC and >500degC, or a broad peak centered around 400degC. For samples that produced two evolutions, the lower temperature peak is more intense than the higher temperature peak, a trend also exhibited by opal-A. This trend is consistent with data from BS, but does not seem consistent with data from BY and GH which evolved most of their H2O >500degC. It may be that dehydration of opal-A and/or rhyolitic glass can result in some preferential loss of lower temperature H2O, to produce traces that more closely resemble BY and GH. This is currently under investigation and results will be reported.
One aspect of the present invention is a double sided hybrid crystal structure including a trigonal Sapphire wafer containing a (0001) C-plane and having front and rear sides. The Sapphire wafer is substantially transparent to light in the visible and infrared spectra, and also provides insulation with respect to electromagnetic radio frequency noise. A layer of crystalline Si material having a cubic diamond structure aligned with the cubic <111> direction on the (0001) C-plane and strained as rhombohedron to thereby enable continuous integration of a selected (SiGe) device onto the rear side of the Sapphire wafer. The double sided hybrid crystal structure further includes an integrated III-Nitride crystalline layer on the front side of the Sapphire wafer that enables continuous integration of a selected III-Nitride device on the front side of the Sapphire wafer.
Under a NASA-ESA collaborative research project, three Al-7-weight-percentage Si samples (MICAST-6, MICAST-7 and MICAST 2-12) were directionally solidified aboard the International Space Station to determine the effect of mitigating convection on the primary dendrite array. The samples were approximately 25 centimeters in length with a diameter of 7.8 millimeter-diameter cylinders that were machined from [100] oriented terrestrially grown dendritic Al-7Si samples and inserted into alumina ampoules within the Sample Cartridge Assembly (SCA) inserts of the Low Gradient Furnace (LGF). The feed rods were partially remelted in space and directionally solidified to effect the [100] dendrite-orientation. MICAST-6 was grown at 5 microns per second for 3.75 centimeters and then at 50 microns per second for its remaining 11.2 centimeters of its length. MICAST-7 was grown at 20 microns per second for 8.5 centimeters and then at 10 microns per second for 9 centimeters of its remaining length. MICAST2-12 was grown at 40 microns per second for 11 centimeters. The thermal gradient at the liquidus temperature varied from 22 to 14 degrees Kelvin per centimeter during growth of MICAST-6, from 26 to 24 degrees Kelvin per centimeter for MICAST-7 and from 33 to 31 degrees Kelvin per centimeter for MICAST2-12. Microstructures on the transverse sections along the sample length were analyzed to determine nearest-neighbor spacing of the primary dendrite arms and trunk diameters of the primary dendrite-arrays. This was done along the lengths where steady-state growth prevailed and also during the transients associated with the speed-changes. The observed nearest-neighbor spacings during steady-state growth of the MICAST samples show a very good agreement with predictions from the Hunt-Lu primary spacing model for diffusion controlled growth. The observed primary dendrite trunk diameters during steady-state growth of these samples also agree with predictions from a coarsening-based model. The radial macrosegregation and "steepling" caused by thermosolutal convection during terrestrial growth of the Al-7Si was not observed in the space-grown MICAST samples.
The CLASP (Chromospheric Lyman-Alpha Spectro- Polarimeter) rocket experiment, in addition to the ultraviolet region of the Ly alpha emission line (121.57 nm), emission lines of Si III (120.65 nm) and OV (121.83 nm) is can be observed. These are optically thin line compared to a Ly alpha line, if Rarere captured its polarization, there is a possibility that dripping even a new physical diagnosis chromosphere-transition layer. In particular, OV bright light is a release from the transition layer, further, three P one to one S(sub 0) is a forbidden line (cross-triplet transition between lines), it was not quite know whether to polarization.
Ceramic environmental barrier coatings (EBC) and SiCSiC ceramic matrix composites (CMCs) will play a crucial role in future aircraft propulsion systems because of their ability to significantly increase engine operating temperatures, improve component durability, reduce engine weight and cooling requirements. Advanced EBC systems for SiCSiC CMC turbine and combustor hot section components are currently being developed to meet future turbine engine emission and performance goals. One of the significant material development challenges for the high temperature CMC components is to develop prime-reliant, environmental durable environmental barrier coating systems. In this paper, the durability and performance of advanced Electron Beam-Physical Vapor Deposition (EB-PVD) NASA HfO2-Si and YbGdSi(O) EBC bond coat top coat systems for SiCSiC CMC have been summarized. The high temperature thermomechanical creep, fatigue and oxidation resistance have been investigated in the laboratory simulated high-heat-flux environmental test conditions. The advanced NASA EBC systems showed promise to achieve 1500C temperature capability, helping enable next generation turbine engines with significantly improved engine component temperature capability and durability.
One aspect of the present invention is a double sided hybrid crystal structure including a trigonal Sapphire wafer containing a (0001) C-plane and having front and rear sides. The Sapphire wafer is substantially transparent to light in the visible and infrared spectra, and also provides insulation with respect to electromagnetic radio frequency noise. A layer of crystalline Si material having a cubic diamond structure aligned with the cubic <111> direction on the (0001) C-plane and strained as rhombohedron to thereby enable continuous integration of a selected (SiGe) device onto the rear side of the Sapphire wafer. The double sided hybrid crystal structure further includes an integrated III-Nitride crystalline layer on the front side of the Sapphire wafer that enables continuous integration of a selected III-Nitride device on the front side of the Sapphire wafer.
Background (what): SI (International System of Units)-traceable Microwave Radiometer calibration; Motivation (why): NWP (Numerical Weather Prediction), FCDR (Fundamental Climate Data Record); Technology (how): NIST (National Inst. of Standards and Technology) blackbody target for ; Standards: Status & Future Plans. Development of a National Standard for Microwave Brightness Temperature (TB) at NIST.
Metallic core formation in differentiated bodies in the inner solar system can takeplace between low pressures (near 1 bar) to much higher pressures (up to 100 GPa). Mostthermodynamic models of metal-silicate equilibria utilize activity coefficients for metallic tracersin Fe liquids, nearly all of which have been carried out at low pressures. This study focuses onthe effect of pressure on activity coefficients for Au, P, V, Mn, Ga, Zn, Cd, Sn, W, Pb, and Nb inliquid Fe-Si alloys. From a series of experiments at 10 GPa, 2373 K containing variable Sicontent in a metallic liquid we have derived epsilon interaction parametersin FeSi liquids (εMSi). Comparison of 1 GPa and 10 GPa data shows no difference except for Nb. Epsilonparameters derived from low pressure experiments can thus be used to calculate activitycoefficients for application to higher pressure processes (at least to 10 GPa).
Ballistic-electron-emission microscopy has been used to investigate the effects of strain on Si l-x Ge x alloys. Lifting of the degeneracy of the conduction-band minimum of SiGe due to lattice deformation has been directly measured by application of BEEM spectroscopy to Ag/Si structures.
We present measurements of prototype thin film Al microwave kinetic inductance detectors (MKIDs) intended for application in the sub-mm astronomy balloon experiment EXCLAIM. The device we show is dark, or non-optically coupled, and contains 16 coplanar waveguide (CPW) resonators etched into a 261 nm sputter deposited Al layer on a Si wafer. The resonators span the f0 = 3.5 - 4 GHz range, and include both lambda=2 and lambda=4 resonators. Each resonator is coupled to the feedline using one of three alternating coupling designs. We performed transmission line measurements of the device for a series of excitation powers ranging from -90 dBm to -30 dBm, and at a series of base temperatures ranging from 73 mK to 400 mK. We observed quality factors of up to Qi 107 at a base temperature of 73 mK. The lambda=2 and lambda=4 resonators performed similarly, achieving comparable Qi values. The results of these measurements are actively informing the fi nal design of the EXCLAIM instrument. EXCLAIM will incorporate six spectrometers, each containing an array of over 300 resonators in the 420-540 GHz range.
Using 3-D finite difference time domain (FDTD) modeling, it is shown that micro-cone arrays obtained by anisotropic wet etching of Si have high potential for concentrating light on compact photodetector mesas of mid-wave infrared (MWIR) focal plane arrays (FPAs). The proposed structures can be heterogeneously integrated with FPAs possessing high quantum efficiency. They can be used to reduce the thermal noise and, potentially, increase the operating temperature of FPAs while maintaining high sensitivity of the photodetectors.
In the present paper, we use Si IV 1393.755 Å spectral line observed by the Interface Region Imaging Spectrograph (IRIS) in the quiet-Sun to determine physical nature of the solar transition region (TR) oscillations. We analyze the properties of these oscillations using wavelet tools (e.g., power, cross-power, coherence, and phase difference) along with the stringent noise model (i.e., power-law + constant). We estimate the period of the intensity and Doppler velocity oscillations at each chosen location in the quiet-Sun (QS) and quantify the distribution of the statistically significant power and associated periods in one bright and two dark regions. In the bright TR region, the mean periods in intensity and velocity are 7 min, and 8 min respectively. In the dark region, the mean periods in intensity and velocity are 7 min, and 5.4 min respectively. We also estimate the phase difference between the intensity and Doppler velocity oscillations at each location. The statistical distribution of phase difference is estimated, which peaks at -119°± 13°, 33°± 10°, 102°± 10° in the bright region, while at -153°± 13°, 6°± 20°, 151°± 10° in the dark region. The statistical distribution reveals that the oscillations are caused by propagating slow magnetoacoustic waves encountered with the TR. Some of these locations may also be associated with the standing slow waves. Even, in the given time domain, several locations exhibit presence of both propagating and standing oscillations at different frequencies.
In this paper, we use the Si IV 1393.755 Å spectral line observed by the Interface Region Imaging Spectrograph (IRIS) in the quiet-Sun (QS) to determine the physical nature of the solar transition region (TR) oscillations. We analyse the properties of these oscillations using wavelet tools (e.g. power, cross-power, coherence, and phase difference) along with the stringent noise model (i.e. power law + constant). We estimate the period of the intensity and Doppler velocity oscillations at each chosen location in the QS and quantify the distribution of the statistically significant power and associated periods in one bright region and two dark regions. In the bright TR region, the mean periods in intensity and velocity are 7 min and 8 min, respectively. In the dark regions, the mean periods in intensity and velocity are 7 min and 5.4 min, respectively. We also estimate the phase difference between the intensity and Doppler velocity oscillations at each location. The statistical distribution of the phase difference is estimated, which peaks at −119° ± 13°, 33° ± 10°, 102° ± 10° in the bright region and at −153° ± 13°, 6° ± 20°, 151° ± 10° in the dark regions. The statistical distribution reveals that the oscillations are caused by propagating slow magneto-acoustic waves encountered with the TR. Some of these locations may also be associated with standing slow waves. Moreover, in the given time domain, several locations exhibit the presence of both propagating and standing oscillations at different frequencies.
It is shown that due to high speed and large volume of production, anisotropic wet etching of Si is a unique method of manufacturing high quality micropyramidal arrays for silicon photonics. Four types of arrays were fabricated: (i) square pyramids with the 54.7 slope of the sidewall surface, (ii) microcones with the 45 slope of sidewall surface, (iii) inverted square pyramids with 54.7 slope, and (iv) inverted triangular pyramids with different angles of the sidewalls. It is shown that the first type of arrays has a capability to produce tightly focused mid-wave infrared (MWIR) beams at the tips of the pyramids. Other arrays can be also used as light concentrators and various multifunctional microphotonic components.
The Climate Absolute Radiance and Refractivity Observatory (CLARREO) Pathfinder (CPF) consists of an Earthviewing reflected solar (RS) spectrometer that will measure the Earth-reflected solar radiation from International Space Station with an SI-traceable radiometric uncertainty of 0.3% (1-sigma). The high-accuracy CPF measurements will provide an in-orbit reference for intercalibrating other spaceflight RS instruments. The CPF intercalibration team has been tasked to develop a state-of-the-art approach to calibrate the shortwave channel (300-5000 nm) of the Clouds and the Earth’s Radiant Energy System (CERES) instrument and the reflective solar bands (RSB) of the Visible Infrared Imaging Radiometer Suite (VIIRS) instrument, both onboard the NOAA-20 satellite, against the CPF benchmark measurements. The aimed intercalibration methodology uncertainty for both the target instruments is also 0.3%. To meet this stringent intercalibration accuracy, the CPF team has developed methods for mitigating the impacts of spatial, spectral, and angular differences between the intercalibration footprints from the CPF and target instruments. To further alleviate uncertainty, the CPF team will employ Polarization Distribution Models (PDMs) to characterize the polarization state of the Earth-reflected radiance as a function of the intercalibration footprint scene type, solar and viewing geometry, and wavelength. The PDMs will assist in identifying low-polarized scene radiances for meticulously intercalibrating the polarization sensitive VIIRS instrument against the significantly-less polarization-sensitive CPF instrument. This paper will highlight the CPF mission overview, the details of the CPF intercalibration approach, and additional outcomes of the CPF intercalibration studies that may benefit the broader remote sensing community.community.