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DOE OSTI2022

Soil resistance and recovery during neotropical forest succession

The recovery of soil conditions is crucial for successful ecosystem restoration and, hence, for achieving the goals of the UN Decade on Ecosystem Restoration. Here, we assess how soils resist forest conversion and agricultural land use, and how soils recover during subsequent tropical forest succession on abandoned agricultural fields. Our overarching question is how soil resistance and recovery depend on local conditions such as climate, soil type and land-use history. For 300 plots in 21 sites across the Neotropics, we used a chronosequence approach in which we sampled soils from two depths in old-growth forests, agricultural fields (i.e. crop fields and pastures), and secondary forests that differ in age (1–95 years) since abandonment. We measured six soil properties using a standardized sampling design and laboratory analyses. Soil resistance strongly depended on local conditions. Croplands and sites on high-activity clay (i.e. high fertility) show strong increases in bulk density and decreases in pH, carbon (C) and nitrogen (N) during deforestation and subsequent agricultural use. Resistance is lower in such sites probably because of a sharp decline in fine root biomass in croplands in the upper soil layers, and a decline in litter input from formerly productive old-growth forest (on high-activity clays). Soil recovery also strongly depended on local conditions. During forest succession, high-activity clays and croplands decreased most strongly in bulk density and increased in C and N, possibly because of strongly compacted soils with low C and N after cropland abandonment, and because of rapid vegetation recovery in high-activity clays leading to greater fine root growth and litter input. Furthermore, sites at low precipitation decreased in pH, whereas sites at high precipitation increased in N and decreased in C : N ratio. Extractable phosphorus (P) did not recover during succession, suggesting increased P limitation as forests age. These results indicate that no single solution exists for effective soil restoration and that local site conditions should determine the restoration strategies.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2021

Origin and limit of the recovery of damaged information by time reversal

Recently it was found that scrambled information can be partially recovered by a time-reversed evolution, even after being damaged by an intruder. Here we reconsider the origin of the information recovery, and argue that the presence of classical chaos does not preclude it and only leads to a quantitative reduction of the recovery ratio. We also show how decoherence (i.e., entanglement with the intruder) limits the recovery, by proving an upper bound on the recovery ratio in terms of the entangling power of the intruder's action.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2019

Analysis of Diode Reverse Recovery Effect on ZVS Condition for GaN-Based LLC Resonant Converter

LLC resonant converter can achieve zero voltage switching (ZVS) for primary-side devices and zero current switching (ZCS) for secondary-side rectifiers. However, the reverse recovery and junction capacitance (C j ) of secondary-side diode critically affect the ZVS condition of primary-side switches. The effect of C j has been discussed in literature, but not the reverse recovery. In this paper, the reverse recovery charge (Q rr ) is converted to an equivalent capacitance (C rr_eq ) for the study of primary-side ZVS performance. An accurate model during deadtime is derived and further applied to characterize ZVS performance with different reverse recovery charges in different regions. The concept of establishing parameter C total to consider both C j and C rr_eq is proposed to evaluate the effect of the secondary-side rectifiers. This concept provides the guideline for diode and synchronous rectification MOSFET selection to ensure ZVS condition for LLC converters. To verify the concept and the derived model,a 200/400 V 400 W LLC resonant converter prototype operating from 200 to 700 kHz is built and its ZVS performances with different diodes are compared. Two issues caused by Q rr effect, including V ds reverse charging and asymmetrical waveform during deadtime, are explained thoroughly as well.

42 ENGINEERING↗

DOE OSTI2015

Toward an integrated monitoring framework to assess the effects of tropical forest degradation and recovery on carbon stocks and biodiversity

Tropical forests harbor a significant portion of global biodiversity and are a critical component of the climate system. Reducing deforestation and forest degradation contributes to global climate-change mitigation efforts, yet emissions and removals from forest dynamics are still poorly quantified. We reviewed the main challenges to estimate changes in carbon stocks and biodiversity due to degradation and recovery of tropical forests, focusing on three main areas: (1) the combination of field surveys and remote sensing; (2) evaluation of biodiversity and carbon values under a unified strategy; and (3) research efforts needed to understand and quantify forest degradation and recovery. The improvement of models and estimates of changes of forest carbon can foster process-oriented monitoring of forest dynamics, including different variables and using spatially explicit algorithms that account for regional and local differences, such as variation in climate, soil, nutrient content, topography, biodiversity, disturbance history, recovery pathways, and socioeconomic factors. Generating the data for these models requires affordable large-scale remote-sensing tools associated with a robust network of field plots that can generate spatially explicit information on a range of variables through time. By combining ecosystem models, multiscale remote sensing, and networks of field plots, we will be able to evaluate forest degradation and recovery and their interactions with biodiversity and carbon cycling. In conclusion, improving monitoring strategies will allow a better understanding of the role of forest dynamics in climate-change mitigation, adaptation, and carbon cycle feedbacks, thereby reducing uncertainties in models of the key processes in the carbon cycle, including their impacts on biodiversity, which are fundamental to support forest governance policies, such as Reducing Emissions from Deforestation and Forest Degradation.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2019

Anisohydric behavior linked to persistent hydraulic damage and delayed drought recovery across seven North American tree species

Summary The isohydry‐anisohydry spectrum has become a popular way to characterize plant drought responses and recovery processes. Despite the proven utility of this framework for understanding the interconnected physiological changes plants undergo in response to water stress, new challenges have arisen pertaining to the traits and tradeoffs that underlie this concept. To test the utility of this framework for understanding hydraulic traits, drought physiology and recovery, we applied a 6 wk experimental soil moisture reduction to seven tree species followed by a 6 wk recovery period. Throughout, we measured hydraulic traits and monitored changes in gas exchange, leaf water potential, and hydraulic conductivity. Species’ hydraulic traits were not coordinated, as some anisohydric species had surprisingly low resistance to embolism (P 50 ) and negative safety margins. In addition to widespread hydraulic damage, these species also experienced reductions in photosynthesis and stem water potential during water stress, and delayed recovery time. Given that we observed no benefit of being anisohydric either during or after drought, our results indicate the need to reconsider the traits and tradeoffs that underlie anisohydric behavior, and to consider the environmental, biological and edaphic processes that could allow this strategy to flourish in forests.

Kannenberg, Steven A.↗

DOE OSTI2025

Dynamic in vivo monitoring of granum structural changes of Ctenanthe setosa (Roscoe) Eichler during drought stress and subsequent recovery

Investigating the effects of drought stress and subsequent recovery on the structure and function of chloroplasts is essential to understanding how plants adapt to environmental stressors. We investigated Ctenanthe setosa (Roscoe) Eichler, an ornamental plant that can tolerate prolonged drought periods (40 and 49 days of water withdrawal). Conventional biochemical, biophysical, physiological and (ultra)structural methods combined for the first time in a higher plant with in vivo small-angle neutron scattering (SANS) were used to characterize the alterations induced by drought stress and subsequent recovery. Upon drought stress, no significant changes occurred in the chloroplast ultrastructure, chlorophyll content, 77K fluorescence emission spectra and maximal quantum efficiency of PSII (Qy dark), but the actual quantum efficiency of PSII (Qy light) decreased, the amounts of PSI-LHCII complexes and PSII monomers declined, and that of PSII supercomplexes increased. Thickness of the leaf and of the adaxial hypodermis, chloroplast length and granum repeat distance (RD) values decreased upon drought stress, as shown by light microscopy and SANS, respectively. Because of the very slight (nm-range) changes in RD values, the large biological variability (significant differences in RD values among the leaves and studied leaf regions) and the invasive sampling required for this method, transmission electron microscopy (TEM) hardly showed significant differences. On the other side, in situ SANS analyses provided a unique insight in vivo into the fast structural recovery of the granum structure of drought-stressed leaves, which happened already 18 h after re-watering, while functional and biochemical recovery took place on a longer time scale.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2015

Modeling the Mesoscale Transport of Lithium-Magnetite Electrodes Using Insight from Discharge and Voltage Recovery Experiments

A multi-scale mathematical model, which accounts for mass transport on the crystal and agglomerate length-scales, is used to investigate the electrochemical performance of lithium-magnetite electrochemical cells. Experimental discharge and voltage recovery data are compared to three sets of simulations, which incorporate crystal-only, agglomerate-only, or multi-scale transport effects. Mass transport diffusion coefficients are determined by fitting the simulated voltage recovery times to experimental data. In addition, a further extension of the multi-scale model is proposed which accounts for the impact of agglomerate size distributions on electrochemical performance. The results of the study indicate that, depending on the crystal size, the low utilization of the active material is caused by transport limitations on the agglomerate and/or crystal length-scales. For electrodes composed of small crystals (6 and 8 nm diameters), it is concluded that the transport limitations in the agglomerate are primarily responsible for the long voltage recovery times and low utilization of the active mass. In the electrodes composed of large crystals (32 nm diameter), the slow voltage recovery is attributed to transport limitations on both the agglomerate and crystal length-scales.

25 ENERGY STORAGE↗

DOE OSTI2022

Data for Optimizing Chemical-Free Pretreatment for Maximizing Oil/Lipid Recovery from Transgenic Bioenergy Crops and its Rapid Analysis Using Time Domain-NMR

Transgenic bioenergy crops have shown the potential to produce vegetative oil by accumulating energy-rich triacylglyceride molecules that can be converted into biofuels (biodiesel and biojet). These transgenic crops cater to improved biofuel yield by providing lipids along with cellulosic sugars. Efficient bioprocessing technologies are needed to utilize these transgenic plants to their maximum potential. To this end, this study investigates a low- and high-severity chemical-free hydrothermal pretreatment of transgenic oilcane 1566 bagasse with in situ lipids to maximize the recovery of lipids for biodiesel and fermentable sugars for ethanol with minimal inhibitor generation. Hydrothermal pretreatment at 170°C recovered ∼25% of total lipids in the pretreatment liquor, leaving the remainder in bagasse residue for hexane recovery post fermentation. The recovery of lipids in pretreatment liquor remained constant beyond 170°C. Along with lipids, ∼35% w/w and ∼50% w/w fermentable sugars were recovered post saccharification from bagasse pretreated at 170°C and 210°C for 20 min, respectively. Hydrothermal pretreatment at 170°C for 20 min provided the optimum conditions for maximum recovery of lipids and cellulosic sugars that resulted in enhanced biofuel yield per unit biomass. High severity pretreatment increased the generation of inhibitors beyond the tolerance of fermentation microorganisms. In addition, the application of time-domain proton NMR spectroscopy was extended to bioprocessing. NMR technology facilitated the analysis of total lipids, the composition of fatty acids, and the characterization of free and bound lipids in untreated and pretreated oilcane 1566 bagasse subsequent to each step of biomass to biofuel conversion.

Conversion↗

DOE OSTI2013

Advanced Membrane Separation Technologies for Energy Recovery from Industrial Process Streams

Recovery of energy from relatively low-temperature waste streams is a goal that has not been achieved on any large scale. Heat exchangers do not operate efficiently with low-temperature streams and thus require such large heat exchanger surface areas that they are not practical. Condensing economizers offer one option for heat recovery from such streams, but they have not been widely implemented by industry. A promising alternative to these heat exchangers and economizers is a prototype ceramic membrane system using transport membrane technology for separation of water vapor and recovery of heat. This system was successfully tested by the Gas Technology Institute (GTI) on a natural gas fired boiler where the flue gas is relatively clean and free of contaminants. However, since the tubes of the prototype system were constructed of aluminum oxide, the brittle nature of the tubes limited the robustness of the system and even limited the length of tubes that could be used. In order to improve the robustness of the membrane tubes and make the system more suitable for industrial applications, this project was initiated with the objective of developing a system with materials that would permit the system to function successfully on a larger scale and in contaminated and potentially corrosive industrial environments. This required identifying likely industrial environments and the hazards associated with those environments. Based on the hazardous components in these environments, candidate metallic materials were identified that are expected to have sufficient strength, thermal conductivity and corrosion resistance to permit production of longer tubes that could function in the industrial environments identified. Tests were conducted to determine the corrosion resistance of these candidate alloys, and the feasibility of forming these materials into porous substrates was assessed. Once the most promising metallic materials were identified, the ability to form an alumina membrane layer on the surface of the metallic tubes was evaluated. Evaluation of this new style of membrane tube involved exposure to SO 2 containing gases as well as to materials with a potential for fouling. Once the choice of substrate and membrane materials and design were confirmed, about 150 tubes were fabricated and assembled into three modules. These modules were mounted on an industrial size boiler and their performance carefully monitored during a limited testing period. The positive results of this performance test confirm the feasibility of utilizing such a system for recovery of heat and water from industrial waste streams. The improved module design along with use of long metallic substrate tubes with a ceramic membrane on the outer surface resulted in the successful, limited scale demonstration of the Transport Membrane Condenser (TMC) technology in the GTI test facility. This test showed this technology can successfully recover a significant amount of heat and water from gaseous waste streams. However, before industry will make the investment to install a full scale TMC, a full scale system will need to be constructed, installed and successfully operated at a few industrial sites. Companies were identified that had an interest in serving as a host site for a demonstration system.

Keiser, James R.↗

DOE OSTI2012

Reuse of Produced Water from CO 2 Enhanced Oil Recovery, Coal-Bed Methane, and Mine Pool Water by Coal-Based Power Plants

Power generation in the Illinois Basin is expected to increase by as much as 30% by the year 2030, and this would increase the cooling water consumption in the region by approximately 40%. This project investigated the potential use of produced water from CO 2 enhanced oil recovery (CO 2 -EOR) operations; coal-bed methane (CBM) recovery; and active and abandoned underground coal mines for power plant cooling in the Illinois Basin. Specific objectives of this project were: (1) to characterize the quantity, quality, and geographic distribution of produced water in the Illinois Basin; (2) to evaluate treatment options so that produced water may be used beneficially at power plants; and (3) to perform a techno-economic analysis of the treatment and transportation of produced water to thermoelectric power plants in the Illinois Basin. Current produced water availability within the basin is not large, but potential flow rates up to 257 million liters per day (68 million gallons per day (MGD)) are possible if CO 2 -enhanced oil recovery and coal bed methane recovery are implemented on a large scale. Produced water samples taken during the project tend to have dissolved solids concentrations between 10 and 100 g/L, and water from coal beds tends to have lower TDS values than water from oil fields. Current pretreatment and desalination technologies including filtration, adsorption, reverse osmosis (RO), and distillation can be used to treat produced water to a high quality level, with estimated costs ranging from $2.6 to $10.5 per cubic meter ($10 to $40 per 1000 gallons). Because of the distances between produced water sources and power plants, transportation costs tend to be greater than treatment costs. An optimization algorithm was developed to determine the lowest cost pipe network connecting sources and sinks. Total water costs increased with flow rate up to 26 million liters per day (7 MGD), and the range was from $4 to $16 per cubic meter ($15 to $60 per 1000 gallons), with treatment costs accounting for 13-23% of the overall cost. Results from this project suggest that produced water is a potential large source of cooling water, but treatment and transportation costs for this water are large.

20 FOSSIL-FUELED POWER PLANTS↗

DOE OSTI2013

Recovery Act: ArcelorMittal USA Blast Furnace Gas Flare Capture

The U.S. Department of Energy (DOE) awarded a financial assistance grant under the American Recovery and Reinvestment Act of 2009 (Recovery Act) to ArcelorMittal USA, Inc. (ArcelorMittal) for a project to construct and operate a blast furnace gas recovery boiler and supporting infrastructure at ArcelorMittal’s Indiana Harbor Steel Mill in East Chicago, Indiana. Blast furnace gas (BFG) is a by-product of blast furnaces that is generated when iron ore is reduced with coke to create metallic iron. BFG has a very low heating value, about 1/10th the heating value of natural gas. BFG is commonly used as a boiler fuel; however, before installation of the gas recovery boiler, ArcelorMittal flared 22 percent of the blast furnace gas produced at the No. 7 Blast Furnace at Indiana Harbor. The project uses the previously flared BFG to power a new high efficiency boiler which produces 350,000 pounds of steam per hour. The steam produced is used to drive existing turbines to generate electricity and for other requirements at the facility. The goals of the project included job creation and preservation, reduced energy consumption, reduced energy costs, environmental improvement, and sustainability.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

DOE OSTI2019

Exploration of Ni and V Recovery from Petroleum By-Products (Abstract)

The primary objective of the project is to establish process procedures needed for the extraction and recovery of Nickel (Ni) and Vanadium (V) from U.S. petroleum wastes/by-products, with the goal of reducing U.S. dependence on imports of these materials that are critical in energy related applications. In this joint project, National Energy Technology Laboratory and Sumitomo Chemical Company, Limited, will explore Ni and V process recovery parameters based on experimental data produced in the project - information which is not available in the literature but that is necessary to determine the economic viability of the proposed separation and recovery technology. Petroleum wastes/by-products are known to contain high levels of Ni and V. The approach being taken for Ni and V recovery is based on information contained in U.S. Utility Patent Application 15/428,817.

02 PETROLEUM↗

DOE OSTI2019

Hydraulic Testing of the Lost Lake Aquifer Near Recovery Well RWM 8

Groundwater beneath the M-Area HWMF is contaminated with chlorinated ethenes including trichloroethylene (TCE) and tetrachloroethylene (PCE). SRS operates a network of recovery wells designed to hydraulically contain and capture the high concentration VOC plume in the Lost Lake Aquifer Zone (LLAZ) (Figure 1). The recovery wells are connected to the M-1 Air Stripper and the system is permitted by the South Carolina Department of Environmental Control (SCDHEC) to operate at a total flow of 610 gpm. RWM 8, which is one of ten operational recovery wells, has historically operated at a flow rate of approximately 40 gpm. RWM 8 was installed with four separate 10-ft screens that spanned the LLAZ with a continuous gravel pack spaced as shown in Figure 2. The three uppermost screens are located within the LLAZ whereas the deepest screen is located within the middle sand of the Crouch Branch Confining Unit (CBCU). Area Closure Projects (ACP) installed a permanent packer in May 2019 to isolate the lowest screen from the pump with the goal being to target the zone of highest concentration in the LLAZ. ACP expressed concern that a substantial portion of the flow from RWM 8 comes from the lower screen. With this screen isolated from service, flow from the well may be below the desired operational envelope for the well. The reconfiguration of RWM 8 presented an opportunity to re-evaluate the performance characteristics of the well. Following placement of the packer and relocation of the pump, the well was redeveloped. To assess the effects of eliminating the lower screen, a step-drawdown test was planned. The purpose of this test was to establish new baseline well performance properties including specific capacity, well efficiency, and well loss coefficients. Data from the step-drawdown testing was also used to estimate a maximum pumping rate for RWM 8 under the new configuration. The setup for the step-drawdown test facilitated a subsequent constant rate aquifer pumping test aimed at determining aquifer hydraulic properties. Properties estimated for the LLAZ included transmissivity and storativity. Following shutdown of RWM 8, recovery data were also collected and analyzed to estimate aquifer properties. This report discusses the hydrologic tests conducted following the reconfiguration of RWM 8. The information provided in this report may serve as input to subsequent updates to the groundwater flow and contaminant transport model for A/M Area.

42 ENGINEERING↗

DOE OSTI2023

Functionalized Mesoporous Carbon Materials for Effective Recovery of Rare Earth Elements from NdFeB Magnet Scrap

The increasing demand and high dependence on international supplies of rare earth elements (REEs) have prompted the US to explore alternative resources and sustainable technologies for domestic REE production. One potential resource is the secondary electronic and industrial wastes at DoD complexes and across the US. These hazardous wastes require high costs for the maintenance and remediation, but their high-REE contents offer unique opportunities for REE recovery. Current hydrometallurgical technologies for REE extraction are energy intensive and costly, with low REE recovery efficiency and the generation of hazardous secondary wastes. Thus, it is crucial to develop high efficiency and environmental-friendly technologies for REE extraction and recovery from the secondary wastes. This project aims to develop novel functionalized mesoporous carbon materials for effective recovery of REEs from NdFeB magnet scrap. The proposed novel functionalized materials will be applied in a solid-liquid separation platform that can effectively extract, recover and separate REEs from NdFeB magnet scrap (the current focus), but also from other secondary electronic/industrial wastes in the future, minimize the generation of secondary hazardous wastes, and offset the management costs for existing waste streams.

36 MATERIALS SCIENCE↗

DOE OSTI2023

End-Use Savings Shapes Measure Documentation: Variable Refrigerant Flow with Heat Recovery and Dedicated Outdoor Air System

Building on the successfully completed effort to calibrate and validate the U.S. Department of Energy's ResStock™ and ComStock™ models over the past 3 years, the objective of this work is to produce national data sets that empower analysts working for federal, state, utility, city, and manufacturer stakeholders to answer a broad range of analysis questions. The goal of this work is to develop energy efficiency, electrification, and demand flexibility end-use load shapes (electricity, gas, propane, or fuel oil) that cover a majority of the high-impact, market-ready (or nearly market-ready) measures. "Measures" refers to energy efficiency variables that can be applied to buildings during modeling. An end-use savings shape is the difference in energy consumption between a baseline building and a building with an energy efficiency, electrification, or demand flexibility measure applied. It results in a time-series profile that is broken down by end use and fuel (electricity or on-site gas, propane, or fuel oil use) at each time step. ComStock is a highly granular, bottom-up model that uses multiple data sources, statistical sampling methods, and advanced building energy simulations to estimate the annual subhourly energy consumption of the commercial building stock across the United States. The baseline model intends to represent the U.S. commercial building stock as it existed in 2018. The methodology and results of the baseline model are discussed in the final technical report of the End-Use Load Profiles project. This documentation focuses on a single heating, ventilation, and air-conditioning (HVAC) end-use savings shape measure - a variable refrigerant flow with heat recovery (VRF HR) heating and cooling system coupled with a dedicated outdoor air system (DOAS) for ventilation. This measure replaces existing multi-zone variable air volume (VAV) systems or single-zone rooftop units (RTU) with a VRF HR system coupled with a DOAS that includes an energy/heat recovery ventilator (E/HRV). The measure covers 53% of exisiting building stock's floor area and is not applicable to HVAC system types using district heating or cooling or buildings/spaces that include high-ventilation spaces such as kitchens where the amount of exhaust air is large. A DOAS with E/HRV is used to provide required outdoor ventilation air to spaces since ventilation air is generally not supplied by a VRF HR system. An exhaust air energy recovery ventilator (ERV ) with sensible and latent heat exchange is added to humid climate zones while a heat recovery ventilator (HRV ) with sensible only exchange is added to drier climate zones. The ERV is modeled as a fixed membrane plate counterflow heat exchanger, while the HRV is modeled as a sensible-only fixed aluminum plate counterflow heat exchanger. Both systems include a bypass (for temperature control and economizer lockout) and minimum exhaust temperature control for frost prevention.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

DOE OSTI2024

IB3A Helium Recovery System

An evaluation of the Fermilab's helium cryogenics test facilities has identified a pressing need for a helium recovery system in the Technical Division's Industrial Building 3a (IB3A). The IB3A facility, which plays a crucial role in testing components for various research projects, including the High-Luminosity LHC Accelerator Upgrade and Mu2e, currently vents helium into the air. Implementing recovery practices is essential due to helium's non-renewable nature and the goal of sustaining the Fermilab's scientific operations long-term. This poster covers benefits helium recovery for Fermilab and highlights the most important aspects of current helium recovery effort.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2024

Characterization Inform Sustainable Recovery of Critical Minerals from Fossil Energy Waste Feedstocks

Rare earth elements (REE) and other critical minerals (CM, e.g., Co, Ni, Li) have important uses in green energy and modern technologies, yet are vulnerable to potential supply chain disruptions. One potential domestic CM source is fossil energy wastes, such as acid mine drainage (AMD) and treatment solids (AMD solids), coal combustion ash, and Oil and Gas (O&G) drilling wastes (drill cuttings and produced waters). While they can contain lower CM concentrations then traditional ore, the quantity and fast availability as waste feedstock makes them a promising CM resource. To explore their promise, researchers at DOE’s National Energy Technology Laboratory (NETL) have collected and analyzed CM data for aforementioned fossil energy wastes, and utilized advanced geochemical characterization (e.g., synchrotron microprobe and sequential extraction) to identify the CM speciation and binding environments, and developed sustainable and targeted CM recovery. Successful examples include: (1) the discovery of easily mobile REE phases in Ca-rich coal combustion ash and developing a patented REE recovery process from Ca-rich Powder River Basin coal ash; (2) the successful identification of REE/Co/Ni/Zn hosting phases in acid mine drainage treatment solids (AMD solids) with diverse chemical composition (Al, Mn, or Fe-rich) informing the sequential recovery of different REE/CMs from AMD solids; (3) the recovery potential of Li and other CMs in O&G produced waters and drill cuttings. The innovations driven by characterization have the potential to offset the cost of waste management and wastewater treatments while reducing the cost and environmental footprint of CM extraction.

Stuckman, Mengling↗

DOE OSTI2025

Resource Recovery for the Wastewater Industry

This information sheet discusses the technology pillar, Resource Recovery, as a pathway toward improving wastewater infrastructure sustainability and resiliency. To supplement existing literature on current technologies and policies for improving resiliency at wastewater (WW) treatment plants, this document aims to accomplish the following: • Summarize wastewater sludge recovery methods • Summarize biogas production and codigestion methods • Serve as a comprehensive (though not exhaustive) repository for resource recovery for wastewater utilities The Resource Recovery Technical Information Sheet should be viewed as a general guide to established best practices for the water and wastewater (W/WW) sector when considering implementing energy capture technologies. Additional details on associated energy capture avenues such as combined heat and power (CHP), renewable energy, and inline hydropower from tertiary effluent in W/WW facilities are presented in the Energy Capture Technology Information Sheet.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗