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NASA NTRS1984

Laser-induced volatilization and ionization of microparticles

A method for the laser vaporization and ionization of individual micron-size particles is presented whereby a particle is ionized by a laser pulse while in flight in the beam. Ionization in the beam offers a real-time analytical capability and eliminates any possible substrate-sample interferences during an analysis. An experimental arrangement using a high-energy Nd-YAG laser is described, and results are presented for ions generated from potassium biphthalate particles (1.96 micron in diameter). The method proposed here is useful for the chemical analysis of aerosol particles by mass spectrometry and for other spectroscopic and chemical kinetic studies.

Sinha, M. P.↗

NASA NTRS1994

Determination of the Residence Time of Food Particles During Aseptic Sterilization

The paper describes a non-invasive method to measure the time an individual particle takes to move through a length of stainless steel pipe. The food product is in two phase flow (liquids and solids) and passes through a pipe with pressures of approximately 60 psig and temperatures of 270-285 F. The proposed problem solution is based on the detection of transitory amplitude and/or phase changes in a microwave transmission path caused by the passage of the particles of interest. The particles are enhanced in some way, as will be discussed later, such that they will provide transitory changes that are distinctive enough not to be mistaken for normal variations in the received signal (caused by the non-homogeneous nature of the medium). Two detectors (transmission paths across the pipe) will be required and place at a known separation. A minimum transit time calculation is made from which the maximum velocity can be determined. This provides the minimum residence time. Also average velocity and statistical variations can be computed so that the amount of 'over-cooking' can be determined.

Carl, J. R.↗

NASA NTRS2000

Forward Monte Carlo Computations of Polarized Microwave Radiation

Microwave radiative transfer computations continue to acquire greater importance as the emphasis in remote sensing shifts towards the understanding of microphysical properties of clouds and with these to better understand the non linear relation between rainfall rates and satellite-observed radiance. A first step toward realistic radiative simulations has been the introduction of techniques capable of treating 3-dimensional geometry being generated by ever more sophisticated cloud resolving models. To date, a series of numerical codes have been developed to treat spherical and randomly oriented axisymmetric particles. Backward and backward-forward Monte Carlo methods are, indeed, efficient in this field. These methods, however, cannot deal properly with oriented particles, which seem to play an important role in polarization signatures over stratiform precipitation. Moreover, beyond the polarization channel, the next generation of fully polarimetric radiometers challenges us to better understand the behavior of the last two Stokes parameters as well. In order to solve the vector radiative transfer equation, one-dimensional numerical models have been developed, These codes, unfortunately, consider the atmosphere as horizontally homogeneous with horizontally infinite plane parallel layers. The next development step for microwave radiative transfer codes must be fully polarized 3-D methods. Recently a 3-D polarized radiative transfer model based on the discrete ordinate method was presented. A forward MC code was developed that treats oriented nonspherical hydrometeors, but only for plane-parallel situations.

Battaglia, A.↗

NASA NTRS1990

Magnetic particle inspection

The purpose of this experiment is to familiarize the student with magnetic particle inspection and relate it to classification of various defects. Magnetic particle inspection is a method of detecting the presence of cracks, laps, tears, inclusions, and similar discontinuities in ferromagnetic materials such as iron and steel. This method will most clearly show defects that are perpendicular to the magnetic field. The Magnaglo method uses a liquid which is sprayed on the workpiece to be inspected, and the part is magnetized at the same time. The workpiece is then viewed under a black light, and the presence of discontinuity is shown by the formation of a bright indication formed by the magnetic particles over the discontinuity. The equipment and experimental procedures are described.

Sastri, Sankar↗

NASA NTRSDate not supplied

Exploration of Particle Size Engineering and Microencapsulation Technologies for Multifunctional Applications

There is a critical need for high performance materials for functional and space-based applications, including tires for exploratory rovers and external structures for landing vehicles. Novel ternary borides, such as iron aluminum boride (Fe2AlB2) and molybdenum aluminum boride (MoAlB), have emerged as potential materials for such application owing to their hardness, mechanical behavior and oxidation resistance. In this poster presentation, we will present different methods of fabricating these particles and engineering them for additive manufacturing and other related manufacturing practices. As an integral component of this study, we will demonstrate technologies to (a) synthesize these particles and (b) microencapsulate these particles with bioplastics like polylactic acid (PLA). The resulting particles will be evaluated for their processability as coatings on hydroxyapatite and Inconel particles using microstructural and flowability studies. It is expected that these particles can be used for 3D printing.

ceramics↗

NASA NTRS1975

Comparison of two methods of performing the Thellier experiment

Two methods for performing the Thellier experiment on paleointensity determinations are compared. The first method is essentially that of Coe (1967) and the second is a slight modification of it. Prepared samples containing different species of magnetic particles are used, and both methods are always performed on the same sample. The study is designed to accent procedural differences between the two methods. It is shown that only the Coe method yields linear PNRM-PTRM (Partial ThermoRemanent Magnetization) plots for single domain and pseudo-single domain particles, because it maintains the symmetry between high-temperature VRM (Viscous Remanent Magnetization) and spontaneous decay, whereas for the modified Coe method the spontaneous decay is enhanced. For multidomain remanence, even the Coe method yields a nonlinear concave-up PNRM-PTRM plot. Paleointensity determinations employing only the ratio NRM/TRM provide no means of evaluating the reliability of the results.

Levi, S.↗

NASA NTRS1983

Computer simulation of surface and film processes

Adequate computer methods, based on interactions between discrete particles, provide information leading to an atomic level understanding of various physical processes. The success of these simulation methods, however, is related to the accuracy of the potential energy function representing the interactions among the particles. The development of a potential energy function for crystalline SiO2 forms that can be employed in lengthy computer modelling procedures was investigated. In many of the simulation methods which deal with discrete particles, semiempirical two body potentials were employed to analyze energy and structure related properties of the system. Many body interactions are required for a proper representation of the total energy for many systems. Many body interactions for simulations based on discrete particles are discussed.

Tiller, W. A.↗

NASA NTRS1985

Performance Test of Laser Velocimeter System for the Langley 16-foot Transonic Tunnel

An investigation in the Langley 16-Foot Transonic Tunnel has been conducted in which a laser velocimeter was used to measure free-stream velocities from Mach 0.1 to 1.0 and the flow velocities along the stagnating streamline of a hemisphere-cylinder model at Mach 0.8 and 1.0. The flow velocity was also measured at Mach 1.0 along the line 0.533 model diameters below the model. These tests determined the performance characteristics of the dedicated two-component laser velocimeter at flow velocities up to Mach 1.0 and the effects of the wind tunnel environment on the particle-generating system and on the resulting size of the generated particles. To determine these characteristics, the measured particle velocities along the stagnating streamline at the two Mach numbers were compared with the theoretically predicted gas and particle velocities calculated using a transonic potential flow method. Through this comparison the mean detectable particle size (2.1 micron) along with the standard deviation of the detectable particles (0.76 micron) was determined; thus the performance characteristics of the laser velocimeter were established.

Meyers, J. F.↗

NASA NTRS1984

Absolute and angular efficiencies of a microchannel-plate position-sensitive detector

This paper presents a characterization of a commercially available position-sensitive detector of energetic ions and neutrals. The detector consists of two microchannel plates followed by a resistive position-encoding anode. The work includes measurement of absolute efficiencies of H(+), He(+), and O(+) ions in the energy range between 250 and 5000 eV, measurement of relative detection efficiencies as a function of particle impact angle, and a simple method for accurate measurement of the time at which a particle strikes the detector.

Gao, R. S.↗

NASA NTRS1985

Colloidal Oxide Properties and Kinetic Studies

Silica based oxide particles prepared by various methods are compared in terms of their gellation kinetics, densification kinetics, and microable structural evolutions begin at very low temperature. Additional work reported in literature further suggested that the colloidal behaviors and the dried gel structures of the same oxide from different preparation techniques differ fundamentally. These differences significantly affect the densification kinetics and the product microstructure. Gravitational segregation of particles of different sizes in a gravitational field is modelled as a diffusion/segregation problem. A structural free volume model was used to describe the activation process of jump statistics. The sizes of the particles, the interstices, and their packing topology are accounted for in the estimation of the free volume. An attempt frequency is ascribed to particles to account for the vibrational rearrangement during powder packing.

Chen, I. W.↗

NASA NTRS1988

Calibration of single particle sizing velocimeters using photomask reticles

The development of photomask reticle calibration standards for single particle instruments is discussed. The calibration method studied involves the use of photomask reticles where the particle artifacts are actually disks of chrome thin film in the clear field reticles produced by photolithography and etching processes. Consideration is given to various aspects of theory, design, and performance.

Hirleman, E. D.↗

NASA NTRS1990

An investigation of the effects of seeding in laser velocimeter systems

Errors in laser velocimeter measurements associated with the lag of seeding particles in subsonic and transonic flows were investigated experimentally and theoretically. In a low-speed flow, errors exceeding 5 percent were measured for particle diameters greater than 5 microns. In transonic flows, errors up to 60 percent were measured for particles with 2-3-micron diameters and up to 30 percent for 1-2-micron particles. A three-dimensional method was developed to determine the magnitude of errors due to the lag in seeding particle response based on a simplified particle force balance model and an empirical coefficient of drag model for spherical bodies. A one-dimensional version of this model was shown to be successful in correcting velocity measurements in both the subsonic and transonic flow regions.

Jones, Gregory S.↗

NASA NTRS1983

Apparatus for continuous, fast, and precise measurements of position and velocity of a small spherical particle

The position and velocity of optically levitated glass spheres (radii 10-20 microns) movng in a gas are measured accurately, rapidly, and continuously using a high-speed rotating polygon mirror. The experimental technique developed here has repeatable position accuracies better than 20 microns. Each measurement takes less than 1 microsec and can be repeated every 100 microsec. The position of the levitated glass spheres can be manipulated accurately by modulating the laser power with an acoustic optic modulator. The technique provides a fast and accurate method to study general particle dynamics in a fluid.

Venkataraman, T. S.↗

NASA NTRS2011

Spectral Analyses and Radiation Exposures from Several Ground-Level Enhancement (GLE) Solar Proton Events: A Comparison of Methodologies

Several methods for analyzing the particle spectra from extremely large solar proton events, called Ground-Level Enhancements (GLEs), have been developed and utilized by the scientific community to describe the solar proton energy spectra and have been further applied to ascertain the radiation exposures to humans and radio-sensitive systems, namely electronics. In this paper 12 GLEs dating back to 1956 are discussed, and the three methods for describing the solar proton energy spectra are reviewed. The three spectral fitting methodologies are EXP [an exponential in proton rigidity (R)], WEIB [Weibull fit: an exponential in proton energy], and the Band function (BAND) [a double power law in proton rigidity]. The EXP and WEIB methods use low energy (MeV) GLE solar proton data and make extrapolations out to approx.1 GeV. On the other hand, the BAND method utilizes low- and medium-energy satellite solar proton data combined with high-energy solar proton data deduced from high-latitude neutron monitoring stations. Thus, the BAND method completely describes the entire proton energy spectrum based on actual solar proton observations out to ~10 GeV. Using the differential spectra produced from each of the 12 selected GLEs for each of the three methods, radiation exposures are presented and discussed in detail. These radiation exposures are then compared with the current 30-day and annual crew exposure limits and the radiation effects to electronics.

Atwell, William↗

NASA NTRS1983

Settling of fixed erythrocyte suspension droplets

It is pointed out that when particles behave collectively rather than individually, the fractionation of micron-size particles on the basis of size, density, and surface characteristics by centrifugation and electrophoresis is hindered. The formation and sedimentation of droplets containing particles represent an extreme example of collective behavior and pose a major problem for these separation methods when large quantities of particles need to be fractionated. Experiments are described that measure droplet sizes and settling rates for a variety of particles and droplets. Expressions relating the particle concentration in a drop to measurable quantities of the fluids and particles are developed. The number of particles in each droplet is then estimated, together with the effective droplet density. Red blood cells from different animals fixed in glutaraldehyde provide model particle groups.

Omenyi, S. N.↗

NASA NTRS2001

Monte Carlo track structure for radiation biology and space applications

Over the past two decades event by event Monte Carlo track structure codes have increasingly been used for biophysical modelling and radiotherapy. Advent of these codes has helped to shed light on many aspects of microdosimetry and mechanism of damage by ionising radiation in the cell. These codes have continuously been modified to include new improved cross sections and computational techniques. This paper provides a summary of input data for ionizations, excitations and elastic scattering cross sections for event by event Monte Carlo track structure simulations for electrons and ions in the form of parametric equations, which makes it easy to reproduce the data. Stopping power and radial distribution of dose are presented for ions and compared with experimental data. A model is described for simulation of full slowing down of proton tracks in water in the range 1 keV to 1 MeV. Modelling and calculations are presented for the response of a TEPC proportional counter irradiated with 5 MeV alpha-particles. Distributions are presented for the wall and wall-less counters. Data shows contribution of indirect effects to the lineal energy distribution for the wall counters responses even at such a low ion energy.

NASA Center JSC↗

NASA NTRSDate not supplied

Observation of Deep Convective Cloud-Top Height and Vertical Temperature Structure of Hurricane Using Hyperspectral Infrared Sounder and its Single-Field-View Retrieval Products

Hurricanes, severe tropical cyclones (TC), or typhoons are significant natural disasters that often result in substantial loss of life and property damage. Numerous studies have indicated that changes in TC intensity are closely linked to deep convective clouds (DCC), with stronger TCs typically exhibiting higher cloud top heights (CTH) compared to weaker TCs. The CTH can help determine if a tropical depression is at the onset of rapid intensification based on case studies. Therefore, accurate determination of TC CTH will be greatly helpful for monitoring TC development and studying TC dynamics. One traditional and most common method to derive CHT from satellite observations is using the thermal brightness temperature in atmospheric channels to match the sounding temperature profile. However, it was found that thermally derived CTH has a lower bias of approximately 1 km, and this bias tends to worsen for the tallest clouds. A new method using the hyperspectral infrared sounder will be presented. From the measurements of Cross-track Infrared Sounder (CrIS) on S-NPP and J-1, along with radiative transfer simulations, we identified the inverted-V spectral feature in the ozone (O3) band (near 9.6 μm) corresponding to high clouds. The depth of the inverted-V can be used to estimate the CTH. Since the depth is computed using the peak absorption O3 channel and the nearby most transparent O3 channel in this O3 band, the uncertainties associated with cloud emissivity and scattering by cloud particles in the traditional method can be ignored. From several hurricane case studies, we found that the CHT derived using this method can accurately capture the structure of the cloud tops in the eyewall, spiral rainbands, and surrounding regions. For example, Hurricane Dorian on September 2, 2019, showed a nicely outward-sloping and circular shape eye cloud in the early morning, but the circular shape of the eyewall cloud became distorted in the afternoon. For various hurricanes we examined, the distribution of CHT for the eyewall clouds differed significantly. To better study the thermodynamic structure of hurricane clouds, this research will analyze the vertical temperature profiles from a new single Field of View (SFOV) Sounder Atmospheric Products (SiFSAP), derived using CrIS and the Advanced Technology Microwave Sounder (ATMS) onboard SNPP and JPSS-1. SiFSAP has a spatial resolution of 15 km at nadir, which surpasses most global weather and climate models and other current operational sounding products. The combined use of ATMS and CrIS allows for retrievals near hurricane eyewalls and spiral rainbands. Wind fields from NASA’s Modern-Era Retrospective Analysis for Research and Applications Version-2 (MERRA-2) and ERA5 will be used to characterize transport, and comparisons between the model temperature and water vapor profiles with the corresponding SiFSAP products will also be provided.

SiFSAP↗

NASA NTRS2010

Effects of Ice Particle Size Vertical Inhomogeneity on the Passive Remote Sensing of Ice Clouds

The solar reflectance bi-spectral (SRBS) and infrared split-window (IRSpW) methods are two of the most popular techniques for passive ice cloud property retrievals from multispectral imagers. Ice clouds are usually assumed to be vertically homogeneous in global operational algorithms based on these methods, although significant vertical variations of ice particle size are typically observed in ice clouds. In this Study we investigate uncertainties in retrieved optical thickness, effective particle size, and ice water path introduced by a homogeneous cloud assumption in both the SRBS and IRSpW methods, and focus on whether the assumption can lead to significant discrepancies between the two methods. The study simulates the upwelling spectral radiance associated with vertically structured clouds and passes the results through representative SRBS and IRSpW retrieval algorithms. Cloud optical thickness is limited to values for which IRSpW retrievals are possible (optical thickness less than about 7). When the ice cloud is optically thin and yet has a significant ice particle size vertical variation, it is found that both methods tend to underestimate the effective radius and ice water path. The reason for the underestimation is the nonlinear dependence of ice particle scattering properties (extinction and single scattering albedo) on the effective radius. Because the nonlinearity effect is stronger in the IRSpW than the SRBS method, the IRSpW-based IWP tends to be smaller than the SRBS counterpart. When the ice cloud is moderately optically thick, the IRSpW method is relatively insensitive to cloud vertical structure and effective radius retrieval is weighted toward smaller ice particle size, while the weighting function makes the SRBS method more sensitive to the ice particle size in the upper portion of the cloud. As a result, when ice particle size increases monotonically toward cloud base, the two methods are in qualitative agreement; in the event that ice particle size decreases toward cloud base, the effective radius and ice water path retrievals based on the SRBS method are substantially larger than those from the IRSpW. The main findings of this Study Suggest that the homogenous cloud assumption can affect the SRBS and IRSpW methods to different extents and, consequently, can lead to significantly different retrievals. Therefore caution should be taken when comparing and combining the ice cloud property retrievals from these two methods.

Zhang, Zhibo↗