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At least 397 records · Page 22
All sourcesNASA NTRSDOE OSTI
NASA NTRS2001

Flame Synthesis Used to Create Metal-Catalyzed Carbon Nanotubes

Metal-catalyzed carbon nanotubes are highly ordered carbon structures of nanoscale dimensions. They may be thought of as hollow cylinders whose walls are formed by single atomic layers of graphite. Such cylinders may be composed of many nested, concentric atomic layers of carbon or only a single layer, the latter forming a single-walled carbon nanotube. This article reports unique results using a flame for their synthesis. Only recently were carbon nanotubes discovered within an arc discharge and recognized as fullerene derivatives. Today metal-catalyzed carbon nanotubes are of great interest for many reasons. They can be used as supports for the metal catalysts like those found in catalytic converters. Open-ended nanotubes are highly desirable because they can be filled by other elements, metals or gases, for battery and fuel cell applications. Because of their highly crystalline structure, they are significantly stronger than the commercial carbon fibers that are currently available (10 times as strong as steel but possessing one-sixth of the weight). This property makes them highly desirable for strengthening polymer and ceramic composite materials. Current methods of synthesizing carbon nanotubes include thermal pyrolysis of organometallics, laser ablation of metal targets within hydrocarbon atmospheres at high temperatures, and arc discharges. Each of these methods is costly, and it is unclear if they can be scaled for the commercial synthesis of carbon nanotubes. In contrast, flame synthesis is an economical means of bulk synthesis of a variety of aerosol materials such as carbon black. Flame synthesis of carbon nanotubes could potentially realize an economy of scale that would enable their use in common structural materials such as car-body panels. The top figure is a transmission electron micrograph of a multiwalled carbon nanotube. The image shows a cross section of the atomic structure of the nanotube. The dark lines are individual atomic layer planes of carbon, seen here in cross section. They form a nested series of concentric cylinders, much like the growth rings on a tree. This sample was obtained by the supported catalyst method, whereby the nanoscale catalysts are dispersed on a substrate providing their support. The substrate with catalyst particles was immersed within an acetylene diffusion flame to which nitrogen had been added to eliminate soot formation. Upon removal from the flame, the nanotubes were dispersed on a holder suitable for electron microscopy. Although not seen in the figure, the tube diameter reflects that of the catalyst particle.

VanderWal, Randy L.↗
NASA NTRS2000

Apse-Alignment of the Uranian Rings

An explanation of the dynamical mechanism for apse-alignment of the eccentric Uranian rings is necessary before observations can be used to determine properties such as ring masses, particle sizes, and elasticities. The leading model relies on the ring self-gravity to accomplish this task, yet it yields equilibrium masses which are not in accord with Voyager radio measurements. We explore possible solutions such that the self-gravity and the collisional terms are both involved in the process of apse-alignment. We consider limits that correspond to a hot and a cold ring, and show that pressure terms may play a significant role in the equilibrium conditions for the narrow Uranian rings. In the cold ring case, where the scale height of the ring near periapse is comparable to the ring particle size, we introduce a new pressure correction pertaining to a region of the ring where the particles are locked in their relative positions and jammed against their neighbors, and the velocity dispersion is so low that the collisions are nearly elastic. In this case, we find a solution such that the ring self-gravity maintains apse-alignment against both differential precession (m = 1 mode) and the fluid pressure. We apply this model to the Uranian alpha ring, and show that, compared to the previous self-gravity model, the mass estimate for this ring increases by an order of magnitude. In the case of a hot ring, where the scale height can reach a value as much as fifty times larger than a particle size, we find velocity dispersion profiles that result in pressure forces which act in such a way as to alter the ring equilibrium conditions, again leading to a ring mass increase of an order of magnitude; however, such a velocity dispersion profile would require a different mechanism than is currently envisioned for establishing heating/cooling balance in a finite-sized, inelastic particle ring. Finally, we introduce an important correction to the model of Chiang and Goldreich.

Mosqueira, I.↗
NASA NTRS1989

Magnetohydrodynamic waves and particle acceleration in a coronal loop

A model is presented for the acceleration of electrons in a flaring solar coronal loop. It is suggested that the primary energy release event in the flare establishes a spectrum of MHD waves within the loop which accelerate electrons by wave-particle resonant interactions. The nature of the MHD oscillations are described and numerical and analytic solution of the dispersion relation are examined. It is found that the behavior of a particle depends on whether or not it is in resonance with the wave spectrum. Resonant particles follow chaotic trajectories and can diffuse in velocity space between wave effective potentials, thereby gaining energy.

De La Beaujardiere, Jean-Francois↗
NASA NTRS2004

Plasma Dispersion Function for the Kappa Distribution

The plasma dispersion function is computed for a homogeneous isotropic plasma in which the particle velocities are distributed according to a Kappa distribution. An ordinary differential equation is derived for the plasma dispersion function and it is shown that the solution can be written in terms of Gauss' hypergeometric function. Using the extensive theory of the hypergeometric function, various mathematical properties of the plasma dispersion function are derived including symmetry relations, series expansions, integral representations, and closed form expressions for integer and half-integer values of K.

Podesta, John J.↗
NASA NTRS1991

The modified plasma dispersion function

The modified plasma dispersion function (MPDF), based on the generalized Lorentzian (kappa) particle distribution function, is introduced, and a comprehensive set of graphs of the real and imaginary parts of the MPDF is presented. For any positive integral value of kappa, MPDF is calculated in closed form as a finite series. It is demonstrated how the MPDF approaches the plasma dispersion function in the limit as kappa yields infinity, a result to be expected since the kappa distribution function formally approaches the Maxwellian as kappa yields infinity. It is concluded that the MPDF can provide a tool in studying microinstabilities in plasmas when the particle distribution function is not only the standard generalized Lorentzian, but also of the Lorentzian type, including the loss-cone, bi-Lorentzian, and product bi-Lorentzian distributions.

Summers, Danny↗
NASA NTRS1993

Particle-Gas Dynamics in the Midplane of a Protoplanetary Nebula

In this paper, we study the stage of planetary formation during which the particulate material is still dispersed as centimeter-to-meter sized primordial aggregates. During this stage, particles are able to settle toward the midplane into a layer of mass density comparable to or much greater than that of the gas. Nonlinear, coupled interactions between the particles and the nebula gas become significant and ultimately determine the vertical profiles of the particle density and the mean velocities of the particles and the nearby gas. This is the environment in which the earliest planetesimals probably form. Our numerical models rely on the Reynolds averaged Navier-Stokes equations for the gas and particles and are fully viscous and turbulent (and, for the particles. compressible). Our turbulence modeling uses a Prandtl local shear parametrization, validated by laboratory experiments. We have developed a new model for particle diffusion involving the profile of the nebula gas turbulence and the particle Schmidt number, which is a function of particle size and density. We model a cool, quiescent nebula at 1 AU (280 K) and 10 AU (90 K) and a higher temperature stage (1000 K) at 1 AU. Our main results include: (a) rapid accretion of planetesimals by gravitationally unstable fragmentation on an orbital time scale (the 'Goldreich-Ward instability') is unlikely to occur until objects have already accreted by some other process to the mass of the largest known meteorite samples, if at all; (b) from 'seeds' as small as 10 m, growth of 10- to 100-km planetesimals can proceed rapidly by drift-augmented accretion in the particle-rich midplane with orbital decay of about 1% for the growing planetesimals; (c) outward transport of vapor and small entrained chips can account for significant radial compositional and mineralogical mixing in primitive meteorite parent bodies. Other implications may be drawn concerning particle random collisional velocities and the time scales of midplane turbulence.

Cuzzi, Jeffrey N.↗
NASA NTRS1985

Survey of probable micrometer-sized Earth-orbital debris fragments in the NASA-JSC cosmic dust sample collection

A program to collect extraterrestrial dust samples from the stratosphere using impactors mounted on NASA U-2 and WB-57F aircraft is discussed. Sample collection, preparation, and analysis techniques are described and the particle types found are reviewed. Preliminary examination of the particles indicates that they represent not only extraterrestrial material, but some fraction of terrestrial contamination from both natural and manmade sources. This examination involves a combination of optical microscopy, scanning electron microscopy (SEM) and qualitative bulk elemental analysis using an energy-dispersive X-ray spectrometer (EDS) to characterize each particle. The cosmic dust collection contains samples of at least three classes of material that may present some hazard to extended spacecraft operations in near-Earth orbit: (1) micrometeorites/cosmic dust, (2) aluminum oxide spheres, and (3) alloy spherules and fragments.

Clanton, U. S.↗
NASA NTRS2016

Electromagnetic Cyclotron Waves in the Solar Wind: Wind Observation and Wave Dispersion Analysis

Wind observed long-lasting electromagnetic cyclotron waves near the proton cyclotron frequency on 11 March 2005, in the descending part of a fast wind stream. Bi-Maxwellian velocity distributions are fitted for core protons, beam protons, and alpha-particles. Using the fitted plasma parameters we conduct kinetic linear dispersion analysis and find ion cyclotron and/or firehose instabilities grow in six of 10 wave intervals. After Doppler shift, some of the waves have frequency and polarization consistent with observation, thus may be correspondence to the cyclotron waves observed.

cyclotron↗
NASA NTRS1979

Dynamics of a stellar bar

The dynamical properties of a prolate bar have been studied by means of a three-dimensional computer model. The bar pattern rotates in the sense of the total angular momentum. The mean particle motion is a rapid streaming in the direction of pattern rotation as seen from a frame that rotates with the bar. Rotation rates that would be inferred from observation are significantly (2-3 times) faster than the pattern rotation speed. Velocity dispersions are anisotropic with the largest component along the bar. Particles oscillate in the bar potential significantly faster than pattern rotation. About 25% of the star orbits are near 2:2:1 resonance with the slow motion along the bar. Particle motion is highly ordered in the bar. Observable properties are described; where comparisons can be made, observable properties are in agreement with observations of brightness contours, velocity fields, and velocity dispersions. The bar has nearly exponential density profiles.

Miller, R. H.↗
NASA NTRS1995

Demonstration of a stabilized alumina/ethanol colloidal dispersion technique for seeding high temperature air flows

Laser anemometry enables the measurement of complex flow fields via the light scattered from small particles entrained in the flow. In the study of turbomachinery, refractory seed materials are required for seeding the flow due to the high temperatures encountered. In this work we present a pH stabilization technique commonly employed in ceramic processing to obtain stable dispersions for generating aerosols of refractory seed material. By adding submicron alumina particles to a preadjusted pH solution of ethanol, a stable dispersion is obtained which when atomized, produces a high quality aerosol. Commercial grade alumina powder is used with a moderate size distribution. Other metal oxide powders in various polar solvents could also be used once the point of zero charge (pH(pzc)) of the powder in the solvent has been determined. Laser anemometry measurements obtained using the new seeding technique are compared to measurements obtained using Polystyrene Latex (PSL) spheres as the seed material.

Wernet, Mark P.↗
NASA NTRS1973

Analysis of the ultrafine fraction of the Apollo 14 regolith

Analyses were obtained on more than 2400 randomly selected particles from the sub-37 micron (ultrafine) fraction of ten Apollo 14 regolith samples. The analyses were conducted with an energy dispersive electron microprobe system. The semiquantitative data were used to group the particles into ten categories. The pyroxene/plagioclase and olivine/plagioclase ratios are inconsistent with those ratios in the Apollo 14 breccias and rocks. The data suggest that fragmented basalts similar to Apollo 12 olivine basalts may have made significant contributions to the ultrafine fraction of the Fra Mauro regolith. Among a number of unusual particles encountered are brown, birefringent lath-shaped grains with 60 wt % SiO2 and 34 wt % FeO(FeSi2O5) and a glass with 20 to 25 wt % CaO, 0 to 8 wt % MgO, 40 to 45 wt % Al2O3 and approximately 30 wt % SiO2.

Finkelman, R. B.↗
NASA NTRS1986

Thin-sectioning and microanalysis of individual extraterrestrial particles

A long standing constraint on the study of micrometeorites has centered on difficulties in preparing them for analysis. This is due largely to their small dimensions and consequent practical limitations on sample manipulation. Chondritic micrometeorites provide a good example; although much has been learned about their chemistry and mineralogy almost nothing was known about such basic properties as texture and petrographic associations. The only way to assess such properties is to examine microstructure indigenous to the particles. Unfortunately, almost all micrometeorites, out of necessity, have been crushed and dispersed onto appropriate substances prior to analysis, and most information about texture and petrography was lost. Recently, thin-sections of individual extraterrestrial particles have been prepared using an ultramicrotome equipped with a diamond knife. This procedure has been applied to stratospheric micrometeorites and Solar Max impact debris. In both cases the sections have enabled observation of a variety of internal particle features, including textures, porosity, and petrographic associations. The sectioning procedure is described and analysis results for chondritic micrometeoroids and select particles from Solar Max are presented.

Bradley, J. P.↗
NASA NTRS1991

Evaluation of an efficient statistical transport model for turbulent droplet dispersion in dilute combusting sprays

Evaluation of an efficient statistical transport model for turbulent droplet dispersion is made for a dilute spray of methanol droplets injected into a turbulent, axisymmnetric methane-fuelled diffusion flame burning in stagnant air. In the dispersion model, a computational parcel representing a group of physical particles (droplets) is considered to have a normal probability density function (pdf) in space. The mean is determined by Lagrangian tracking through a sequence of stochastically generated turbulent eddies and the variance is evaluated from a statistical formulation based on the linearized particle equations of motion. The basic validity of this model is established through comparison with available experimental data and with theoretical predictions using a conventional stochastic direct modeling approach. The conclusion of the evaluation is that the proposed dispersion model compares favorably with experimental data and provides a valid technique for simulating turbulent combusting sprays with significant computational savings over conventional methods.

Litchford, Ron J.↗
NASA NTRS1987

Numerical simulations of collisions between rotating particles

Numerical simulations of Keplerian systems consisting of 200 mutually colliding rotating particles show that friction and surface irregularity reduce the equilibrium velocity dispersion and transfer some of the energy of random velocities to rotational velocities. The results confirm the theoretical predictions of Salo (1987). Simulations are performed for identical and different particle sizes, and for a power-law distribution of sizes. Taking rotation into account is not found to alter the previously observed Rayleigh distribution of eccentricities and inclinations, while the components of the rotational velocities are found to follow a Gaussian distribution. Application to the rarefied regions of Saturn's rings suggests that friction is able to reduce the equilibrium geometric thickness by about one-half.

Salo, H.↗
NASA NTRS1965

Anodization process produces opaque, reflective coatings on aluminum

Opaque, reflective coatings are produced on aluminum articles by an anodizing process wherein the anodizing bath contains an aqueous dispersion of finely divided insoluble inorganic compounds. These particles appear as uniformly distributed occlusions in the anodic deposit on the aluminum.

Source record↗
NASA NTRS1975

Value contamination avoidance devices

Mechanical redesign methods were used to minimize contamination damage of conventional fluid components and a contamination separator device was developed for long term reusable space vehicles. These were incorporated into an existing 50.8 mm poppet valve and tested for damage tolerance in a full size open loop flow system with gaseous and liquid nitrogen. Cyclic and steady flow conditions were tested with particles of 125 to 420 micrometers aluminum oxide dispersed in the test fluids. Nonflow life tests (100,000 cycles) were made with two valve configurations in gaseous hydrogen. The redesigned valve had an acceptable cycle life and improved tolerance to contamination damage when the primary sealing surfaces were coated with thin coatings of hard plastic (Teflon S and Kynar). Analytical studies and flow testing were completed of four different versions of the separator. overall separation efficiencies in the 55-90% range were measured with these non-optimum configurations.

Endicott, D. L.↗
NASA NTRS1984

The scattering of energetic particles by waves in a finite beta plasma

Solutions are presented for the dispersion relation of waves propagating parallel to the ambient magnetic field, in a plasma having an arbitrary ratio of thermal to magnetic pressure, beta. Previous results applicable only to wave frequencies much lower than the ion cyclotron frequency are extended to include all frequencies lower than the electron cyclotron frequency. The cyclotron turnovers are found to occur at significantly lower frequencies in finite beta plasmas. Cyclotron damping is significant for small wavelength waves. These results show that in energetic particle scattering by electromagnetic turbulence in a plasma with beta value greater than 40, scattering by waves with wave frequencies greater than the ion cyclotron frequency can be neglected. This condition is satisfied in many astrophysical plasmas.

Davila, J. M.↗