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At least 397 records · Page 22

Ceramic susceptor for induction bonding of metals, ceramics, and plastics

A thin (.005) flexible ceramic susceptor (carbon) was discovered. It was developed to join ceramics, plastics, metals, and combinations of these materials using a unique induction heating process. Bonding times for laboratory specimens comparing state of the art technology to induction bonding were cut by a factor of 10 to 100 times. This novel type of carbon susceptor allows for applying heat directly and only to the bondline without heating the entire structure, supports, and fixtures of a bonding assembly. The ceramic (carbon film) susceptor produces molten adhesive or matrix material at the bond interface. This molten material flows through the perforated susceptor producing a fusion between the two parts to be joined, which in many instances has proven to be stronger than the parent material. Bonding can be accomplished in 2 minutes on areas submitted to the inductive heating. Because a carbon susceptor is used in bonding carbon fiber reinforced plastics and ceramics, there is no radar signature or return making it an ideal process for joining advanced aerospace composite structures.

Fox, Robert L.↗

The ISPM solar-wind ion composition spectrometer

The International Solar Polar Mission (ISPM) Solar-Wind Ion Composition Spectrometer which determines elemental and ionic-charge composition, and the temperatures and mean speeds of all major solar-wind ions, from H through Fe, at solar wind speeds ranging from 145 km/sec (protons) to 1352 km/sec (Fe+8) is described. The instrument, which covers an energy per charge range from 110 eV/q to 66.7 keV/q in 13 min, combines an electrostatic analyzer with postacceleration, followed by a time-of-flight and energy measurement. Conditions and processes in the region of the corona where the solar wind is accelerated; location of the source regions of the solar wind in the corona; coronal heating processes; the extent and causes of variations in the composition of the solar atmosphere; plasma processes in the solar wind; acceleration of energetic particles in the solar wind; the thermalization and acceleration of interstellar ions in the solar wind, and their composition; and the composition and behavior of the plasma in the Jovian magnetosphere are studied.

Gloeckler, G.↗

Complementary use of monochromatic and white-beam X-ray micro-diffraction for the investigation of ancient materials

Archaeological artefacts are often heterogeneous materials where several phases coexist in a wide grain size distribution. Most of the time, retrieving structure information at the micrometre scale is of great importance for these materials. Particularly, the organization of different phases at the micrometre scale is closely related to optical or mechanical properties, manufacturing processes, functionalities in ancient times and long-term conservation. Between classic X-ray powder diffraction with a millimetre beam and transmission electron microscopy, a gap exists and structure and phase information at the micrometre scale are missing. Using a micrometre-size synchrotron X-ray beam, a hybrid approach combining both monochromatic powder micro-diffraction and Laue single-crystal micro-diffraction was deployed to obtain information from nanometre- and micrometre-size phases, respectively. Therefore providing a way to bridge the aforementioned gap, this unique methodology was applied to three different types of ancient materials that all show a strong heterogeneity. In Roman terra sigillata, the specific distribution of nanocrystalline hematite is mainly responsible for the deep-red tone of the slip, while the distribution of micrometre-size quartz in ceramic bodies reflects the change of manufacturing process between pre-sigillata and high-quality sigillata periods. In the second example, we investigated the modifications occurring in Neolithic and geological flints after a heating process. By separating the diffracted signal coming from the nano- and the micrometre scale, we observed a domain size increase for nanocrystalline quartz in geological flints and a relaxation of the residual strain in larger detritic quartz. In conclusion, through the study of a Roman iron nail, we showed that the carburation process to strengthen the steel was mainly a surface process that formed 10–20 µm size domains of single–crystal ferrite and nanocrystalline cementite.

36 MATERIALS SCIENCE↗

A comprehensive magnetohydrodynamic model of the Venus ionosphere

The MHD Venus ionospheric model of Shinegawa and Cravens (1988) is improved here by including the energy equations for ions and electrons in a self-consistent manner. This new model reproduces observed electron density and magnetic field profiles very well, while the basic MHD process of the Venus ionosphere remain virtually unchanged. The results indicate that including energetics does not significantly alter the density and magnetic field profiles. Under unmagnetized conditions, heat fluxes for both ions and electrons must be imposed to reproduce the observed plasma temperature profiles. A heat source for the ions is probably present at higher altitudes in the magnetized ionosphere. Heating processes do not play a significant role in the dynamics at low altitudes.

Shinagawa, H.↗

Processing Parameter Effects on Residual Stress and Mechanical Properties of Selective Laser Melted Ti6Al4V

Selective laser melting (SLM) process is characterized by large temperature gradients resulting in high levels of residual stress within the additively manufactured metallic structure. SLM-processed Ti6Al4V yields a martensitic microstructure due to the rapid solidification and results in a ductility generally lower than a hot working equivalent. Post-process heat treatments can be applied to SLM components to remove in-built residual stress and improve ductility. Residual stress buildup and the mechanical properties of SLM parts can be controlled by varying the SLM process parameters. This investigation studies the effect of layer thickness on residual stress and mechanical properties of SLM Ti6Al4V parts. This is the first-of-its kind study on the effect of varying power and exposure in conjunction with keeping the energy density constant on residual stress and mechanical properties of SLM Ti6Al4V components. It was found that decreasing power and increasing exposure for the same energy density lowered the residual stress and improved the % elongation of SLM Ti6Al4V parts. Increasing layer thickness resulted in lowering the residual stress at the detriment of mechanical properties. The study is based on detailed experimental analysis along with finite element simulation of the process using ABAQUS to understand the underlying physics of the process.

36 MATERIALS SCIENCE↗

RELAP5-3D Modeling of Heat Transfer Components (Intermediate Heat Exchanger and Helical-Coil Steam Generator) for NGNP Application

The Next Generation Nuclear Plant project is aimed at the research and development of a helium-cooled high-temperature gas reactor that could generate both electricity and process heat for the production of hydrogen. The heat from the high-temperature primary loop must be transferred via an intermediate heat exchanger to a secondary loop. Using RELAP5-3D, a model was developed for two of the heat exchanger options a printed-circuit heat exchanger and a helical-coil steam generator. The RELAP5-3D models were used to simulate an exponential decrease in pressure over a 20 second period. The results of this loss of coolant analysis indicate that heat is initially transferred from the primary loop to the secondary loop, but after the decrease in pressure in the primary loop the heat is transferred from the secondary loop to the primary loop. A high-temperature gas reactor model should be developed and connected to the heat transfer component to simulate other transients.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Transition region and chromospheric signatures of impulsive heating events. II. Modeling

Results from the Solar Maximum Mission showed a close connection between the hard X-ray (HXR) and transition region (TR) emission in solar flares. Analogously, the modern combination of RHESSI and IRIS data can inform the details of heating processes in ways that were never before possible. We study a small event that was observed with RHESSI, IRIS, SDO, and Hinode, allowing us to strongly constrain the heating and hydrodynamical properties of the flare, with detailed observations presented in a previous paper. Long duration redshifts of TR lines observed in this event, as well as many other events, are fundamentally incompatible with chromospheric condensation on a single loop. We combine RHESSI and IRIS data to measure the energy partition among the many magnetic strands that comprise the flare. Using that observationally determined energy partition, we show that a proper multithreaded model can reproduce these redshifts in magnitude, duration, and line intensity, while simultaneously being well constrained by the observed density, temperature, and emission measure. We comment on the implications for both RHESSI and IRIS observations of flares in general, namely that: (1) a single loop model is inconsistent with long duration redshifts, among other observables; (2) the average time between energization of strands is less than 10 s, which implies that for a HXR burst lasting 10 minutes, there were at least 60 strands within a single IRIS pixel located on the flare ribbon; (3) the majority of these strands were explosively heated with an energy distribution well described by a power law of slope ≈−1.6; (4) the multi-stranded model reproduces the observed line profiles, peak temperatures, differential emission measure distributions, and densities.

79 ASTRONOMY AND ASTROPHYSICS↗

Magnetospheric space plasma investigations

Topics and investigations covering this period of this semiannual report period (August 1994 - January 1995) are as follows: (1) Generalized SemiKinetic (GSK) modeling of the synergistic interaction of transverse heating of ionospheric ions and magnetospheric plasma-driven electric potentials on the auroral plasma transport. Also, presentations of GSK modeling of auroral electron precipitation effects on ionospheric plasma outflows, of ExB effects on such outflow, and on warm plasma thermalization and other effects during refilling with pre-existing warm plasmas; (2) Referees' reports received on the statistical study of the latitudinal distributions of core plasmas along the L = 4.6 field line using DE-1/RIMS data. Other work is concerned in the same field, field-aligned flows and trapped ion distributions; and (3) A short study has been carried out on heating processes in low density flux tubes in the outer plasmasphere. The purpose was to determine whether the high ion temperatures observed in these flux tubes were due to heat sources operating through the thermal electrons or directly to the ions. Other investigations center along the same area of plasmasphere-ionosphere coupling. The empirical techniques and model, the listing of hardware calibrated, and/or tested, and a description of notable meetings attended is included in this report, along with a list of all present publication in submission or accepted and those reference papers that have resulted from this work thus far.

Comfort, Richard H.↗

Benchmarking a 9Cr-2WVTa Reduced Activation Ferritic Martensitic Steel Fabricated via Additive Manufacturing

Reduced activation ferritic (RAF) martensitic steels are promising candidates for the first wall of fusion reactors. However, current manufacturing capabilities call for these components to be made by welding wrought plates. This limits design freedom and necessitates the use of post-weld heat treatments (PWHT) in accordance with the boiler and pressure vessel code. Additive manufacturing (AM) can offer a unique solution to solve this challenge by leveraging the layer-wise deposition strategy to come up with temper bead deposition techniques to eliminate post-processing heat treatments (PPHT). However, it is necessary to benchmark the properties of RAF steels fabricated by AM with their wrought counterparts to identify the process-structure-property correlation, which is the goal of this study. The study demonstrates that while tensile properties at room temperature and high temperatures are satisfactory, the as fabricated and samples after PPHT have significant heterogeneity in tensile elongation. This has been attributed to the presence of discontinuities in the build. The as-fabricated samples have an average tensile strength of 1190 + 12 MPa and an average elongation of 15 + 5% at room temperature and 658 ± 20 MPa ultimate tensile strength (UTS) and 14 ± 7% at 600 °C. After the post-weld heat treatment, mechanical properties decrease to around 600–650 MPa and an elongation between 20–25% at room temperature to 300 MPa UTS and 25–28% elongation at 600 °C. The characterization of microstructures at various length scales demonstrates that the as-fabricated structure has a significant fraction of delta ferrite in a lath martensitic matrix. No precipitates could be identified in the as-fabricated structure. PPHT led to a decrease in the area fraction of delta ferrite and precipitation of M 23 C 6 and MX. Detailed characterization clearly demonstrates that the lack of precipitates in the as-fabricated structure could be due to the slow tempering response of the alloy. Finally, the needs to develop new alloys to achieve the objectives stated above are articulated.

36 MATERIALS SCIENCE↗

A System Concept for the Advanced Post-TRMM Rainfall Profiling Radars

Atmospheric latent heating field is fundamental to all modes of atmospheric circulation and upper mixed layer circulations of the ocean. The key to understanding the atmospheric heating process is understanding how and where precipitation occurs. The principal atmospheric processes which link precipitation to atmospheric circulation include: (1) convective mass fluxes in the form of updrafts and downdrafts; (2) microphysical. nucleation and growth of hydrometeors; and (3) latent heating through dynamical controls on the gravitation-driven vertical mass flux of precipitation. It is well-known that surface and near-surface rainfall are two of the key forcing functions on a number of geophysical parameters at the surface-air interface. Over ocean, rainfall variation contributes to the redistribution of water salinity, sea surface temperature, fresh water supply, and marine biology and eco-system. Over land, rainfall plays a significant role in rainforest ecology and chemistry, land hydrology and surface runoff. Precipitation has also been closely linked to a number of atmospheric anomalies and natural hazards that occur at various time scales, including hurricanes, cyclones, tropical depressions, flash floods, droughts, and most noticeable of all, the El Ninos. From this point of view, the significance of global atmospheric precipitation has gone far beyond the science arena - it has a far-reaching impact on human's socio-economic well-being and sustenance. These and many other science applications require the knowledge of, in a global basis, the vertical rain structures, including vertical motion, rain intensity, differentiation of the precipitating hydrometeors' phase state, and the classification of mesoscale physical structure of the rain systems. The only direct means to obtain such information is the use of a spaceborne profiling radar. It is important to mention that the Tropical Rainfall Measuring Mission (TRMM) have made a great stride forward towards this ultimate goal. The Precipitation Radar (PR) aboard the TRMM satellite is the first ever spaceborne radar dedicated to three-dimensional, global precipitation measurements over the tropics and the subtropics, as well as the detailed synopsis of a wide range of tropical rain storm systems. In only twelve months since launch, the PR, together with other science instruments abroad the satellite have already provided unprecedented insights into the rainfall systems. It is anticipated the a lot more exciting and important rain observations would be made by TRMM throughout its mission duration. While TRMM has provided invaluable data to the user community, it is only the first step towards advancing our knowledge on rain processes and its contributions to climate variability. It is envisioned that a TRMM follow-on mission is needed in such a way to capitalize on the pioneering information provided by TRMM, and its instrument capability must be extended beyond TRMM in such a way to fully address the key science questions from microphysical to climatic time scale. In fact, a number of new and innovative mission concepts have recently put forth for this purpose. Almost all of these new concepts have suggested the utility of a more advanced, high-resolution, Doppler-enabled, vertical profiling radar that can provide multi-parameter observations of precipitation. In this paper, a system concept for a second- gene ration precipitation radar (PR-2) which addresses the above requirements will be described.

Im, Eastwood↗

A theory of heating of quiet solar corona

A theory is proposed to discuss the creation of hot solar corona. We pay special attention to the transition region and the low corona, and consider that the sun is quiet. The proposed scenario suggests that the protons are heated by intrinsic Alfvénic turbulence, while the ambient electrons are heated by the hot protons via collisions. The theory contains two prime components: the generation of the Alfvénic fluctuations by the heavy minor ions in the transition region and second, the explanation of the temperature profile in the low solar atmosphere. The proposed heating process operates continuously in time and globally in space.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Investigation of poly(phenylacetylene) derivatives for carbon precursor with high carbon yield and good solubility

This paper investigates a family of poly(phenylacetylene) derivatives with a p-electrons conjugated polymer backbone and side groups containing only sp 2 and sp carbons. The objective is to identify the suitable carbon precursor that is processible and can be transformed to carbonaceous material with high carbon yield by a simple (one-step) thermal transformation process (without any external reagent). Poly(phenylacetylene) with para-substituted acetylene group poly(PA-A) shows an exceptionally high C-yield (~90%) in one-step heating from ambient temperature to 1000 °C under N 2 atmosphere. Unfortunately, this poly(PA-A) polymer is quite sensitive to heat and light with very limited solubility. On the other hand, poly(phenylacetylene) with para-substituted phenylacetylene group, i.e. poly(PA-PA), offers a relatively high C-yield (~80%) and also good solubility in common organic solvents, such as toluene and tetrahydrofuran (THF). Several uniform dark-red poly(PA-PA) fibers with smooth surface and fiber diameter in the range of 3–6 μm were prepared from 30 wt% poly(PA-PA)/THF solution using electrospinning technique. Furthermore, the resulting precursor fibers were converted to the corresponding carbon structure in a one-step thermal heating process under N 2 atmosphere. Both X-ray and Raman spectra show the polymorphous carbon morphology with the graphene crystalline domains.

36 MATERIALS SCIENCE↗

Process intensification in hydrothermal liquefaction of biomass: A review

Hydrothermal liquefaction (HTL) presents a promising pathway for converting wet biomass resources into biofuels, offering significant advantages over conventional methods. However, numerous challenges must be addressed for HTL scale-up, including energy provision for the endothermic process, heat and mass transfer limitations, slurry concentration and pumpability challenges, char and coke formation, and continuous phase separation. This review explores key strategies such as autothermal HTL, which improves process efficiency and reduces external energy requirements by coupling exothermic and endothermic reactions within the same reactor, thereby simplifying reactor design and reducing operational costs. Additionally, multistage HTL processes are highlighted for their ability to optimize biocrude quality and yield by fractionating biomass conversion stages, resulting in higher energy returns on investment and better-quality biocrude. Solvothermal HTL and integration techniques for aqueous phase are also discussed. Furthermore, the HTL patent landscape is discussed to provide insights into current technological advancements. This review aims to offer a comprehensive understanding of process intensification in HTL, highlighting innovative solutions to enhance the efficiency and scalability of the process for sustainable biofuel production.

Biocrude oil↗

The Solar Wind Ion Composition Spectrometer

The Solar Wind Ion Composition Spectrometer (SWICS) on Ulysses is designed to determine uniquely the elemental and ionic-charge composition, and the temperatures and mean speeds of all major solar-wind ions, from H through Fe, at solar wind speeds ranging from 175 km/s (protons) to 1280 km/s (Fe(8+)). The instrument, which covers an energy per charge range from 0.16 to 59.6 keV/e in about 13 min, combines an electrostatic analyzer with postacceleration, followed by a time-of-flight and energy measurement. The measurements made by SWICS will have an impact on many areas of solar and heliospheric physics, in particular providing essential and unique information on: (1) conditions and processes in the region of the corona where the solar wind is accelerated; (2) the location of the source regions of the solar wind in the corona; (3) coronal heating processes; (4) the extent and causes of variations in the composition of the solar atmosphere; (5) plasma processes in the solar wind; (6) the acceleration of energetic particles in the solar wind; (7) the thermalization and acceleration of interstellar ions in the solar wind, and their composition; and (8) the composition, charge states, and behavior of the plasma in various regions of the Jovian magnetosphere.

Gloeckler, G.↗

Critical Magnetic Field Strengths for Unipolar Solar Coronal Plumes In Quiet Regions and Coronal Holes?

Coronal plumes are bright magnetic funnels that are found in quiet regions and coronal holes that extend high into the solar corona whose lifetimes can last from hours to days. The heating processes that make plumes bright involve the magnetic field at the base of the plume, but their intricacies remain mysterious. Raouafi et al. (2014) infer from observation that plume heating is a consequence of magnetic reconnection at the base, whereas Wang et al. (2016) infer that plume heating is a result of convergence of the magnetic flux at the plume's base, or base flux. Both papers suggest that the base flux in their plumes is of mixed polarity, but do not quantitatively measure the base flux or consider whether a critical magnetic field strength is required for plume production. To investigate the magnetic origins of plume heating, we track plume luminosity in the 171 Å wavelength as well as the abundance and strength of the base flux over the lifetimes of six unipolar coronal plumes. Of these, three are in coronal holes and three are in quiet regions. For this sample, we find that plume heating is triggered when convergence of the base flux surpasses a field strength of approximately 300 − 500 Gauss, and that the luminosity of both quiet region and coronal hole plumes respond similarly to the strength of the magnetic field in the base.

Avallone, Ellis↗

Analysis of self-heating of thermally assisted spin-transfer torque magnetic random access memory

Thermal assistance has been shown to significantly reduce the required operation power for spin torque transfer magnetic random access memory (STT-MRAM). Proposed heating methods include modified material stack compositions that result in increased self-heating or external heat sources. Here, we analyze the self-heating process of a standard perpendicular magnetic anisotropy STT-MRAM device through numerical simulations in order to understand the relative contributions of Joule, thermoelectric Peltier and Thomson, and tunneling junction heating. A 2D rotationally symmetric numerical model is used to solve the coupled electro-thermal equations including thermoelectric effects and heat absorbed or released at the tunneling junction. We compare self-heating for different common passivation materials, positive and negative electrical current polarity, and different device thermal anchoring and boundaries resistance configurations. The variations considered are found to result in significant differences in maximum temperatures reached. Average increases of 3 K, 10 K, and 100 K for different passivation materials, positive and negative polarity, and different thermal anchoring configurations, respectively, are observed. Furthermore, the highest temperatures, up to 424 K, are obtained for silicon dioxide as the passivation material, positive polarity, and low thermal anchoring with thermal boundary resistance configurations. Interestingly it is also found that due to the tunneling heat, Peltier effect, device geometry, and numerous interfacial layers around the magnetic tunnel junction (MTJ), most of the heat is dissipated on the lower potential side of the magnetic junction. We have observed this asymmetry in heating and is important as thermally assisted switching requires heating of the free layer specifically and this will be significantly different for the two polarity operations, set and reset.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

CODE-TO-CODE BENCHMARK STUDY FOR THERMAL STRESS MODELING AND PRELIMINARY ANALYSIS OF THE HIGH-TEMPERATURE SINGLE HEAT PIPE EXPERIMENT

Microreactors are very small nuclear reactors with typical thermal-energy output of up to 20 MWth. The microreactor concept is gaining more and more attention for safe, robust, and reliable supply of electricity for remote locations and to meet industrial process heat needs. Heat-pipe-cooled microreactor is one of the microreactors being investigated at Idaho National Laboratory. In the heat-pipe-cooled microreactor, heat pipes remove heat from the reactor core as a passive heat-transfer device, so the fluid circulation is not required for cooling, which can substantially simplify the overall reactor design. However, given the extremely high temperatures in the core region and potentially large temperature gradients across the structure materials, thermal stresses need to be well-analyzed to ensure structural integrity during normal operations and accident scenarios for the heat-pipe-cooled microreactor designs. This paper discusses finite element method-based thermal-stress analysis for the high-temperature single heat-pipe test article in the Single Primary Heat Extraction and Removal Emulator (SPHERE) facility at Idaho National Laboratory, using two commercial software packages, Abaqus and STAR-CCM+. A code-to-code benchmark study was performed to crosscheck the model setup and capability of each code and to gain insights into the potential thermal stress concerns from the current experimental setup. It is observed the significant thermal stresses happen at the locations where the largest temperature gradients appeared between heat pipe and electric heater. The temperature fields have good agreements between Abaqus and STAR-CCM+, while the induced thermal stresses show modest deviations probably due to differences of meshing engines used in these two codes.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗