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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 397 records · Page 22
All sourcesNASA NTRSDOE OSTI
DOE OSTI2018

Rich Soliton Structures for the Kraenkel-Manna-Merle (KMM) System in Ferromagnetic Materials

A particular attention is paid to investigate the Kraenkel-Manna-Merle (KMM) system, which can describe the nonlinear short-wave propagation in saturated ferromagnetic materials with zero-conductivity in an external field. A class of exact soliton solutions is constructed via the generalized G{sup ′}/G-expansion method. Some novel soliton structures are excited by choosing the arbitrary functions in the solution as certain specific functions. Hump-soliton, cusp-soliton, loop-soliton, and kink-soliton are observed graphically. The results reveal the system theoretically possesses extremely rich soliton structures.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2019

Oxygen Vacancy-Induced Room Temperature Ferromagnetism in Rutile TiO{sub 2}

As oxygen vacancies play an important role in ferromagnetism of rutile TiO{sub 2}, a method of γ-ray irradiates rutile TiO{sub 2} single crystals was subtly proposed to study the effect of oxygen vacancies on magnetic properties. Remarkably, room temperature ferromagnetism was observed in γ-ray irradiated rutile TiO{sub 2} single crystals, and the saturation magnetization is the strongest when dose is 4 × 10{sup 4} Gy which assigned to ESR results. Since the displacement threshold energy of Ti atom is much bigger than that of O atom, the defects produced by γ-irradiation are mainly oxygen vacancies. After irradiation, XPS, PL spectra indicate the presence of oxygen vacancies(V{sub O}), Ti{sup 3+}, and V{sub O}-Ti{sup 3+} composite defects.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2019

Thermal analysis of VCSEL arrays based on first principle theory and finite element method

Al{sub x}Ga{sub 1−x}As is a main epitaxial material of 850-nm VCSEL. In order to analyze lattice match and heat production, the band gap of Al{sub x}Ga{sub 1−x}As was built, using the first-principles calculation theory. In addition, based on thermoelectric coupling three-dimensional (3D) finite element method, details on the surface temperature distributions of different 850-nm VCSEL arrays were analyzed. Array spacing and array form have an effect on heat dissipation of VCSEL arrays. The diamond array with 18 light emitting units shows the best thermal stability among others.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2015

The Effects of Cold Work on the Microstructure and Mechanical Properties of Intermetallic Strengthened Alumina-Forming Austenitic Stainless Steels

In order to achieve energy conversion efficiencies of > 50 pct for steam turbines/boilers in power generation systems, materials are required that are both strong and corrosion-resistant at > 973 K (700 A degrees C), and economically viable. Austenitic steels strengthened with Laves phase, NiAl and Ni3Al precipitates, and alloyed with aluminum to improve oxidation resistance, are potential candidate materials for these applications. The microstructure and microchemistry of recently developed alumina-forming austenitic stainless steels have been characterized by scanning electron microscopy, transmission electron microscopy, and synchrotron X-ray diffraction. Different thermo-mechanical treatments were performed on these steels to improve their mechanical performance. These reduced the grain size significantly to the nanoscale (similar to 100 nm) and the room temperature yield strength to above 1000 MPa. A solutionizing anneal at 1473 K (1200 A degrees C) was found to be effective for uniformly redistributing the Laves phase precipitates that form upon casting. (C) The Minerals, Metals & Materials Society and ASM International 2015

Hu, B.↗
DOE OSTI2018

Rapid Separation of Copper Phase and Iron-Rich Phase From Copper Slag at Low Temperature in a Super-Gravity Field

A novel approach for quickly separating a metal copper phase and iron-rich phase from copper slag at low temperature is proposed based on a super-gravity method. The morphology and mineral evolution of the copper slag with increasing temperature were studied using in situ high-temperature confocal laser scanning microscopy and ex situ scanning electron microscopy and X-ray diffraction methods. Fe{sub 3}O{sub 4} particles dispersed among the copper slag were transformed into FeO by adding an appropriate amount of carbon as a reducing agent, forming the slag melt with SiO{sub 2} at low temperature and assisting separation of the copper phase from the slag. Consequently, in a super-gravity field, the metallic copper and copper matte were concentrated as the copper phase along the super-gravity direction, whereas the iron-rich slag migrated in the opposite direction and was quickly separated from the copper phase. Increasing the gravity coefficient (G) significantly enhanced the separation efficiency. After super-gravity separation at G = 1000 and 1473 K (1200 °C) for 3 minutes, the mass fraction of Cu in the separated copper phase reached 86.11 wt pct, while that in the separated iron-rich phase was reduced to 0.105 wt pct. The recovery ratio of Cu in the copper phase was as high as up to 97.47 pct.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Effect of a High Magnetic Field on γ′ Phase for Ni-Based Single Crystal Superalloy During Directional Solidification

The effect of a high magnetic field on the γ′ phase of Ni-based single crystal superalloy during directional solidification is investigated experimentally. The results clearly indicate that the magnetic field significantly reduces the γ′ phase size. Further, the quenching experiment is carried out, and the results found that the length of mushy zone is obviously decreased under a high magnetic field. Based on both experimental results and nucleation mechanism, it is found that the decrease of γ′ phase size should be attributed to the fact that a high magnetic field causes the increase of temperature gradient in front of solid/liquid interface and leads to the increase of undercooling of γ′ phase.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Effect of Hydrogen Addition on Softening and Melting Reduction Behaviors of Ferrous Burden in Gas-Injection Blast Furnace

The softening and melting reduction behaviors of ferrous burden in a gas-injection blast furnace (BF) have been investigated experimentally with the assistance of H{sub 2}. The results indicate that the initial softening temperature of the burden in the BF is lower than that in the traditional BF, while the opposite trend is observed for its melting and dripping temperatures, thus widening the softening range and narrowing the melting zone. As a result, the permeability of the stock column is apparently improved, owing to the decreased amount of the produced melt. After H{sub 2} gas is added, the thickness of the iron shell of the burden pellet increases, and the quantity of its liquid wüstite core decreases due to the higher reduction degree. The reduction rate of iron oxides is much faster than the carburization rate with the H{sub 2} addition, and the dripping behavior of the ferrous burden is determined by the carburization with a high reduction potential. After taking into account the effects of H{sub 2} addition on the iron oxide reduction rate, melt quantity, burden microstructure, and energy consumed by the gas-injection BF, it has been concluded that the optimal H{sub 2} content lies in the range between 10 and 15 pct.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Mechanical Properties and Microstructural Evolution of Yb-Modified Al-20%Si Alloy

In the study, the mechanical properties and microstructural evolution of hypereutectic Al-20%Si-xYb alloys (x = 0, 0.1, 0.3, 0.5 and 0.7 wt.%) were studied. The as-prepared samples were characterized by scanning electron microscopy, optical microscope, x-ray diffraction (XRD) and electron probe microanalysis. The characterization results showed with the addition amount of Yb increasing to 0.5%, the eutectic Si structure was gradually modified from coarse needle-like/platelet-like structure into fine coral-like fibrous structure and the primary Si phases were gradually converted from coarse platelet-like/star-like/polygonal shape into fine blocky shape. In particular, according to the results of WDS and XRD analyses, the Yb-rich intermetallic phase in the Al-20%Si alloy is Al{sub 3}Yb. Tensile test was carried out to study the mechanical properties of Al-20%Si-x%Yb alloys, and results showed that the elongation and ultimate tensile strength increased by 73.6% and 64.5%, respectively.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Sagging Mechanisms of Three-Layer Aluminum Clad Foils used in the Heat Exchanger in the Brazing Process

The sagging mechanisms of a three-layer aluminum clad foils (AA4343/AA3003Mod/AA4343) with final rolling reduction of 20-50% during brazing were studied. The results show that the sagging behavior of the aluminum brazed foils during the brazing cycle can be divided into four stages: Stage I is the slight sagging stage, during which sagging deformation can almost be ignored; Stage II is referred to as the accelerative sagging stage, and the sagging behavior is mainly ascribed to recovery. In stage II, the greater the reduction ratio is, the earlier the recovery ends, and the smaller the value of the sagging distance is. Stage III is the slow sagging stage, and sliding deformation along the grain boundaries is responsible for the slow sagging rate. Stage IV is the erosion stage. During stage IV, the coarsely recrystallized grains can inhibit erosion and are helpful in obtaining excellent sagging resistance, while the foils with finely recrystallized grains or non-recrystallized structure show severe erosion and limited sagging resistance.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Interfacial Characteristics Investigation for One-Step EDM Drilling of Cooling Holes in TBCs

In this study, the one-step electrical discharge machining of inclined cooling holes is performed in thermal-barrier-coated nickel-based superalloys via the assisting electrode method. The effects of the process parameters, including the inclination angle, peak current, pulse duration, and duty cycle, on interfacial characteristics of cooling holes were investigated. The research results are as follows: After machining, the hardness of TBCs increases slightly and the adhesion strength of ceramic coating has a slight reduction. Delamination prevailingly appears at the ceramic coating/bonding coating interface, and its length at the trailing edge is greater than that at the leading edge. Increasing either the discharge energy or the duty cycle also aggravates the severity of the delamination. Under an excessive peak current of 22.5 A, the complete spalling of the ceramic coating occurs in the vicinity of the holes. Additionally, a reduction in the inclination angle results in a significant increase in delamination cracking and poorer interface integrity. The interfacial microstructure features of the holes vary with the inclination angle. The large-scale spalling of ceramic coating is prone to occur at the trailing edge when using an inclination angle of 30°. The spattering is susceptible to appear at the entrance of the holes under inclination angles of 60° and 75°, and its composition is primarily Ni, C, Zr, Cr, Nb, Fe, and Cu.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Microstructure and Mechanical Property Inhomogeneities of a Modified AZ80 Magnesium Alloy Wide Plate Under Horizontal Flat Die Extrusion

In the present paper, inhomogeneities in the microstructure and mechanical properties of a modified AZ80 plate under industrial production conditions were investigated. The results indicated that the microstructure of the edge and middle region shows more homogeneous and fine recrystallized grains. Additionally, more coarse recrystallized grains existed between the edge and the middle region. The ultimate tensile strength and yield strength of the edge region of the plate are maximal (287 and 162 MPa), and those near the 1/8 W region are minimal (259 and 152 MPa). The grain size increased from 19.5 to 27.2 μm along the center layer to the surface layer. The ultimate tensile stress (yield stress) increases from 258 (121 MPa) to 284 MPa (176 MPa) in the direction from the surface layer to the middle layer. The microhardness decreased from the surface layer (72HV) to the center layer (64HV). The metal strain state and temperature distribution lead to different degrees of dynamic recrystallization, which causes the microstructure and mechanical properties of the plate.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Electrochemical Corrosion Behavior of 5083 Aluminum Alloy Subjected to Laser Shock Peening

This paper investigates the effect of ablative coating used during laser shock peening (LSP) on corrosion behavior of 5083 aluminum alloy in artificial seawater. Micro-hardness, residual stress, and surface morphology of the specimens were measured. The corrosion behavior was investigated by electrochemical test. Surface corrosion morphologies after electrochemical tests were examined by SEM and EDS. The results show that surface roughness and surface compressive residual stress of the specimen treated by LSP without ablative coating (LSPwC) are lower than that of the specimen treated by LSP with ablative coating under the same laser energy. The open-circuit potentials and self-corrosion potentials of the specimens treated by LSP and LSPwC both shift positively, and the diameters of the capacitor arcs were larger after LSP and LSPwC. The corrosion resistance of 5083 aluminum alloy is improved by LSP and LSPwC. Moreover, superior corrosion resistance is achieved without using the ablative coating during LSP.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Adsorption and Surface Diffusion of Metals on α-Al2O3 for Advanced Manufacturing Applications

Abstract The adsorption and diffusion of Mo and Nb adatoms on the $$\alpha$$ α -Al 2 O 3 (0001) surface were explored using density functional theory-based methods. Adsorption energies of Mo and Nb adatoms at minima sites on the surface were determined. Mo and Nb adatoms prefer to adsorb to the same locations on the surface, and larger adsorption energies calculated for Nb compared to Mo indicate that Nb adatom-surface interactions are stronger than Mo. Using minima adsorption sites as initial and final locations for surface diffusion, energy barriers for diffusion were calculated using the nudged elastic band method. Overall, Mo and Nb follow roughly the same diffusion paths. The diffusion pre-factors for Mo and Nb are similar; however, Mo diffusion has a lower energy barrier and thus a larger diffusion coefficient compared with Nb. These results provide insight into the role of surface diffusion of Mo and Nb adatoms during advanced manufacturing processes.

Biaggne, Austin (ORCID:0000000328074960)↗
DOE OSTI2021

Anomalous X-Ray Scattering and Extended X-Ray Absorption Fine Structure Study of the Local Structure of CrFeCoNiMo x (x = 0.11, 0.18, and 0.23) High-Entropy Alloys

Anomalous x-ray scattering (AXS) and extended x-ray absorption fine structure (EXAFS) were used to determine the local structure of Mo in CrFeCoNiMo x (x = 0.11, 0.18, and 0.23), a high-entropy alloy with a face-centered cubic (FCC) lattice. No superlattice peaks were observed down to the 10 -4 intensity level. This observation along with the nearly constant decrease of the FCC diffraction peaks above the Mo K absorption edge suggests that Mo atoms have no preferred site occupancy in the FCC lattice. Modeling of the EXAFS data suggests a local chemical order in CrFeCoNiMo x , where in Mo-rich samples (e.g., x = 0.23), Mo atoms are preferably surrounded by lighter atoms, such as Cr.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2022

Combined Experimental and Computational Study of Molybdenum and Niobium for Nuclear Sensor Application

Due to their novel electromagnetic and thermal properties, molybdenum (Mo) and niobium (Nb) become optimal temperature sensor materials for nuclear energy applications. We leveraged voltage recorded during a heat ramp to tune a computational method to predict the Seebeck electromotive force (EMF) of Mo and Nb. Using a combined Density Functional Theory (DFT) and Boltzmann Transport Equations (BTE) method the voltage was predicted but did not include the effects of temperature on atomic structure. Combining Ab Initio Molecular Dynamics (AIMD) and BTE included temperature effects on structure optimization and yielded voltages in a good agreement with experiment. Lanthanum (La) and Phosphorus (P) additives in Mo and Nb, respectively, could increase the EMF compared to those of the pure metals. The presence of oxygen (O) in Mo increases the EMF while O in Nb slightly reduces the EMF. Furthermore, our studies suggested that heat treatment-induced structural changes that lead to a reduction in voltage occur not only at the mesoscale as previously understood but also at the atomic scale.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗