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At least 397 records · Page 22

Sample preparation methods for scanning electron microscopy of homogenized Al-Mg-Si billets: A comparative study

Characterization of Mg-Si precipitates is crucial for optimizing the homogenization heat treatment of Al-Mg-Si alloys. Although sample preparation is key for high quality scanning electron microscopy imaging, most common methods lead to dealloying of Mg-Si precipitates. In this article we systematically evaluate different sample preparation methods: mechanical polishing, etching with various reagents, and electropolishing using different electrolytes. We demonstrate that the use of a nitric acid and methanol electrolyte for electropolishing a homogenized Al-Mg-Si alloy prevents the dissolution of Mg-Si precipitates, resulting in micrographs of higher quality. This preparation method is investigated in depth and the obtained scanning electron microscopy images are compared with transmission electron micrographs: the shape and size of Mg-Si precipitates appear very similar in either method. The scanning electron micrographs allow proper identification and measurement of the Mg-Si phases including needles with lengths of roughly 200 nm. These needles are β″ precipitates as confirmed by high resolution transmission electron microscopy. - Highlights: •Secondary precipitation in homogenized 6xxx Al alloys is crucial for extrudability. •Existing sample preparation methods for SEM are improvable. •Electropolishing with nitric acid/methanol yields superior quality in SEM. •The obtained micrographs are compared to TEM micrographs.

36 MATERIALS SCIENCE↗

A comparative study between experimental results and numerical predictions of multi-wall structural response to hypervelocity impact

Over the last three decades, multiwall structures have been analyzed extensively, primarily through experiment, as a means of increasing the protection afforded to spacecraft structure. However, as structural configurations become more varied, the number of tests required to characterize their response increases dramatically. As an alternative, numerical modeling of high-speed impact phenomena is often being used to predict the response of a variety of structural systems under impact loading conditions. This paper presents the results of a preliminary numerical/experimental investigation of the hypervelocity impact response of multiwall structures. The results of experimental high-speed impact tests are compared against the predictions of the HULL hydrodynamic computer code. It is shown that the hypervelocity impact response characteristics of a specific system cannot be accurately predicted from a limited number of HULL code impact simulations. However, if a wide range of impact loadings conditions are considered, then the ballistic limit curve of the system based on the entire series of numerical simulations can be used as a relatively accurate indication of actual system response.

Schonberg, William P.↗

Comparative Study of Magnetic Properties of Nanoparticles by High-Frequency Heat Dissipation and Conventional Magnetometry

The rate of heating of a water-based colloid of uniformly sized 15 nm magnetic nanoparticles by high-amplitude and high-frequency ac magnetic field induced by the resonating LC circuit (nanoTherics Magnetherm) was measured. The results are analyzed in terms of specific energy absorption rate (SAR). Fitting field amplitude and frequency dependences of SAR to the linear response theory, magnetic moment per particles was extracted. The value of magnetic moment was independently evaluated from dc magnetization measurements (Quantum Design MPMS) of a frozen colloid by fitting field-dependent magnetization to Langevin function. The two methods produced similar results, which are compared to the theoretical expectation for this particle size. Additionally, analysis of SAR curves yielded effective relaxation time.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

Comparative Study of foF2 Measurements with IRI-2007 Model Predictions During Extended Solar Minimum

The unusually deep and extended solar minimum of cycle 2324 made it very difficult to predict the solar indices 1 or 2 years into the future. Most of the predictions were proven wrong by the actual observed indices. IRI gets its solar, magnetic, and ionospheric indices from an indices file that is updated twice a year. In recent years, due to the unusual solar minimum, predictions had to be corrected downward with every new indices update. In this paper we analyse how much the uncertainties in the predictability of solar activity indices affect the IRI outcome and how the IRI values calculated with predicted and observed indices compared to the actual measurements.Monthly median values of F2 layer critical frequency (foF2) derived from the ionosonde measurements at the mid-latitude ionospheric station Juliusruh were compared with the International Reference Ionosphere (IRI-2007) model predictions. The analysis found that IRIprovides reliable results that compare well with actual measurements, when the definite (observed and adjusted) indices of solar activityare used, while IRI values based on earlier predictions of these indices noticeably overestimated the measurements during the solar minimum.One of the principal objectives of this paper is to direct attention of IRI users to update their solar activity indices files regularly.Use of an older index file can lead to serious IRI overestimations of F-region electron density during the recent extended solar minimum.

Ionosphere↗

Small Bowel Dose Parameters Predicting Grade ≥3 Acute Toxicity in Rectal Cancer Patients Treated With Neoadjuvant Chemoradiation: An Independent Validation Study Comparing Peritoneal Space Versus Small Bowel Loop Contouring Techniques

Purpose: To determine whether volumes based on contours of the peritoneal space can be used instead of individual small bowel loops to predict for grade ≥3 acute small bowel toxicity in patients with rectal cancer treated with neoadjuvant chemoradiation therapy. Methods and Materials: A standardized contouring method was developed for the peritoneal space and retrospectively applied to the radiation treatment plans of 67 patients treated with neoadjuvant chemoradiation therapy for rectal cancer. Dose-volume histogram (DVH) data were extracted and analyzed against patient toxicity. Receiver operating characteristic analysis and logistic regression were carried out for both contouring methods. Results: Grade ≥3 small bowel toxicity occurred in 16% (11/67) of patients in the study. A highly significant dose-volume relationship between small bowel irradiation and acute small bowel toxicity was supported by the use of both small bowel loop and peritoneal space contouring techniques. Receiver operating characteristic analysis demonstrated that, for both contouring methods, the greatest sensitivity for predicting toxicity was associated with the volume receiving between 15 and 25 Gy. Conclusion: DVH analysis of peritoneal space volumes accurately predicts grade ≥3 small bowel toxicity in patients with rectal cancer receiving neoadjuvant chemoradiation therapy, suggesting that the contours of the peritoneal space provide a reasonable surrogate for the contours of individual small bowel loops. The study finds that a small bowel V15 less than 275 cc and a peritoneal space V15 less than 830 cc are associated with a less than 10% risk of grade ≥3 acute toxicity.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

A comparative study of discrete fracture network and equivalent continuum models for simulating flow and transport in the far field of a hypothetical nuclear waste repository in crystalline host rock

One of the major challenges of simulating flow and transport in the far field of a geologic repository in crystalline host rock is related to reproducing the properties of the fracture network over the large volume of rock with sparse fracture characterization data. Various approaches have been developed to simulate flow and transport through the fractured rock. The approaches can be broadly divided into Discrete Fracture Network (DFN) and Equivalent Continuum Model (ECM). The DFN explicitly represents individual fractures, while the ECM uses fracture properties to determine equivalent continuum parameters. In this paper, we compare DFN and ECM in terms of upscaled observed transport properties through generic fracture networks. The major effort was directed on making the DFN and ECM approaches similar in their conceptual representations. This allows for separating differences related to the interpretation of the test conditions and parameters from the differences between the DFN and ECM approaches. The two models are compared using a benchmark test problem that is constructed to represent the far field (1 × 1 × 1 km 3 ) of a hypothetical repository in fractured crystalline rock. The test problem setting uses generic fracture properties that can be expected in crystalline rocks. The models are compared in terms of the: 1) effective permeability of the domain, and 2) nonreactive solute breakthrough curves through the domain. The principal differences between the models are mesh size, network connectivity, matrix diffusion and anisotropy. We demonstrate how these differences affect the flow and transport. Finally, we identify the factors that should be taken in consideration when selecting an approach most suitable for the site-specific conditions.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

A System Level Comparative Study of SecondarySide Rectifiers for UAV Wireless Power Transfer in High-Altitude Airborne Energy Platforms

Wireless power transfer (WPT) systems for unmanned aerial vehicles (UAVs) must satisfy stringent design requirements to ensure reliable operation under constraints related to efficiency, thermal performance, altitude, weight, and reliability, particularly in airborne and high-altitude environments. Thermal management becomes increasingly challenging at higher altitudes due to reduced air density, while reliability is strongly affected by the number and complexity of active components. The weight and compactness of secondary-side rectifiers directly impact UAV flight endurance and system integration, influencing energy consumption and payload allocation. These factors collectively define the practical feasibility of UAV WPT systems and guide rectifier topology selection. This paper presents a comparative and experimentally validated evaluation framework for secondary-side rectifiers under UAV-specific constraints. Three representative rectifier architectures are analyzed using component-based assessment of weight, thermal behavior, and reliability, together with experimental efficiency measurements obtained from a 1 kW WPT prototype. The results show that the single-switch active rectifier achieves the highest peak efficiency of approximately 93.2% and an overall efficiency of 91%, while also offering advantages in weight and reliability. The findings demonstrate how constraint-oriented analysis, combined with experimental validation, enables informed selection of secondary-side rectifiers for UAV wireless power transfer applications, including emerging airborne and high-altitude platforms.

Asa, Erdem [ORNL] (ORCID:0000000190884812)↗

A comparative study of plasma heating by ion acoustic and modified two-stream instabilities at subcritical quasi-perpendicular shocks

Plasma heating due to the ion acoustic instability and the modified two-stream instability is examined for quasi-perpendicular subcritical shocks. Electron and ion heating is investigated as a function of upstream electron to ion temperature ratio and plasma beta using second-order heating rates. A simple shock model is employed in which the cross-field electron-ion drift speed is adjusted until the total (adiabatic plus anomalous) heating matches that required by the Rankine-Hugoniot relations. Quantities such as the width of the shock and the maximum electric field fluctuations are also calculated, and the results are compared with the ISEE data set of subcritical bow shock crossings. The observed width of the shock, the amount of plasma heating, and the low-frequency electric field intensity are in reasonably good agreement with the calculations for the modified two-stream instability. On the other hand, the wave intensities at higher frequency are about 4 orders of magnitude smaller than those predicted for the ion acoustic instability at saturation, consistent with the fact that the measured shock widths imply cross-field drift speeds that are below threshold for this instability. It is therefore concluded that the dissipation at these shocks is most likely due to the lowest frequency, modified two-stream instability.

Winske, D.↗

Comparative study of flare control laws

A digital 3-D automatic control law was developed to achieve an optimal transition of a B-737 aircraft between various initial glid slope conditions and the desired final touchdown condition. A discrete, time-invariant, optimal, closed-loop control law presented for a linear regulator problem, was extended to include a system being acted upon by a constant disturbance. Two forms of control laws were derived to solve this problem. One method utilized the feedback of integral states defined appropriately and augmented with the original system equations. The second method formulated the problem as a control variable constraint, and the control variables were augmented with the original system. The control variable constraint control law yielded a better performance compared to feedback control law for the integral states chosen.

Nadkarni, A. A.↗

A comparative study of SAR data compression schemes

The amount of data collected from spaceborne remote sensing has substantially increased in the last years. During same time period, the ability to store or transmit data has not increased as quickly. At this time, there is a growing interest in developing compression schemes that could provide both higher compression ratios and lower encoding/decoding errors. In the case of the spaceborne Synthetic Aperture Radar (SAR) earth observation system developed by the French Space Agency (CNES), the volume of data to be processed will exceed both the on-board storage capacities and the telecommunication link. The objective of this paper is twofold: to present various compression schemes adapted to SAR data; and to define a set of evaluation criteria and compare the algorithms on SAR data. In this paper, we review two classical methods of SAR data compression and propose novel approaches based on Fourier Transforms and spectrum coding.

Lambert-Nebout, C.↗

A comparative study of the atomic structures of Ge-doped As 4 S 3 and P 4 Se 3 molecular glasses

The structures of pseudo-binary P-Se and As-S glasses with compositions close to the P 4 Se 3 and As 4 S 3 stoichiometry with a few atom %Ge doping were determined using Monte Carlo simulations constrained by density and x-ray scattering measurements. We find that these glasses consist predominantly of P 4 Se 3 and As 4 S 3 molecules. The Ge doping results in some important differences between the two glasses. The P-Se glass displays significantly higher intermolecular connectivity via P-Se-Ge linkages, consistent with the significantly higher glass transition temperature and lower fragility of this liquid compared to its As-S counterpart. We also speculate that a consequence of this difference in the intermolecular connectivity would be to delay any pressure induced conversion from a molecular to a network structure for the Ge doped P-Se glass compared to the Ge-doped As-S glass.

36 MATERIALS SCIENCE↗

Comparative study of magnetic ordering in bulk and nanoparticles of Sm{sub 0.65}Ca{sub 0.35}MnO{sub 3}: Magnetization and electron magnetic resonance measurements

To explore the effect of size reduction to nanoscale on the hole doped Sm{sub 0.65}Ca{sub 0.35}MnO{sub 3} compound, dc magnetic measurements and electron magnetic resonance (EMR) were done on bulk and nanoparticle samples in the temperature range 10 ≤ T ≤ 300 K. Magnetization measurement showed that the bulk sample undergoes a charge ordering transition at 240 K and shows a mixed magnetic phase at low temperature. However, the nanosample underwent a ferromagnetic transition at 75 K, and the charge ordered state was destabilized on size reduction down to nanoscale. The low-temperature ferromagnetic component is found to be enhanced in nanoparticles as compared to their bulk counterpart. Interestingly around room temperature, bulk particles show higher magnetization where as at low temperature nanoparticles show higher magnetization. Ferromagnetism in the bulk is due to super exchange where as ferromagnetism in nanoparticles is due to uncompensated spins of the surface layer. Temperature variation of EMR parameters correlates well with the results of magnetic measurements. The magnetic behaviour of the nanoparticles is understood in terms of the core shell scenario.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Comparative study of spermatogonial survival after X-ray exposure, high LET (HZE) irradiation or spaceflight

Spermatogonial cell loss has been observed in rats flown on Space Lab 3, Cosmos 1887, Cosmos 2044 and in mice following irradiation with X-ray or with HZE particle beams. Spermatogonial loss is determined by cell counting in maturation stage-6 seminferous tubules. With the exception of iron, laboratory irradiation experiments (with mice) revealed a similar pattern of spermatogonial loss proportional to the radiation dose at levels less than 0.1 Gy. Helium and argon irradiation resulted in a 5-percent loss of spermatogonia after only 0.01 Gy exposure. Significant spermatogonial loss (45 percent) occurred at this radiation level with iron particle beams. The loss of spermatogonia during each spaceflight was less than 10 percent when compared to control (nonflight) animals.

Sapp, W. J.↗

Comparative Study on Deep Learning Methods for Defect Identification and Classification in Composite Aerostructure Material

Aircraft structures are required to have a high level of quality to satisfy their need for light weight, efficient flight, and withstanding high loads over their lifespan. These aerostructures are typically made from composite material due to their good tensile strength and resistance to compression. To ensure their structural integrity, the composite material requires inspection for common flaws such as porosity, delaminations, voids, foreign object debris, and other defects. Ultrasonic testing (UT) is a popular non-destructive inspection (NDI) technique used for effectively evaluating composite material. Current inspection methods rely heavily on human experience and are extremely time consuming. Therefore, there is a need for the development of techniques to reduce the manual inspection time. This work compares the performance of different deep learning-based methods in the identification and classification of defects. Deep learning has shown great promise in numerous fields, and we show its effectiveness in the evaluation of composite aerostructure material. Furthermore, the methods developed here are both highly reliable with a top recall value of 98.63% as well as extremely efficient requiring an average of 4 seconds during the inferencing stage to evaluate new composites.

composites↗

Comparative Study of High-Resolution LysB29(Nε-myristoyl) des(B30) Insulin Structures Display Novel Dynamic Causal Interrelations in Monomeric-Dimeric Motions

The treatment of insulin-dependent diabetes mellitus is characterized by artificial supplementation of pancreatic β-cell ability to regulate sugar levels in the blood. Even though various insulin analogs are crucial for reasonable glycemic control, understanding the dynamic mechanism of the insulin analogs may help to improve the best-protracted insulin analog to assist people with type 1 diabetes (T1D) to live comfortably while maintaining tight glycemic control. Here, we present the high-resolution crystal structure of NN304, known as insulin detemir, to 1.7 Å resolution at cryogenic temperature. We computationally further investigated our crystal structure’s monomeric-dimeric conformation and dynamic profile by comparing it with a previously available detemir structure (PDB ID: 1XDA). Our structure (PDB ID: 8HGZ), obtained at elevated pH, provides electrostatically triggered minor movements in the equilibrium between alternate conformational substates compared to the previous structure, suggesting it might induce an intermediate state in the dissociation pathway of the insulin detemir’s hexamer:dihexamer equilibrium. Supplemented with orientational cross-correlation analysis by a Gaussian network model (GNM), this alternate oligomeric conformation offers the distinct cooperative motions originated by loose coupling of distant conformational substates of a protracted insulin analog that has not been previously observed.

59 BASIC BIOLOGICAL SCIENCES↗

Comparative Study of Three Reconnection X Line Models at the Earth's Dayside Magnetopause Using in Situ Observations

This work examines the large-scale aspects of magnetic field reconnection at the Earth's dayside magnetopause. We use two sets of reconnection events, which are identified mostly by the in situ detection of accelerated and Alfvenic plasma flows. We intercompare three analytical models that predict the reconnection X line location and orientation, namely, the Trattner et al. (2007) and Swisdak and Drake (2007) models and also a modified version of the component merging model. In the first set of reconnection observations, we show three fortuitous, quasi-simultaneous dayside magnetopause crossing events where two widely separated spacecraft detect reconnection signatures, and the X line location and orientation can be inferred from the observations. We compare X line model predictions to those inferred from observations. These three reconnection events indicate the presence of an extended (greater than 7 Earth radii in length), component-type reconnection X line on Earth's dayside magnetopause connecting and structuring the reconnection signatures at locations far apart. In the second set of reconnection events, we analyze the X line models' performance in predicting the observed reconnection outflow direction, i.e., its north-south and/or east-west senses, in a total of 75 single, rather than multiple and quasi-simultaneous, magnetopause crossing events, where reconnection-associated plasma flows were clearly present. We found that the Swisdak and Drake's (2007) X line model performs slightly better, albeit not statistically significant, when predicting both accelerated plasma flow north-south and east-west components in 73% and 53% of the cases, respectively, as compared to the Trattner et al. (2007) model (70% north-south and 42% east-west) and the modified component merging model (66% north-south and 50% east-west).

Souza, V. M.↗

A COMPARATIVE STUDY OF OPTICAL/ULTRAVIOLET VARIABILITY OF NARROW-LINE SEYFERT 1 AND BROAD-LINE SEYFERT 1 ACTIVE GALACTIC NUCLEI

The ensemble optical/ultraviolet (UV) variability of narrow-line Seyfert 1 (NLS1)-type active galactic nuclei (AGNs) is investigated, based on a sample selected from the Sloan Digital Sky Survey (SDSS) Stripe 82 region with multi-epoch photometric scanning data. As a comparison, a control sample of broad-line Seyfert 1 (BLS1)-type AGNs is also incorporated. To quantify properly the intrinsic variation amplitudes and their uncertainties, a novel method of parametric maximum likelihood is introduced that has, as we argued, certain virtues over previously used methods. The majority of NLS1-type AGNs exhibit significant variability on timescales from about 10 days to a few years with, however, smaller amplitudes on average compared to BLS1-type AGNs. About 20 NLS1-type AGNs that show relatively large variations are presented and may deserve future monitoring observations, for instance, reverberation mapping. The averaged structure functions of variability, constructed using the same maximum likelihood method, show remarkable similarity in shape for the two types of AGNs on timescales longer than about 10 days, which can be approximated by a power law or an exponential function. This, along with other similar properties, such as the wavelength-dependent variability, is indicative of a common dominant mechanism responsible for the long-term optical/UV variability of both NLS1- and BLS1-type AGNs. Toward the short timescales, however, there is tentative evidence that the structure function of NLS1-type AGNs continues to decline, whereas that of BLS1-type AGNs flattens with some residual variability on timescales of days. If this can be confirmed, it may suggest that an alternative mechanism, such as X-ray reprocessing, starts to dominate in BLS1-type AGNs, but not in NLS1-type AGNs, on such timescales.

79 ASTRONOMY AND ASTROPHYSICS↗

Viscosity models for pure hydrocarbons at extreme conditions: A review and comparative study

Here, viscosity is a critical fundamental property required in many applications in the chemical and oil industries. In this review the performance of seven select viscosity models, representative of various predictive and correlative approaches, is discussed and evaluated by comparison to experimental data of 52 pure hydrocarbons including straight-chain alkanes, branched alkanes, cycloalkanes, and aromatics. This analysis considers viscosity data to extremely high-temperature, high-pressure conditions up to 573 K and 300 MPa. Unsatisfactory results are found, particularly at high pressures, with the Chung-Ajlan-Lee-Starling, Pedersen-Fredenslund, and Lohrenz-Bray-Clark models commonly used for oil reservoir simulation. If sufficient experimental viscosity data are readily available to determine model-specific parameters, the free volume theory and the expanded fluid theory models provide generally comparable results that are superior to those obtained with the friction theory, particularly at pressures higher than 100 MPa. Otherwise, the entropy scaling method by Lötgering-Lin and Gross is recommended as the best predictive model.

02 PETROLEUM↗