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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 397 records · Page 22
All sourcesNASA NTRSDOE OSTI
DOE OSTI2013

Borehole Calibration Facilities to Support Gamma Logging for Hanford Subsurface Investigation and Contaminant Monitoring - 13516

Repeated gamma logging in cased holes represents a cost-effective means to monitor gamma-emitting contamination in the deep vadose zone over time. Careful calibration and standardization of gamma log results are required to track changes and to compare results over time from different detectors and logging systems. This paper provides a summary description of Hanford facilities currently available for calibration of logging equipment. Ideally, all logging organizations conducting borehole gamma measurements at the Hanford Site will take advantage of these facilities to produce standardized and comparable results. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRS2006

The HST/STIS Next Generation Spectral Library

During Cycles 10, 12, and 13, we obtained STIS G230LB, G430L, and G750L spectra of 378 bright stars covering a wide range in abundance, effective temperature, and luminosity. This HST/STIS Next Generation Spectral Library was scheduled to reach its goal of 600 targets by the end of Cycle 13 when STIS came to an untimely end. Even at 2/3 complete, the library significantly improves the sampling of stellar atmosphere parameter space compared to most other spectral libraries by including the near-UV and significant numbers of metal poor and super-solar abundance stars. Numerous calibration challenges have been encountered, some expected, some not; these arise from the use of the E1 aperture location, non-standard wavelength calibration, and, most significantly, the serious contamination of the near-UV spectra by red light. Maximizing the utility of the library depends directly on overcoming or at least minimizing these problems, especially correcting the UV spectra.

Gregg, M. D.↗
DOE OSTI2021

Assessing laser powder bed fusion system geometric errors through artifact-based methods

Additive manufacturing (AM) machines have developed more rapidly than standardized frameworks needed for the qualification of their geometric capabilities. While some manufacturer-specific methods exist to test capabilities and perform some calibration tasks, standardization efforts have only recently been undertaken in the form of ISO/ASTM 52902. In this study, the recommended methodology prescribed by the standard was implemented by building geometric artifacts with a laser powder bed fusion (LPBF) system and performing dimensional inspection with a coordinate measurement machine (CMM), amongst other methods. Typical dimensional capabilities of the LPBF system are identified and commentary is made on applying metrology methods, detecting geometric error, and diagnosing base causes in the LPBF system. In doing so, favored metrology practices and measurement analysis methods auxiliary to the standard are proposed. Artifact measurements were used to characterize beam positioning error and beam offset error. Methods for decoupling the effects of error sources are proposed. Difficulties in the inspection of AM components are identified, and the effects of various CMM measurement strategies are evaluated. Insights on the application of the new standard are presented, along with commentary as to its fitness for the LPBF process.

Berez, J.↗
DOE OSTI2016

Calculating Measurement Uncertainty of the “Conventional Value of the Result of Weighing in Air”

The conventional value of the result of weighing in air is frequently used in commercial calibrations of balances. The guidance in OIML D-028 for reporting uncertainty of the conventional value is too terse. When calibrating mass standards at low measurement uncertainties, it is necessary to perform a buoyancy correction before reporting the result. When calculating the conventional result after calibrating true mass, the uncertainty due to calculating the conventional result is correlated with the buoyancy correction. We show through Monte Carlo simulations that the measurement uncertainty of the conventional result is less than the measurement uncertainty when reporting true mass. The Monte Carlo simulation tool is available in the online version of this article.

42 ENGINEERING↗
DOE OSTI2025

Assessment of errors in analytic modeling of permanent magnet electron spectrometers for laser-plasma accelerators

Here, we assess the error in three treatments of a critical electron beam diagnostic for laser-plasma acceleration (LPA) experiments: a permanent magnet electron spectrometer. Since LPA electron spectrometers are often difficult to calibrate due to the scarcity of well-characterized, tunable electron beam sources in the appropriate energy range and the mechanical complexity of electron spectrometers, the standard of calibration is Hall probe measurements. We first compare the electron spectrometer performance between SIMION calculations and the Hall probe measurements. We find up to a 60% (<8%) error in determining the absolute energy for electrons below (above) 80 MeV when using the SIMION-modeled magnetic field vs the measured magnetic field due to SIMION overpredicting fringe field strength. The difference in spectrometer energy resolution is within ∼10% between the modeled and measured fields. We then assess a simple block model, which is commonly used. We find that the simple block model presented here sufficiently captures the predicted as-built spectrometer performance for any application provided that the user can tolerate uncertainties on absolute energy determination up to 5% and errors on energy resolution up to 1%.

Electromagnetic optics↗
NASA NTRS2012

A Low Cost Weather Balloon Borne Solar Cell Calibration Payload

Calibration of standard sets of solar cell sub-cells is an important step to laboratory verification of on-orbit performance of new solar cell technologies. This paper, looks at the potential capabilities of a lightweight weather balloon payload for solar cell calibration. A 1500 gr latex weather balloon can lift a 2.7 kg payload to over 100,000 ft altitude, above 99% of the atmosphere. Data taken between atmospheric pressures of about 30 to 15 mbar may be extrapolated via the Langley Plot method to 0 mbar, i.e. AMO. This extrapolation, in principle, can have better than 0.1 % error. The launch costs of such a payload arc significantly less than the much larger, higher altitude balloons, or the manned flight facility. The low cost enables a risk tolerant approach to payload development. Demonstration of 1% standard deviation flight-to-flight variation is the goal of this project. This paper describes the initial concept of solar cell calibration payload, and reports initial test flight results. .

Snyder, David B.↗
DOE OSTI2019

Production of Particle Reference and Quality Control Materials

Maintaining the superior performance of new analytical instrumentation and pushing the boundaries of ever-smaller particle analysis by methods such as secondary ion mass spectrometry (SIMS) has become limited by the availability of certified particle standards for calibration, quality control, and validation. To meet this growing demand for a reliable and universal approach to the generation of uranium particle reference material, the Pacific Northwest National Laboratory (PNNL) and Savannah River National Laboratory (SRNL) are collaborating on a joint venture that establishes a number of chemical pathways to the fabrication, purification, and stabilization of uranium particle material to within a fixed particle size range, and well-characterized isotopics. PNNL particle standards are designed and tailored to meet the criteria essential to the calibration and benchmarking of instruments used in both the non-destructive and destructive assay of particulate material, typically collected from environmental swipe sampling. Previous testing and optimization of this colloidal approach to particulate material has centred on tight size distributions, singular composition and density, uniform morphology, and tailored isotopic abundances. Extensive validation of this material has since been performed, both at the National Institute of Standards and Technology (NIST) and the International Atomic Energy Agency (IAEA), demonstrating its suitability for quality control needs of large geometry (LG)-SIMS analysis. Building on this momentum, the production of low-enriched uranium particle reference material, with specially tailored isotopics, has moved from development to full operation. Herein, various aspects of the production cycle will be discussed, including detailed accounts of the technical methodologies being employed, as well as insights into the sample characterization and acceptance testing requirements.

Nuclear Safeguards, Particle Standards, IAEA↗
NASA NTRS1996

Calibration improvements to electronically scanned pressure systems and preliminary statistical assessment

Orifice-to-orifice inconsistencies in data acquired with an electronically-scanned pressure system at the beginning of a wind tunnel experiment forced modifications to the standard, instrument calibration procedures. These modifications included a large increase in the number of calibration points which would allow a critical examination of the calibration curve-fit process, and a subsequent post-test reduction of the pressure data. Evaluation of these data has resulted in an improved functional representation of the pressure-voltage signature for electronically-scanned pressures sensors, which can reduce the errors due to calibration curve fit to under 0.10 percent of reading compared to the manufacturer specified 0.10 percent of full scale. Application of the improved calibration function allows a more rational selection of the calibration set-point pressures. These pressures should be adjusted to achieve a voltage output which matches the physical shape of the pressure-voltage signature of the sensor. This process is conducted in lieu of the more traditional approach where a calibration pressure is specified and the resulting sensor voltage is recorded. The fifteen calibrations acquired over the two-week duration of the wind tunnel test were further used to perform a preliminary, statistical assessment of the variation in the calibration process. The results allowed the estimation of the bias uncertainty for a single instrument calibration; and, they form the precursor for more extensive and more controlled studies in the laboratory.

Everhart, Joel L.↗
NASA NTRSDate not supplied

The Genesis Non-flight Implant Sample Archive

Introduction: For the past 20 years the Genesis science community has been analyzing solar wind captured in sample collectors now curated at Johnson Space Center (JSC). Non-flown flight like collector materials (non-flight) considered reference material was always allocated by the JSC Genesis team for testing experimental procedures. However, to expedite Genesis science, distribution of non-flown reference materials were also provided by, D. S. Burnett (Genesis PI, Caltech) and A. J. G. Jurewicz (ASU) who were funded to aid all Genesis PIs by providing engineering test materials archived at Caltech pre-flight as well as ion implants into these materials [1]. Implanted materials (non-flight reference, flight-like semiconductor materials, and NIST SRM glass) received from the Caltech collection during a pilot project are being used to develop an accession procedure for the purpose of making these materials available to researchers in the future. These implant samples are important because they can be utilized as measurement standards [2]. This is a work in progress and this work reports progress in documentation and imaging. The pilot program received 63 implanted reference materials with known implanted ions. Genesis Non-Flight Database: The existing non-flight material database was modified to allow for the description of implant sessions and to allow correlation of the implant information to individual specimens. An implant session has three main components: a known ion, a known dose (ion/cm2), and a known energy (keV). Procedure: Laboratory Procedure. Upon receiving non-flight analytical standards (independently calibrated implants), or implant samples (nominally calibrated implants), they will be imaged in their current containers to capture any information written before being brought into the Genesis Sample Laboratory. Documentation is provided by the donor and used for correlating the data between the implant sessions and implant samples. This information is not verified by Genesis Curation. The microscope used to image samples in the laboratory has an automated stage with a stainless-steel plate to hold samples and a camera that utilizes the software Surveyor to take photomosaic images of the implant samples. The camera attached to the microscope is a QICAM High Performance IEEE 1394 FireWire Digital CCD Camera. This setup, shown in Fig. 1, allows for photomosaics of small-scale samples with a 10x objective or 25x objective. Examples of images taken with this microscope setup are shown in Fig.2 and Fig. 3. After imaging, samples get stored in a clean fluoroware container or polypropylene vial depending on sample size for long term storage. Database Procedure. The Genesis Non-Flight Database currently allows for the addition of implant sessions. The required fields for adding an implant session are the implant session ion, the implant session dose, and the implant session energy. There are also fields for the date and vendor of the sessions as well as a field for if the session was calibrated or not. Once an implant session has been inserted into the database, additional documentation from the session can be attached. The database will automatically assign an Implant Session Number. After inserting an implant session, the implanted samples can be inserted. The fields required for an implant sample are the material of the sample and the size of the sample. The Generic name for the implant sample with be automatically generated by the database once it has been inserted. Implant sample numbers begin with 3X to distinguish from flown Genesis sample numbers. There are also fields for processors to add the location (room, cabinet, tray) and container type (fluoroware, polypropylene vial). Once an implant session and an associated sample(s) have been inserted into the database the sample can be then tied to all associated implant sessions. An implant sample can be tied to multiple implant sessions. Future work: For curation, future work consists of creating an online catalogue for implant samples as well as updating the database with more samples as we receive them. For the scientific community these implant samples have many potential uses. For Genesis research, they are directly applicable for testing and, in some cases, as analytical standards. For non-Genesis research, implants (especially calibrated implants) could be used for calibrating other, unique planetary materials [1].

C D Calva↗
DOE OSTI2016

SU-D-209-01: Can Fluoroscopic Air-Kerma Rates Be Reliably Measured with Solid-State Meters?

Purpose: Ionization chambers remain the standard for calibration of air-kerma rate measuring devices. Despite their strong energy-dependent response, solid state radiation detectors are increasingly used, primarily due to their efficiency in making standardized measurements. To test the reliability of these devices in measuring air-kerma rates, we compared ion chambers measurements with solid-state measurements for various mobile fluoroscopes operated at different beam qualities and air-kerma rates. Methods: Six mobile fluoroscopes (GE OEC models 9800 and 9900) were used to generate test beams. Using various field sizes and dose rate controls, copper attenuators and a lead attenuator were placed at the image receptor in varying combinations to generate a range of air-kerma rates. Air-kerma rates at 30 centimeters from the image receptors were measured using two 6-cm{sup 3} ion chambers with electrometers (Radcal, models 1015 and 9015) and two with solid state detectors (Unfors Xi and Raysafe X2). No error messages occurred during measurements. However, about two months later, one solid-state device stopped working and was replaced by the manufacturer. Two out of six mobile fluoroscopic units were retested with the replacement unit. Results: Generally, solid state and ionization chambers agreed favorably well, with two exceptions. Before replacement of the detector, the Xi meter when set in the “RF High” mode deviated from ion chamber readings by factors of 2 and 10 with no message indicating error in measurement. When set in the “RF Low” mode, readings were within −4% to +3%. The replacement Xi detector displayed messages alerting the user when settings were not compatible with air-kerma rates. Conclusion: Air-kerma rates can be measured favorably well using solid-state devices, but users must be aware of the possibility that readings can be grossly in error with no discernible indication for the deviation.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2020

Specifying Calibration of Energy-Measuring Equipment

Instruments and standards need to be calibrated periodically to ensure that their use yields accurate measurements. Calibration needs, however, vary in sophistication, based on user expectations. This white paper reviews calibration terminology and standards, and describes best practices that have been developed for a) calibrating measurement equipment to ensure some known level of accuracy, and b) accrediting calibration service providers. Calibration is discussed in the context of metrological traceability, and excerpts from laboratory scopes of accreditation are shared to reveal the diversity of terminology and format among them. In an effort to aid those who currently calibrate measuring equipment or who have new or changing needs for calibrating measuring equipment, rationale is provided for why a specification might be used to request calibration services that meet specific test needs. Given the growing interest in using data to manage the energy consumption of systems, and the increasing number and variety of systems (e.g., building, computing) that can report such information, use cases requiring energy data are used to facilitate further discussion and provide examples. Commercially available service providers who are accredited for energy-measuring equipment calibration are compared and contrasted, and a specification template that might be used for requesting this calibration is presented. The specification template should be tailored to meet each user’s needs. To illustrate, an example set of energy-measuring-equipment test conditions (reflecting the planned usage of the device to be calibrated) is used to develop a customized calibration specification, and commercially available service providers are assessed in terms of their qualifications for calibration to that particular implementation of the specification template.

47 OTHER INSTRUMENTATION↗
NASA NTRS2002

Calibration Plans for the Global Precipitation Measurement (GPM)

The Global Precipitation Measurement (GPM) is an international effort led by the National Aeronautics and Space Administration (NASA) of the U.S.A. and the National Space Development Agency of Japan (NASDA) for the purpose of improving research into the global water and energy cycle. GPM will improve climate, weather, and hydrological forecasts through more frequent and more accurate measurement of precipitation world-wide. Comprised of U.S. domestic and international partners, GPM will incorporate and assimilate data streams from many spacecraft with varied orbital characteristics and instrument capabilities. Two of the satellites will be provided directly by GPM, the core satellite and a constellation member. The core satellite, at the heart of GPM, is scheduled for launch in November 2007. The core will carry a conical scanning microwave radiometer, the GPM Microwave Imager (GMI), and a two-frequency cross-track-scanning radar, the Dual-frequency Precipitation Radar (DPR). The passive microwave channels and the two radar frequencies of the core are carefully chosen for investigating the varying character of precipitation over ocean and land, and from the tropics to the high-latitudes. The DPR will enable microphysical characterization and three-dimensional profiling of precipitation. The GPM-provided constellation spacecraft will carry a GMI radiometer identical to that on the core spacecraft. This paper presents calibration plans for the GPM, including on-board instrument calibration, external calibration methods, and the role of ground validation. Particular emphasis is on plans for inter-satellite calibration of the GPM constellation. With its Unique instrument capabilities, the core spacecraft will serve as a calibration transfer standard to the GPM constellation. In particular the Dual-frequency Precipitation Radar aboard the core will check the accuracy of retrievals from the GMI radiometer and will enable improvement of the radiometer retrievals. Observational intersections of the core with the constellation spacecraft are essential in applying this technique to the member satellites. Information from core spacecraft retrievals during intersection events will be transferred to the constellation radiometer instruments in the form of improved calibration and, with experience, improved radiometric algorithms. In preparation for the transfer standard technique, comparisons using the Tropical Rainfall Measuring Mission (TRMM) with sun-synchronous radiometers have been conducted. Ongoing research involves study of critical variables in the inter-comparison, such as correlation with spatial-temporal separation of intersection events, frequency of intersection events, variable azimuth look angles, and variable resolution cells for the various sensors.

Bidwell, S. W.↗
NASA NTRS1988

Calibration support for the Earth Observing System Project

The Earth Observing System Project (EOS) program guidelines establishes significantly more stringent requirements on calibrations of instruments. This requirement is driven by the need for long-term continuity of acquired data sets and the use of measurements in interdisciplinary investigations. Personnel from the Standards and Calibration Office have been supporting the Program and Project in interpreting these goals into specific requirements. Contributions to EOS have included participation in the Panel of Experts which produced a list of consensus items necessary for accomplishing an accurate calibration and suggested EOS Project Calibration Policy, and drafting the announcement of opportunity and bidders information package positions on instrument calibration and data product validation. Technical staffing was provided to the NASA delegates to the Committee on Earth Orbiting Satellites (club of space-faring nations) for the standing working group on Calibration and Data Validation.

Guenther, B. W.↗
NASA NTRS2002

Measurement of Precision Geometric Distances to Three Anchor Points in the Local Universe

Our program, funded by a NASA/SARA 3-yr grant, is designed to measure distances directly with accuracies of 5% to three anchor points in the Local Universe. We are attacking this problem on three fronts, using Very Long Baseline Interferometry (VLBI) observations of NGC 4258, M 33, and Sgr A*. We plan to provide distance estimates, with a minimum of systematic uncertainty, that can be used to re-calibrate several 'standard candles,' such as Cepheid and RR Lyrae variables. This will place the Galactic and extragalactic distance scales on much firmer ground. The program will provide crucial, independent checks and calibrations of extragalactic distance measurements, and will contribute to the ultimate success and impact of the HST Key Project on Extragalactic Distances, the Full-Sky Astrometric Mapping Explorer (FAME), and any future NASA astrometric missions. Additionally, since distances are fundamental to astrophysics, our results will affect a large number of general projects on NASA facilities such as the HST (Hubble Space Telescope), CXO (Chandra X-Ray Observatory), and NGST (Next Generation Space Telescope).

Reid, Mark J.↗
NASA NTRS2003

Measurement of Precision Geometric Distances to Three Anchor Points in the Local Universe

As stated in previous reports, our program, funded by a NASA/SARA 3-yr grant, is designed to measure distances directly with accuracies of 5% to three anchor points in the Local Universe. We are attacking this problem on three fronts, using Very Long Baseline Interferometry (VLBI) observations of NGC 4258, M 33, and Sgr A*. We plan to provide distance estimates, with a minimum of systematic uncertainty, that can be used to re- calibrate several "standard candles," such as Cepheid and RR Lyrae variables. This Will place the Galactic and extragalactic distance scales on much firmer ground. The program will provide crucial, independent checks and calibrations of extragalactic distance measurements, and will contribute to the ultimate success and impact of the HST Key Project on Extragalactic Distances and any future NASA astrometric missions. Additionally, since distances are fundamental to astrophysics, our results will affect a large number of general projects on NASA facilities such as the HST, CXO, and JWST.

Reid, Mark J.↗
DOE OSTI2017

The Impact of Indoor and Outdoor Radiometer Calibration on Solar Measurements

This study addresses the effect of calibration methodologies on calibration responsivities and the resulting impact on radiometric measurements. The calibration responsivities used in this study are provided by NREL's broadband outdoor radiometer calibration (BORCAL) and a few prominent manufacturers. The BORCAL method provides outdoor calibration responsivity of pyranometers and pyrheliometers at a 45 degree solar zenith angle and responsivity as a function of solar zenith angle determined by clear-sky comparisons to reference irradiance. The BORCAL method also employs a thermal offset correction to the calibration responsivity of single-black thermopile detectors used in pyranometers. Indoor calibrations of radiometers by their manufacturers are performed using a stable artificial light source in a side-by-side comparison of the test radiometer under calibration to a reference radiometer of the same type. These different methods of calibration demonstrated 1percent to 2 percent differences in solar irradiance measurement. Analyzing these values will ultimately enable a reduction in radiometric measurement uncertainties and assist in developing consensus on a standard for calibration.

14 SOLAR ENERGY↗
DOE OSTI2016

A thioacidolysis method tailored for higher‐throughput quantitative analysis of lignin monomers

Abstract Thioacidolysis is a method used to measure the relative content of lignin monomers bound by β‐O‐4 linkages. Current thioacidolysis methods are low‐throughput as they require tedious steps for reaction product concentration prior to analysis using standard GC methods. A quantitative thioacidolysis method that is accessible with general laboratory equipment and uses a non‐chlorinated organic solvent and is tailored for higher‐throughput analysis is reported. The method utilizes lignin arylglycerol monomer standards for calibration, requires 1–2 mg of biomass per assay and has been quantified using fast‐GC techniques including a Low Thermal Mass Modular Accelerated Column Heater (LTM MACH). Cumbersome steps, including standard purification, sample concentrating and drying have been eliminated to help aid in consecutive day‐to‐day analyses needed to sustain a high sample throughput for large screening experiments without the loss of quantitation accuracy. The method reported in this manuscript has been quantitatively validated against a commonly used thioacidolysis method and across two different research sites with three common biomass varieties to represent hardwoods, softwoods, and grasses.

09 BIOMASS FUELS↗
DOE OSTI2016

The Impact of Indoor and Outdoor Radiometer Calibration on Solar Measurements: Preprint

Accurate solar radiation data sets are critical to reducing the expenses associated with mitigating performance risk for solar energy conversion systems, and they help utility planners and grid system operators understand the impacts of solar resource variability. The accuracy of solar radiation measured by radiometers depends on the instrument performance specification, installation method, calibration procedure, measurement conditions, maintenance practices, location, and environmental conditions. This study addresses the effect of calibration methodologies and the resulting calibration responsivities provided by radiometric calibration service providers such as the National Renewable Energy Laboratory (NREL) and manufacturers of radiometers. Some of these radiometers are calibrated indoors, and some are calibrated outdoors. To establish or understand the differences in calibration methodology, we processed and analyzed field-measured data from these radiometers. This study investigates calibration responsivities provided by NREL's broadband outdoor radiometer calibration (BORCAL) and a few prominent manufacturers. The reference radiometer calibrations are traceable to the World Radiometric Reference. These different methods of calibration demonstrated 1% to 2% differences in solar irradiance measurement. Analyzing these values will ultimately assist in determining the uncertainties of the radiometer data and will assist in developing consensus on a standard for calibration.

14 SOLAR ENERGY↗