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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 397 records · Page 22
All sourcesNASA NTRSDOE OSTI
DOE OSTI2016

Self-aligned grating couplers on template-stripped metal pyramids via nanostencil lithography

We combine nanostencil lithography and template stripping to create self-aligned patterns about the apex of ultrasmooth metal pyramids with high throughput. Three-dimensional patterns such as spiral and asymmetric linear gratings, which can couple incident light into a hot spot at the tip, are presented as examples of this fabrication method. Computer simulations demonstrate that spiral and linear diffraction grating patterns are both effective at coupling light to the tip. The self-aligned stencil lithography technique can be useful for integrating plasmonic couplers with sharp metallic tips for applications such as near-field optical spectroscopy, tip-based optical trapping, plasmonic sensing, and heat-assisted magnetic recording.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2016

A nanoemitter based on a superconducting material

The coherence of an electron beam is crucial for the performance of electron microscopy, coherent diffractive imaging, holography, and many other advanced instrumentation methods that rely on the phase coherence of electron waves. Here we present a reliable method for preparing a niobium nanoemitter, which is thermally and chemically stable. The tip apex is a (100) facet with a lateral dimension of ∼1 nm, surrounded by four (310) facets. Adsorption of one monolayer of noble gas, particularly Xe, onto the nanoemitter greatly enhances the emission current and current stability. This electron source will probably possess both spatial and temporal coherence if the emitter is cooled below the superconducting temperature.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2017

Etching of Cr tips for scanning tunneling microscopy of cleavable oxides

Here, we report a detailed three-step roadmap for the fabrication and characterization of bulk Cr tips for spin-polarized scanning tunneling microscopy. Our strategy uniquely circumvents the need for ultra-high vacuum preparation of clean surfaces or films. First, we demonstrate the role of ex situ electrochemical etch parameters on Cr tip apex geometry, using scanning electron micrographs of over 70 etched tips. Second, we describe the suitability of the in situ cleaved surface of the layered antiferromagnet La 1.4 Sr 1.6 Mn 2 O 7 to evaluate the spin characteristics of the Cr tip, replacing the ultra-high vacuum-prepared test samples that have been used in prior studies. Third, we outline a statistical algorithm that can effectively delineate closely spaced or irregular cleaved step edges, to maximize the accuracy of step height and spin-polarization measurements.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Paschen's curve in microgaps with an electrode surface protrusion

Paschen's curve in microgaps with a hemi-ellipsoidal protrusion on the electrode surface is examined using a two-dimensional fluid model. The breakdown voltage is identified when the discharge enters the subnormal region, according to voltage-current characteristics. It is discovered that the breakdown in a microgap with a surface protrusion on the electrode can result in a combined Paschen's curve, which transits from long-gap (distance between the cathode and anode without the presence of protrusion) behavior at low pressure to short-gap (distance between the protrusion apex to the opposite electrode) behavior at high pressure. As gas pressure decreases, the length of the optimal discharge path increases, automatically moving from the top of the protrusion to its side surface and then to the wider non-protrusion electrode gap. The effects of the protrusion height and radius as well as the discharge polarity on the Paschen's curve are viewed in detail. The effects of the protrusion aspect ratio on field enhancement are also considered. Our report provides insights into the design of microgaps with controlled breakdown voltage across many orders in pressure via engineered electrode morphology.

42 ENGINEERING↗
DOE OSTI2019

Modeling of diamond field emitter arrays for a compact source of high brightness electron beams

Many applications, such as compact accelerators and electron microscopy, demand high brightness electron beams with small source size and ultralow emittance. Diamond emitters manufactured with semiconductor processes can be employed in such compact beam sources. The micrometer-scale pyramid structure of the emitter allows enhancement of the external field compared to that at the substrate, leading to electron emission with small beam size. We investigate the dependence of the field enhancement on the shape of the emitter and the resulting emission characteristics. The beam formation and dynamics are simulated with the LSP particle-in-cell code to obtain the macroscopic observables. To account for the semiconductor charge transport in the bulk material and the tunneling through the surface, a first-principle semiclassical Monte Carlo emission model is developed and applied to the diamond pyramid. Using this Monte Carlo emission model and the result from the geometric field enhancement calculation, we construct a simple model to qualitatively explain the measured emission characteristics. In conclusion, a comparison between our model and experiments indicates that the beam current is mostly emitted at the apex of the emitter.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Pair plasma instability in homogeneous magnetic guide fields

Pair plasmas, collections of both matter and antimatter particles of equal mass, represent a paradigm for the study of basic plasma science, and many open questions exist regarding these unique systems. They are found in many astrophysical settings, such as gamma-ray bursts, and have recently also been produced in carefully designed laboratory experiments. A central research topic in plasma physics is instability; however, unlike their more common ion–electron siblings, pair plasmas are generally thought to be stable to cross field pressure gradients in homogeneous magnetic fields. It is shown here by means of kinetic full-f simulations that, when a pressure gradient is first established, the Gradient-driven Drift Coupling mode is destabilized and becomes turbulent. Force balance is eventually achieved by a combination of flattened pressure profiles due to turbulent transport and establishment of a magnetic field gradient, saturating the growth. During the unstable phase, key physics can be captured by a δf gyrokinetic description, where it is shown analytically and numerically that parallel particle motion results in a coupling of all electromagnetic field components. A fluid model derived therefrom accurately predicts linear eigenmodes and is used to resolve global profile effects. For laser-based electron–positron plasma experiments, prompt instability is predicted with growth times much shorter than plasma lifetimes. Similarly, growth rates are calculated for the planned APEX experiment as well as gamma-ray burst scenarios, suggesting that the instability may contribute to the early evolution of these systems.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2021

Simplified feedback control system for scanning tunneling microscopy

A Scanning Tunneling Microscope (STM) is one of the most important scanning probe tools available to study and manipulate matter at the nanoscale. In a STM, a tip is scanned on top of a surface with a separation of a few Å. Often, the tunneling current between the tip and the sample is maintained constant by modifying the distance between the tip apex and the surface through a feedback mechanism acting on a piezoelectric transducer. This produces very detailed images of the electronic properties of the surface. The feedback mechanism is nearly always made using a digital processing circuit separate from the user computer. Here, we discuss another approach using a computer and data acquisition through the universal serial bus port. We find that it allows successful ultralow noise studies of surfaces at cryogenic temperatures. We show results on different compounds including a type II Weyl semimetal (WTe2), a quasi-two-dimensional dichalcogenide superconductor (2H–NbSe2), a magnetic Weyl semimetal (Co3Sn2S2), and an iron pnictide superconductor (FeSe).

Martín-Vega, Francisco (ORCID:0000000333177833)↗
DOE OSTI2023

Sharp, high numerical aperture (NA), nanoimprinted bare pyramid probe for optical mapping

The ability to correlate optical hyperspectral mapping and high resolution topographic imaging is critically important to gain deep insight into the structure–function relationship of nanomaterial systems. Scanning near-field optical microscopy can achieve this goal, but at the cost of significant effort in probe fabrication and experimental expertise. To overcome these two limitations, we have developed a low-cost and high-throughput nanoimprinting technique to integrate a sharp pyramid structure on the end facet of a single-mode fiber that can be scanned with a simple tuning-fork technique. The nanoimprinted pyramid has two main features: (1) a large taper angle (~70°), which determines the far-field confinement at the tip, resulting in a spatial resolution of 275 nm, an effective numerical aperture of 1.06, and (2) a sharp apex with a radius of curvature of ~20 nm, which enables high resolution topographic imaging. Optical performance is demonstrated through evanescent field distribution mapping of a plasmonic nanogroove sample, followed by hyperspectral photoluminescence mapping of nanocrystals using a fiber-in-fiber-out light coupling mode. Through comparative photoluminescence mapping on 2D monolayers, we also show a threefold improvement in spatial resolution over chemically etched fibers. These results show that the bare nanoimprinted near-field probes provide simple access to spectromicroscopy correlated with high resolution topographic mapping and have the potential to advance reproducible fiber-tip-based scanning near-field microscopy.

47 OTHER INSTRUMENTATION↗
DOE OSTI2025

Impact of threading dislocations on the V-defect assisted lateral carrier injection and recombination in InGaN quantum well LEDs

The nonuniform hole distribution between InGaN quantum wells (QWs) of light emitting diodes (LEDs) has a negative impact on LED efficiency. The uniformity can be increased by using lateral hole injection through sidewalls of V-defects, which form at threading dislocations. However, the inherent coupling between the V-defects and dislocations might affect efficiency of the hole injection and nonradiative recombination. In this work, we have tested the possible impact of the dislocations on the injection and recombination by means of scanning near-field electroluminescence and photoluminescence spectroscopy on single green-emitting InGaN QW LEDs containing large (∼0.5 μm) V-defects. The measurements have not provided any evidence of a lower hole injection efficiency or enhanced nonradiative recombination at the dislocations located at the V-defect facets or their apexes. This shows that large V-defects are excellent volumetric injectors for long wavelength InGaN LEDs. Furthermore, it was established that V-defects are preferential hole injectors even in single quantum well devices. Compared to vertical injection, the V-defect injection allows lowering the operating voltage, which should contribute to an enhanced wall plug efficiency.

42 ENGINEERING↗
DOE OSTI2014

Application of conical 90-degree reflectors for solving the problem of mirror alignment in terahertz-range lasers

We report a study of the conical mirrors with an apex angle of 90° in the resonator of the gas-discharge HCN laser with the radiation wavelength of 337 μm (0.89 THz). Experimental results have shown that such mirrors do not require precise alignment. This makes it possible to improve the radiation stability, significantly simplify the construction of laser and reduce the complexity of its maintenance. (laser applications and other topics in quantum electronics)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2016

Superfocusing of an ultrashort plasmon pulse by a conducting cone

We have shown theoretically the possibility of controlling nanoscale superfocusing of plasmons in a metal conical tip by modulating the carrier frequency of the pulse. The propagation of an ultrashort plasmon pulse in a metal nanoneedle is simulated numerically. The calculation is based on an asymptotic analytical solution of Maxwell's equations for electromagnetic wave propagation in a conical conductor in the vicinity of its apex, obtained by the approximate separation of variables in spherical coordinates. The dependence the field superfocusing on the conductor material, pulse chirp and propagation length is studied. (nanooptics)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2016

Focusing of light at the nanoapex of a metal microtip located above the plane of a dielectric or metal

We study the focusing of the optical electromagnetic radiation energy into a nanoscale spatial region in the vicinity of the nanoapex of a metal microtip located near a dielectric or metal plane. Focusing arises from a symmetric convergence of a surface plasmon TM wave at the nanoapex. The metal boundary near the nanoapex is approximated by a paraboloid of revolution. A numerical model, based on the method of moments, is developed to find the electric field near the tip apex. Calculation results show that, compared to a single tip, the presence of a plane leads to an additional concentration of the electric field near the nanoapex. (nanofocusing)

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2017

Immunogenicity and structures of a rationally designed prefusion MERS-CoV spike antigen

Middle East respiratory syndrome coronavirus (MERS-CoV) is a lineage C betacoronavirus that since its emergence in 2012 has caused outbreaks in human populations with case-fatality rates of ~36%. As in other coronaviruses, the spike (S) glycoprotein of MERS-CoV mediates receptor recognition and membrane fusion and is the primary target of the humoral immune response during infection. Here we use structure-based design to develop a generalizable strategy for retaining coronavirus S proteins in the antigenically optimal prefusion conformation and demonstrate that our engineered immunogen is able to elicit high neutralizing antibody titers against MERS-CoV. We also determined high-resolution structures of the trimeric MERS-CoV S ectodomain in complex with G4, a stem-directed neutralizing antibody. The structures reveal that G4 recognizes a glycosylated loop that is variable among coronaviruses and they define four conformational states of the trimer wherein each receptor-binding domain is either tightly packed at the membrane-distal apex or rotated into a receptor-accessible conformation. As a result, our studies suggest a potential mechanism for fusion initiation through sequential receptor-binding events and provide a foundation for the structure-based design of coronavirus vaccines.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2025

Allosteric inhibition of the IZUMO1–JUNO fertilization complex by the naturally occurring antisperm antibody OBF13

Sperm IZUMO1 binds to egg JUNO, and this interaction is essential for mammalian fertilization. Isolated from a female mouse immunized with syngeneic sperm, the antisperm antibody OBF13 recognizes IZUMO1 and inhibits murine fertilization. How OBF13 interferes with sperm–egg interactions was unknown. Here, we present the X-ray crystal structure of IZUMO1 in complex with OBF13. OBF13 binds to the apex of the four-helix domain of IZUMO1, distant from the JUNO-binding site. Our crystal structure of OBF13-bound IZUMO1 resembles apo-IZUMO1 and differs from the structure of IZUMO1 in complex with JUNO. We identify that OBF13 carries a low level of somatic hypermutation, and through deep mutational scanning, we engineer an affinity-enhanced OBF13 variant. This OBF13 variant single-chain fragment variable decreases the apparent affinity of IZUMO1 for membrane-bound murine JUNO and blocks the binding of acrosome-reacted sperm to eggs, thereby preventing fertilization. We propose allostery between the OBF13 epitope and the JUNO-binding site. OBF13 inhibits a conformational change in IZUMO1, preventing fusion-competent sperm from adhering to murine eggs during fertilization. Surprisingly, murine IZUMO1 binds to hamster JUNO with an affinity ~20-fold higher than to murine JUNO. The decreased affinity caused by OBF13 of murine IZUMO1 for hamster JUNO is sufficient for murine sperm to bind to and fuse with hamster eggs. Our studies provide a structural and mechanistic framework for species-specific, allosteric inhibition of IZUMO1 by a naturally occurring antisperm antibody and offer insights into the development of immunocontraceptives.

Science & Technology - Other Topics↗
DOE OSTI2023

Cellulose synthase-like D movement in the plasma membrane requires enzymatic activity

Cellulose Synthase-Like D (CSLD) proteins, important for tip growth and cell division, are known to generate β-1,4-glucan. However, whether they are propelled in the membrane as the glucan chains they produce assemble into microfibrils is unknown. To address this, we endogenously tagged all eight CSLDs in Physcomitrium patens and discovered that they all localize to the apex of tip-growing cells and to the cell plate during cytokinesis. Actin is required to target CSLD to cell tips concomitant with cell expansion, but not to cell plates, which depend on actin and CSLD for structural support. Like Cellulose Synthase (CESA), CSLD requires catalytic activity to move in the plasma membrane. We discovered that CSLD moves significantly faster, with shorter duration and less linear trajectories than CESA. In contrast to CESA, CSLD movement was insensitive to the cellulose synthesis inhibitor isoxaben, suggesting that CSLD and CESA function within different complexes possibly producing structurally distinct cellulose microfibrils.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2014

Detached dust shell around Wolf-Rayet star WR60-6 in the young stellar cluster VVV CL036

The discovery of a detached dust shell around the Wolf-Rayet (WR) star WR60-6 in the young stellar cluster VVV CL036 is reported. This shell is uncovered through the Spitzer-MIPS 24 μm image, where it appears brightest, and it is invisible at shorter wavelengths. Using new APEX observations and other data available from the literature, we have estimated some of the shell parameters: the inner and outer radii of 0.15 and 0.90 pc, respectively; the overall systemic velocity of the molecular {sup 12}CO(3 → 2) emission of –45.7 ± 2.3 km s{sup –1}; an expansion velocity of the gas of 16.3 ± 1 km s{sup –1}; the dust temperature and opacity of 122 ± 12 K and 1.04, respectively; and an age of 2.8 × 10{sup 4} yr. The WR star displays some cyclic variability. The mass computed for the WR60-6 nebula indicates that the material was probably ejected during its previous stages of evolution. In addition, we have identified a bright spot very close to the shell, which can be associated with the Midcourse Space Experiment source G312.13+00.20.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2014

A CO survey in planet-forming disks: Characterizing the gas content in the epoch of planet formation

We carried out a {sup 12}CO(3-2) survey of 52 southern stars with a wide range of IR excesses (L {sub IR}/L {sub *}) using the single-dish telescopes APEX and ASTE. The main aims were (1) to characterize the evolution of molecular gas in circumstellar disks using L {sub IR}/L {sub *} values as a proxy of disk dust evolution, and (2) to identify new gas-rich disk systems suitable for detailed study with ALMA. About 60% of the sample (31 systems) have L {sub IR}/L {sub *} > 0.01, typical of T Tauri or Herbig AeBe stars, and the rest (21 systems) have L {sub IR}/L {sub *} < 0.01, typical of debris disks. We detect CO(3-2) emission from 20 systems, and 18 (90%) of these have L {sub IR}/L {sub *} > 0.01. However, the spectra of only four of the newly detected systems appear free of contamination from background or foreground emission from molecular clouds. These include the early-type stars HD 104237 (A4/5V, 116 pc) and HD 98922 (A2 III, 507 pc, as determined in this work), where our observations reveal the presence of CO-rich circumstellar disks for the first time. Of the other detected sources, many could harbor gaseous circumstellar disks, but our data are inconclusive. For these two newly discovered gas-rich disks, we present radiative transfer models that simultaneously reproduce their spectral energy distributions and the {sup 12}CO(3-2) line profiles. For both of these systems, the data are fit well by geometrically flat disks, placing them in the small class of non-flaring disks with significant molecular gas reservoirs.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2013

G048.66-0.29: PHYSICAL STATE OF AN ISOLATED SITE OF MASSIVE STAR FORMATION

We present continuum observations of the infrared dark cloud (IRDC) G48.66-0.22 (G48) obtained with Herschel, Spitzer, and APEX, in addition to several molecular line observations. The Herschel maps are used to derive temperature and column density maps of G48 using a model based on a modified blackbody. We find that G48 has a relatively simple structure and is relatively isolated; thus, this IRDC provides an excellent target to study the collapse and fragmentation of a filamentary structure in the absence of complicating factors such as strong external feedback. The derived temperature structure of G48 is clearly non-isothermal from cloud to core scale. The column density peaks are spatially coincident with the lowest temperatures ({approx}17.5 K) in G48. A total cloud mass of {approx}390 M{sub Sun} is derived from the column density maps. By comparing the luminosity-to-mass ratio of 13 point sources detected in the Herschel/PACS bands to evolutionary models, we find that two cores are likely to evolve into high-mass stars (M{sub *} {>=} 8 M{sub Sun }). The derived mean projected separation of point sources is smaller than in other IRDCs but in good agreement with theoretical predications for cylindrical collapse. We detect several molecular species such as CO, HCO{sup +}, HCN, HNC, and N{sub 2}H{sup +}. CO is depleted by a factor of {approx}3.5 compared to the expected interstellar abundance, from which we conclude that CO freezes out in the central region. Furthermore, the molecular clumps, associated with the submillimeter peaks in G48, appear to be gravitationally unbound or just pressure confined. The analysis of critical line masses in G48 shows that the entire filament is collapsing, overcoming any internal support.

79 ASTRONOMY AND ASTROPHYSICS↗