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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 379 records · Page 21
All sourcesNASA NTRSDOE OSTI
NASA NTRS2018

Hall Current Plasma Source Having a Center-Mounted or a Surface-Mounted Cathode

A miniature Hall current plasma source apparatus having magnetic shielding of the walls from ionized plasma, an integrated discharge channel and gas distributor, an instant-start hollow cathode mounted to the plasma source, and an externally mounted keeper, is described. The apparatus offers advantages over other Hall current plasma sources having similar power levels, including: lower mass, longer lifetime, lower part count including fewer power supplies, and the ability to be continuously adjustable to lower average power levels using pulsed operation and adjustment of the pulse duty cycle. The Hall current plasma source can provide propulsion for small spacecraft that either do not have sufficient power to accommodate a propulsion system or do not have available volume to incorporate the larger propulsion systems currently available. The present low-power Hall current plasma source can be used to provide energetic ions to assist the deposition of thin films in plasma processing applications.

Martinez, Rafael A.↗
NASA NTRSDate not supplied

Environmental and Polarization Characterizations of E-Beam Plasma-Based AlF 3 -Passivated Aluminum Mirrors for Astronomical Telescopes

Astronomical space telescopes to study astrophysical phenomena from the far ultraviolet (FUV) to the near infrared (NIR) will require mirror coatings with high reflectance over this entire spectral region. While coatings for the optical and NIR part of the spectrum are fairly well developed with proven performance, the FUV range has presented significant challenges, particularly below 120nm. Recent developments in electron-beam (e-Beam) generated plasma treatment in a SF 6 environments has enabled the effective passivation of aluminum (Al) coatings for applications in the FUV, by native oxide removal and the formation of a AlF 3 passivation layer which could be tuned to any desired AlF 3 thickness. These results have been produced through a collaboration between the Goddard Space Flight Center (GSFC) and the Naval Research Laboratory (NRL). The passivation experiments have been carried out using the Large Area Plasma Processing System (LAPPS) at NRL using bare aluminum samples and provided by the coating group at GSFC. This novel procedure has demonstrated improved Al mirrors with state-of-the-art FUV reflectivity (e.g. R=91% at 121.6nm). In this paper, we will be reporting on environmental testing, micro-roughness, as well as polarization studies of these E-beam treated samples. These characterizations are being done in order to advance the Technology Readiness Level (TRL) for these Al+AlF 3 mirror coatings produced at LAPPS. The ultimate goal is to demonstrate the promise of using this coating technology to deliver reflectance performance plus stability and uniformity over a large area for a future IR/O/UV space telescope observatory.

FUV reflectance↗
DOE OSTI2023

Aqueous based nanoparticle ink

Water-based nanoparticle inks may be formulated to be compatible with printed electronic direct-write methods. The water-based nanoparticle inks may include a functional material (nanoparticle) in combination with an appropriate solvent system. A method may include dispersing nanoparticles in a solvent and printing a circuit in an aerosol jet process or plasma jet process.

Fujimoto, Kiyo↗
NASA NTRS1983

The variable polarity plasma arc welding process: Its application to the Space Shuttle external tank

The technical history of the variable polarity plasma arc (VPPA) welding process being introduced as a partial replacement for the gas shielded tungsten arc process in assembly welding of the space shuttle external tank is described. Interim results of the weld strength qualification studies, and plans for further work on the implementation of the VPPA process are included.

Nunes, A. C., Jr.↗
NASA NTRS1989

Space plasma physics: I - Stationary processes

The physics of stationary processes in space plasmas is examined theoretically in an introduction intended for graduate students. The approach involves the extensive use of numerical simulations. Chapters are devoted to fundamental principles, small-amplitude waves, and the stationary solar plasma system; typical measurement data and simulation results are presented graphically.

Hasegawa, Akira↗
NASA NTRS1983

The expansion of a plasma into a vacuum - Basic phenomena and processes and applications to space plasma physics

In this review attention is called to basic phenomena and physical processes involved in the expansion of a plasma into a vacuum, or the expansion of a plasma into a more tenuous plasma, in particular the fact that upon the expansion, ions are accelerated and reach energies well above their thermal energy. Also, in the process of the expansion a rarefaction wave propagates into the ambient plasma, an ion front moves into the expansion volume, and discontinuities in plasma parameters occur. The physical processes which cause the above phenomena are discussed, and their possible application is suggested for the case of the distribution of ions and electrons (hence plasma potential and electric fields) in the wake region behind artificial and natural obstacles moving supersonically in a rarefied space plasma. To illustrate this, some in situ results are reexamined. Directions for future work in this area via the utilization of the Space Shuttle and laboratory work are also mentioned.

Wright, K. H., Jr.↗
NASA NTRS1991

Collisional processes in cometary plasmas

The interaction of the solar wind with comets is initiated at large distances from the nucleus by the ionization of cometary neutrals. The resulting contamination of the solar wind with cometary ions mass-loads the solar wind flow, causing it to slow down. The plasma-comet interaction is largely collisionless at large cometocentric distances. However, collisional processes become important in the inner coma (within the cometopause). Collisional processes include charge-transfer between solar wind protons and neutrals, ion-neutral friction, electron and ion thermal cooling, and ion-neutral chemistry. For example, the magnetometer on the Giotto spacecraft observed a diamagnetic cavity near closest approach. This cavity is a consequence of the balance between an inward-directed magnetic pressure gradient force and an outward ion-netural frictional force. Thermalization of the cometary ion distribution function by Coulomb collisions is another important process in the inner coma of an active comet.

Cravens, T. E.↗
NASA NTRS1999

The Magnetospheric Multiscale Mission...Resolving Fundamental Processes in Space Plasmas

The Magnetospheric Multiscale (MMS) mission is a multiple-spacecraft Solar-Terrestrial Probe designed to study the microphysics of magnetic reconnection, charged particle acceleration, and turbulence in key boundary regions of Earth's magnetosphere. These three processes, which control the flow of energy, mass, and momentum within and across plasma boundaries, occur throughout the universe and are fundamental to our understanding of astrophysical and solar system plasmas. Only in Earth's magnetosphere, however, are they readily accessible for sustained study through in-situ measurement. MMS will employ five co-orbiting spacecraft identically instrumented to measure electric and magnetic fields, plasmas, and energetic particles. The initial parameters of the individual spacecraft orbits will be designed so that the spacecraft formation will evolve into a three-dimensional configuration near apogee, allowing MMS to differentiate between spatial and temporal effects and to determine the three dimensional geometry of plasma, field, and current structures. In order to sample all of the magnetospheric boundary regions, MMS will employ a unique four-phase orbital strategy involving carefully sequenced changes in the local time and radial distance of apogee and, in the third phase, a change in orbit inclination from 10 degrees to 90 degrees. The nominal mission operational lifetime is two years. Launch is currently scheduled for 2006.

Curtis, S.↗
DOE OSTI2024

Autonomous hybrid optimization of a SiO 2 plasma etching mechanism

Computational modeling of plasma etching processes at the feature scale relevant to the fabrication of nanometer semiconductor devices is critically dependent on the reaction mechanism representing the physical processes occurring between plasma produced reactant fluxes and the surface, reaction probabilities, yields, rate coefficients, and threshold energies that characterize these processes. The increasing complexity of the structures being fabricated, new materials, and novel gas mixtures increase the complexity of the reaction mechanism used in feature scale models and increase the difficulty in developing the fundamental data required for the mechanism. This challenge is further exacerbated by the fact that acquiring these fundamental data through more complex computational models or experiments is often limited by cost, technical complexity, or inadequate models. In this paper, we discuss a method to automate the selection of fundamental data in a reduced reaction mechanism for feature scale plasma etching of SiO 2 using a fluorocarbon gas mixture by matching predictions of etch profiles to experimental data using a gradient descent (GD)/Nelder–Mead (NM) method hybrid optimization scheme. These methods produce a reaction mechanism that replicates the experimental training data as well as experimental data using related but different etch processes.

36 MATERIALS SCIENCE↗
NASA NTRS1991

Physical processes in the plasma mantle of Venus

The results are presented of a study, which analyzed data from 10 Pioneer Venus orbits in order to see whether similar wave particle interaction processes also exist in the corresponding region around Venus. The first conclusion is that the apparent physical processes in the mantle are indeed similar around Venus and Mars. The planetary thermal O(+) ions outside the ionopause interact with the shocked solar wind and excite electrostatic waves close to the lower hybrid frequency. These waves propagate inwards, heating first the electron and deeper down in the ionosphere the thermal ion population. The observed superthermal ions are believed to be the product of this wave particle interaction process. It is also concluded that the wave energy transferred to the thermal electrons is of the right magnitude (about 4 x 10 exp 9 eV/sq cm s) to provide the supplemental heat source necessary to reconcile observed and calculated electron temperatures in the ionosphere.

Szego, K.↗
NASA NTRS1982

Processes in relativistic plasmas

The establishment and maintenance of a Boltzmann distribution in particle kinetic energies is investigated for a plasma with theta = KTe/mc-squared much greater than unity, where m is the electron mass. It is shown that thermalization of the electron gas by binary collisions is not sufficiently effective to maintain the equilibrium distribution when other processes that perturb the equilibrium are taken into account. Electron-positron pair production in electron-electron and electron-ion collisions, and perturbations of a Boltzmann distribution by nonthermal processes are evaluated. Thermalization by means of other mechanisms, such as interaction with plasma waves is discussed, and the opacity of a relativistic plasma is computed for Compton scattering, pair production in the fields of electrons and ions, inverse bremsstrahlung, and synchrotron self-absorption.

Gould, R. J.↗
DOE OSTI2024

Low-temperature etching of silicon oxide and silicon nitride with hydrogen fluoride

Etching of high aspect ratio features into alternating SiO 2 and SiN layers is an enabling technology for the manufacturing of 3D NAND flash memories. In this paper, we study a low-temperature or cryo plasma etch process, which utilizes HF gas together with other gas additives. Compared with a low-temperature process that uses separate fluorine and hydrogen gases, the etching rate of the SiO 2 /SiN stack doubles. Both materials etch faster with this so-called second generation cryo etch process. Pure HF plasma enhances the SiN etching rate, while SiO 2 requires an additional fluorine source such as PF 3 to etch meaningfully. Further, the insertion of H 2 O plasma steps into the second generation cryo etch process boosts the SiN etching rate by a factor of 2.4, while SiO 2 etches only 1.3 times faster. We observe a rate enhancing effect of H 2 O coadsorption in thermal etching experiments of SiN with HF. Ammonium fluorosilicate (AFS) plays a salient role in etching of SiN with HF with and without plasma. AFS appears weakened in the presence of H 2 O. Density functional theory calculations confirm the reduction of the bonding energy when NH 4 F in AFS is replaced by H 2 O.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2021

Unconventional Materials Processing Using Spark Plasma Sintering

Spark plasma sintering (SPS) has gained recognition in the last 20 years for its rapid densification of hard-to-sinter conventional and advanced materials, including metals, ceramics, polymers, and composites. Herein, we describe the unconventional usages of the SPS technique developed in the field. The potential of various new modifications in the SPS technique, from pressureless to the integration of a novel gas quenching system to extrusion, has led to SPS’ evolution into a completely new manufacturing tool. The SPS technique’s modifications have broadened its usability from merely a densification tool to the fabrication of complex-shaped components, advanced functional materials, functionally gradient materials, interconnected materials, and porous filter materials for real-life applications. The broader application achieved by modification of the SPS technique can provide an alternative to conventional powder metallurgy methods as a scalable manufacturing process. The future challenges and opportunities in this emerging research field have also been identified and presented.

36 MATERIALS SCIENCE↗
DOE OSTI2026

Mechanical Behavior of Neutron Irradiated Refractory Multi-Principal Element Alloys Processed via Spark Plasma Sintering

The search for advanced materials capable of withstanding the extreme conditions of Generation IV reactors is a critical area in materials science research. These reactors operate under severe environments, including high temperatures, corrosion, stress, and irradiation damage. Consequently, there is a need for innovative alloy systems to ensure the reliability and longevity of proposed Generation IV reactor components. Refractory multi-principal-element alloys (RMPEA) have emerged as a promising candidate due to their exceptional properties. These alloys, characterized by their composition of multiple principal elements in near-equiatomic ratios, exhibit superior resistance to irradiation damage, reduced void swelling, enhanced microstructural stability, and minimal irradiation-induced hardening. While initial studies on RMPEAs have shown promising results, most research has been limited to thin films, nanocrystalline microstructures, and ion irradiation, which do not accurately represent the behavior of bulk materials. To address this gap, our research focused on the neutron irradiation of bulk RMPEAs. We aim to conduct comprehensive post-irradiation examinations (PIE) of RMPEAs irradiated at the Advanced Test Reactor at Idaho National Laboratory. The RMPEAs were synthesized using spark plasma sintering (SPS) with mechanically alloyed metallurgical powder. The RMPEA specimens are a MoNbTi alloy system with additions of -Zr, and -ZrV. Furthermore, PIE consisted of mechanical testing and advanced materials characterization. The mechanical testing consisted of sub-sized tensile testing, micro- and nano- indentation. Microstructural characterization included scanning electron microscopy and transmission electron microscopy. Mechanical testing coupled with advanced microscopy techniques provides insight into phase morphology and its effects on the mechanical properties of the RMPEA specimens. The results indicate that both pristine and irradiated RMPEA specimens exhibited brittle behavior during tensile testing, which can be attributed to their heterogeneous microstructure. The SPS manufacturing process did not include any post treatment, which resulted in a heterogeneous microstructure. Energy-dispersive X-ray spectroscopy revealed the presence of intermetallic such as laves phases within the microstructure. Specifically, Ti-rich precipitates were observed in the MoNbTi specimen, while Mo-rich precipitates were found in the MoNbTiZrV specimen. Nano-hardness testing of pristine samples showed that the laves phases exhibited higher hardness values compared to the matrix phase, suggesting that precipitate hardening is likely the dominant hardening mechanism in these specimens. The results from this work will be used to build a finite element model to predict mechanical behavior of future MPEA compositions. Thus, enabling for a streamlined approach to developing novel MPEAs for the nuclear industry.

36 - MATERIALS SCIENCE↗