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At least 379 records · Page 21

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NASA NTRSDate not supplied

Silver Foam: A Novel Approach for Long-Term Passive-Dosing of Biocide in Spacecraft Potable Water Systems – Update 2022

A spacecraft water disinfection system suitable for extended length space exploration should meet a list of requirements. It should prevent or control the growth of microbes, prevent or limit biofilm formation, and prevent microbiologically influenced corrosion. In addition, the system should have minimal maintenance requirements, be chemically compatible with all materials in contact with the water, be safe for human consumption, and be suitable to be shared across international spacecraft platforms and mission architectures. Silver ions are a proven broad-spectrum potable water biocide under investigation for future exploration missions. The competing technology for dosing silver ions in future water systems is based on actively dosing the ions via electrolytic production. Several challenges with this approach have prompted additional investigations into alternative dosing techniques. Control-release technology is an attractive option for developing a high-reliability passive silver dosing device. This paper describes the continued development of a nanoparticle/polyurethane (NP/PU) composite foam for the controlled release of silver ions and is intended to build upon previously published work. This paper provides the technical background and performance results (wash testing and ongoing long-term silver ion release testing) from the silver chloride (AgCl) NP/PU composite foams. The goal of the project is to develop a stable and reliable passive-dosing silver ion release device for use in future spacecraft potable water systems.

Tesia D Irwin↗

NASA NTRS2013

Testing of the Advanced Stirling Radioisotope Generator Engineering Unit at NASA Glenn Research Center

The Advanced Stirling Radioisotope Generator (ASRG) is a high-efficiency generator being developed for potential use on a Discovery 12 space mission. Lockheed Martin designed and fabricated the ASRG Engineering Unit (EU) under contract to the Department of Energy. This unit was delivered to NASA Glenn Research Center in 2008 and has been undergoing extended operation testing to generate long-term performance data for an integrated system. It has also been used for tests to characterize generator operation while varying control parameters and system inputs, both when controlled with an alternating current (AC) bus and with a digital controller. The ASRG EU currently has over 27,000 hours of operation. This paper summarizes all of the tests that have been conducted on the ASRG EU over the past 3 years and provides an overview of the test results and what was learned.

Lewandowski, Edward J.↗

NASA NTRSDate not supplied

20 Watt 20 Kelvin Reverse Turbo-Brayton Cycle Cryocooler Testing and Applications

Long-term storage of cryogens is an essential capability required to enable NASA’s anticipated missions to both the Lunar and Martian surfaces. A key component to furthering these capabilities is the development of a high capacity, low temperature cryocooler to allow for zero-boil-off storage of liquid hydrogen propellant. The technology being developed by NASA to meet this objective is a reverse turbo-Brayton cycle cryocooler capable of removing 20 Watts (W) of heat at 20 Kelvin (K). This hardware was recently tested at Creare LLC in a vacuum chamber to simulate a relevant mission environment. This testing demonstrated the hardware’s functionality and established a baseline for the cryocooler’s capabilities. Additional NASA led characterization testing is underway and will provide a broader picture of the operational capability of the cryocooler. This paper will discuss the results of this recent testing, along with highlighting the applications for high capacity cryocoolers on future NASA missions, such as Nuclear Thermal Propulsion (NTP) and a sustainable lunar architecture.

Cryocooler↗

NASA NTRS1980

Automatic control of NASA Langley's 0.3-meter cryogenic test facility

Experience during the past 6 years of operation of the 0.3-meter transonic cryogenic tunnel at the NASA Langley Research Center has shown that there are problems associated with efficient operation and control of cryogenic tunnels using manual control schemes. This is due to the high degree of process crosscoupling between the independent control variables (temperature, pressure, and fan drive speed) and the desired test condition (Mach number and Reynolds number). One problem has been the inability to maintain long-term accurate control of the test parameters. Additionally, the time required to change from one test condition to another has proven to be excessively long and much less efficient than desirable in terms of liquid nitrogen and electrical power usage. For these reasons, studies have been undertaken to: (1) develop and validate a mathematical model of the 0.3-meter cryogenic tunnel process, (2) utilize this model in a hybrid computer simulation to design temperature and pressure feedback control laws, and (3) evaluate the adequacy of these control schemes by analysis of closed-loop experimental data. This paper will present the results of these studies.

Thibodeaux, J. J.↗

DOE OSTI2023

Microstructural Investigation of Precipitation Treated A709 Test Samples

This report presents the microstructural characterization using scanning transmission electron microscopy (STEM) of two creep-tested ESR1150-PT specimens, one short-term and one long-term. The results show that during creep testing, the microstructure of the A709 ESR1150-PT material continues to evolve as expected due to the synergistic effect of strain, temperature and time. Key features include dislocation forest and cell structures, precipitates on grain boundaries, precipitates randomly within grains, and precipitates associated with dislocations. In addition, the STEM study of one ESR1100-SA specimen that has been tested to rupture at a relatively low temperature (550°C) for a relatively long term (16226 h) is also presented. The results show that there is a high density of very fine nano precipitates form on dislocations.

36 MATERIALS SCIENCE↗

NASA NTRS2015

Overview of the 2nd Gen 3.7m HIAD Static Load Test

To support NASAs long term goal of landing humans on Mars, technologies which enable the landing of heavy payloads are being developed. Current entry, decent, and landing technologies are not practical for human class payloads due to geometric constraints dictated by current launch vehicle fairing limitations. Therefore, past and present technologies are now being explored to provide a mass and volume efficient solution to atmospheric entry, including Hypersonic Inflatable Aerodynamic Decelerators (HIADs). In October of 2014, a 3.7m HIAD inflatable structure with an integrated flexible thermal protection sys-tem (F-TPS) was subjected to a static load test series to verify the designs structural performance. The 3.7m HIAD structure was constructed in a 70 deg sphere-cone stacked-toroid configuration using eight inflatable tori, which were joined together using adhesives and high strength textile webbing to help distribute the loads throughout the inflatable structure. The inflatable structure was fabricated using 2nd generation structural materials that permit an increase in use temperature to 400 C+ as compared to the 250 C limitation of the 1st generation materials. In addition to the temperature benefit, these materials also offer a 40 reduction in structure mass. The 3.7m F-TPS was fabricated using high performance materials to protect the inflatable structure from heat loads that would be seen during atmospheric entry. The F-TPS was constructed of 2nd generation TPS materials increasing its heating capability from 35W sq cm to over 100W sq cm. This test article is the first stacked-torus HIAD to be fabricated and tested with a 70 deg sphere-cone. All previous stacked-torus HIADs have employed a 60o sphere-cone. To perform the static load test series, a custom test fixture was constructed. The fixture consisted of a structural tub rim with enough height to allow for dis-placement of the inflatable structure as loads were applied. The tub rim was attached to the floor to provide an airtight seal. The center body of the inflatable structure was attached to a pedestal mount as seen in Figure 1. Using an impermeable membrane seal draped over the test article, partial vacuum was pulled beneath the HIAD, resulting in a uniform static pressure load applied to the outer surface. During the test series an extensive amount of instrumentation was used to characterize deformed shape, shoulder deflection, strap loads, and cord loads as a function of structural configuration and applied static load. In this overview, the 3.7m HIAD static load test series will be discussed in detail, including the 3.7m HIAD inflatable structure and flexible TPS design, test setup and execution, and finally results and conclusions from the test series.

HIAD↗

DOE OSTI2021

Hydraulic Response to Thermal Stimulation Efforts at Raft River Based on Stepped Rate Injection Testing

The injection well stimulation project at the Raft River geothermal field tests the effect of long-term cold water injection and high pressure injection on well injectivity, improvements to which could reduce operating costs. The primary data for analysis and interpretation of the injection test are step-rate flow tests run before each new phase of the injection. These tests were analyzed using a combination of standard pump-test analytical solution methods and methods developed expressly for the observed conditions. The stepped rate injection tests, combined with long-term flow and pressure response data suggest that the well is located within a fractured formation of low transmissivity but high storativity. These calculated parameters appeared to increase with pressure during the first injection test and the higher values were reproduced during the second stepped rate test. Calculated transmissivity and storativity are on the order of 4E-5 m cm 2 and 1E-4 m Pa -1 , respectively. The apparent pressure dependence of fitted hydraulic parameters may reflect near-well fracture compliance that increased the effective radius of the wellbore during the first test. While the type curve fit analysis also suggests that the reservoir behaves as a uniformly fractured reservoir with a radial flow regime, the hydraulic parameters indicate that condition may exist only a very limited distance (<10 m) from the well. Longer-term pressure response suggests that flow in the system effectively reaches steady state in a period of less than a day, which may reflect pressure stabilization resulting from pressure-dependent permeability or a region of much higher permeability located with a few meters of the well. The transmissivity estimates obtained from this analysis, converted to approximate fracture density and aperture, provide useful constraints on the distance to which the thermal front may migrate from the well during the cold water injection phase of the stimulation project. We estimate that the cooling front will migrate less than a tenth of a kilometer over an approximately one-year injection period. Here, the effects of that cooling, however, may be substantial, because increases in permeability have maximum effect nearest the well.

cold water injection↗

DOE OSTI2024

Long-Term Infrasound Sensor Calibration and Characterization

Previous testing has shown that infrasound sensors deployed in the field can exhibit notable deviations from their nominal, lab-based calibrations. These variations may be due to changes in environmental conditions, long-term sensor drift, or other unresolved features. In early 2018, we installed two identical infrasound elements with five infrasound sensors at each element (Chaparral M50A, Chaparral M64LN, CEA/Martec MB2005, CEA/Seismowave MB3a, and Hyperion IFS-5113A). These sensors were accepted or under consideration for use in the International Monitoring System network of the Comprehensive Nuclear-Test-Ban Treaty. Each element had all sensors connected to a single digitizer and port to the atmosphere. We also recorded instrument enclosure air temperature and humidity and external air temperature. Using the MB2005 as the reference, we examine the relative sensor response (both magnitude and phase) as a function of time and frequency and compare it with quarterly laboratory calibrations and environmental conditions. Here, we find that the magnitude response for all sensors exhibits some variability in both the lab and field, with the amplitude variations often >5%. The field-based variations are more severe and occur on both long-term (months) and short-term (hours) timescales. Short-term variability correlates with changes in environmental conditions and is considerable (up to 25%) for the Chaparral M50A and noticeable (∼5%) for the French Alternative Energies and Atomic Energy Commission (CEA) MB3a. Long-term magnitude variability for the Chaparral M50A was up to 50% and does not clearly correlate with environmental conditions. The other sensors show some long-term magnitude offsets, but they have relatively stable responses in the conditions we examined. The MB3a also displays some frequency-dependent magnitude variability and shows a minor dependence on temperature. Phase estimates are stable and near zero for all sensors tested. These results strongly suggest sensor response and variability due to environmental conditions should be considered in future infrasound data interpretation and sensor selection and development.

Fee, David↗

NASA NTRS1987

Soft x ray window encapsulant for HgI2 detectors

HgI2 is an excellent semiconductor material for a low energy, room temperature x-ray spectrometer. The high values of the atomic numbers for its constituent elements gives high x-ray and gamma ray stopping power. The band gap of HgI2 is significantly higher than other commonly used semiconductors. Owing to the large value band gap, the leakage current for HgI2 devices is smaller, thus allowing low noise performance. Devices fabricated from HgI2 crystals have demonstrated energy resolution sufficient to distinguish the x-ray emission from the neighboring elements on the periodic table. Also the power requirements of HgI2 are very low. These characteristics make a HgI2 spectrometer an ideal component in a satellite based detection system. Unfortunately, HgI2 crystals tend to deteriorate with time, even if protected by standard semiconductor encapsulants. This degradation ruins the performance of the device in terms of its energy resolution and pulse amplitude. The degrading mechanism is believed to be material loss occurring from below the electrodes, due to high vapor pressure of HgI2 at room temperature. To address this major obstacle to rapid expansion of HgI2 technology, a research program aimed at improving device stability by encapsulation with inert polymeric materials was carried out. The program focused specifically on optimizing the encapsulant materials and their deposition techniques. The principal objectives for this program were device encapsulation, device testing, and accelerated testing to ensure very long term stability of these high resolution sensors. A variety of encapsulants were investigated with the selection criteria based on their chemical diffusion barrier properties, mechanical stability, reactivity, and morphology of encapsulant films. The investigation covered different classes of encapsulants including solvent based encapsulants, vapor deposited encapsulants, and plasma polymerized encapsulants. A variety of characterization techniques were employed to examine their effectiveness in stabilizing HgI2 devices; these included permeability evaluation, vacuum and heat testing, scanning electron microscopy (SEM) as well as studying the detector performance of coated detectors. The plasma polymerized films appear to have entirely solved the HgI2 degradation problem. Another achievement of this program was the development of an accelerated testing technique which correlates extremely well with long term tesing.

Entine, G.↗

DOE OSTI2021

Thermorheological approach to predict long-term creep of cement mortar from short-term tests

Not provided.

Materials Science↗

NASA NTRS2003

Erosion Resistant Coatings for Polymer Matrix Composites in Propulsion Applications

Polymer Matrix Composites (PMCs) offer lightweight and frequently low cost alternatives to other materials in many applications. High temperature PMCs are currently used in limited propulsion applications replacing metals. Yet in most cases, PMC propulsion applications are not in the direct engine flow path since particulate erosion degrades PMC component performance and therefore restricts their use in gas turbine engines. This paper compares two erosion resistant coatings (SANRES and SANPRES) on PMCs that are useful for both low and high temperature propulsion applications. Collaborating over a multi-year period, researchers at NASA Glenn Research Center, Allison Advanced Developed Company, and Rolls-Royce Corporation have optimized these coatings in terms of adhesion, surface roughness, and erosion resistance. Results are described for vigorous hot gas/particulate erosion rig and engine testing of uncoated and coated PMC fan bypass vanes from the AE 3007 regional jet gas turbine engine. Moreover, the structural durability of these coatings is described in long-term high cycle fatigue tests. Overall, both coatings performed well in all tests and will be considered for applications in both commercial and defense propulsion applications.

Sutter, James K.↗

NASA NTRS1989

Corrosion testing of candidates for the alkaline fuel cell cathode

Current/voltage data was obtained for specially made corrosion electrodes of some oxides and of gold materials for the purpose of developing a screening test of catalysts and supports for use at the cathode of the alkaline fuel cell. The data consists of measurements of current at fixed potentials and cyclic voltammograms. These data will have to be correlated with longtime performance data in order to fully evaluate this approach to corrosion screening. Corrosion test screening of candidates for the oxygen reduction electrode of the alkaline fuel cell was applied to two substances, the pyrochlore Pb2Ru2O6.5 and the spinel NiCo2O4. The substrate gold screen and a sample of the IFC Orbiter Pt-Au performance electrode were included as blanks. The pyrochlore data indicate relative stability, although nothing yet can be said about long term stability. The spinel was plainly unstable. For this type of testing to be validated, comparisons will have to be made with long term performance tests.

Singer, Joseph↗

NASA NTRS2024

Hybrid Thermally Efficient Core (HyTEC) HyTEC Phase 1 – Combustor Final Report

The objective of the HyTEC – Combustor Technology project is to develop technology for a compact, low emissions, rich-burn combustor that maintains a high-level of durability. To accomplish this, the combustor will incorporate CMC liners and a CMC Dome to enable improved air utilization for mixing and NOx reduction. In particular, three technology areas were matured: metallic swirler attachment to the CMC dome, Nickel diffusion in CMC, and EBC advancements with improved durability. The maturation of these technology areas is critical to successfully designing a combustor for an engine intended to demonstrate increased thermal efficiency with integrated high-power density-core engine technologies. As part of the project, multiple swirler attachment architectures were matured through the design process, manufactured, and tested in simulated engine conditions. These architectures utilized two different approaches to attachment: a pressure loaded approach and a clamped approach. Each approach required testing at simulated engine conditions to mature the technology. These tests were developed to ensure that the probable failure mechanisms for each architecture were assessed relative to its long-term durability. After successfully testing both approaches, the pressure loaded approach was chosen based on its simplicity and its similarity to the attachment approach used on lean burn combustors. Finally, this successful testing resulted in the swirler attachment technology achieving TRL 4 status. Another aspect of concern with the metallic swirler attachment is the potential for nickel diffusion into the CMC to cause durability shortfalls. A series of tests were completed to understand both the amount of nickel that is expected to diffuse into the CMC and the effect this diffusion will have on mechanical properties of the CMC. After successfully completing this testing, the reduction in local mechanical properties was found to not have an impact on the overall durability of the CMC Dome. To further improve the overall durability, three different EBC coating architectures were also studied. One of these coatings being the current state of the art for CMC liners with the other two being proposed improvements. Coupons were produced using each coating and subjected to a series of laboratory testing. One coating was found to have an overall superior durability in laboratory testing and survived rig testing without indication of degradation. This successful testing resulted in the EBC technology achieving TRL 5 status. Overall, a design approach was successfully down-selected that achieves both the TPM requirements and the need for TRL 4+ status. This design incorporates a pressure loaded swirler attachment with an improved EBC coating (Architecture 1). This combination allows the continued use of a CMC dome and results in an improved durability for the proposed compact core combustor.

CMC↗

DOE OSTI2021

Accelerated Creep Test Qualification of Creep-Resistance Using the Wilshire–Cano–Stewart Constitutive Model and Stepped Isostress Method

In this paper, a qualification of accelerated creep-resistance of Inconel 718 is assessed using the novel Wilshire–Cano–Stewart (WCS) model and the stepped isostress method (SSM) and predictions are made to conventional creep data. Conventional creep testing is a long-term continuous process; in fact, the ASME B&PV III requires that 10,000+ h of experiments must be conducted to each heat for materials employed in boilers and/or pressure vessel components. This process is costly and not feasible for rapid development of new materials. As an alternative, accelerated creep testing techniques have been developed to reduce the time needed to characterize the creep resistance of materials. Most techniques are based upon the time-temperature-stress superposition principle that predicts minimum-creep-strain-rate (MCSR) and stress-rupture behaviors but lack the ability to predict creep deformation and consider deformation mechanisms that occur for experiments of longer duration. The SSM has been developed, which enables the prediction of creep deformation response as well as reduce the time needed for qualification of materials. The SSM approach has been successful for polymer, polymeric composites, and recently has been introduced for metals. In this study, the WCS constitutive model, calibrated to SSM test data, qualifies the creep resistance of Inconel 718 at 750 °C and predictions are compared to conventional creep testing data. The WCS model has proven to make long-term predictions for stress-rupture, MCSR, creep deformation, and damage in metallic materials. The SSM varies stress levels after time interval adding damage to the material, which can be tracked by the WCS model. The SSM data is calibrated into the model and the WCS model generates realistic predictions of stress-rupture, MSCR, damage, and creep deformation. The calibrated material constants are used to generate predictions of stress-rupture and are postaudit validated using the National Institute of Material Science database. Similarly, the MCSR predictions are compared from previous studies. Finally, the creep deformation predictions are compared with real data and is determined that the results are well in between the expected boundaries. Material characterization and mechanical properties can be determined at a faster rate and with a more cost-effective method. This is beneficial for multiple applications such as in additive manufacturing, composites, spacecraft, and industrial gas turbines.

42 ENGINEERING↗

DOE OSTI2023

Prediction of Long-Term Geochemical Change in Bentonite Based on the Interpretative THMC Model of the FEBEX In Situ Test

Since nuclear energy is crucial in the decarbonization of the energy supply, one hurdle to remove is the handling of high-level radioactive waste (HLW). Disposal of HLW in a deep geological repository has long been deemed a viable permanent option. In the design of a deep geological repository, compacted bentonite is the most commonly proposed buffer material. Predicting the long-term chemical evolution in bentonite, which is important for the safety assessment of a repository, has been challenging because of the complex coupled processes. Models for large-scale tests and predictions based on such models have been some of the best practices for such purposes. An 18-year-long in situ test with two dismantling events provided a unique set of chemical data that allowed for studying chemical changes in bentonite. In this paper, we first developed coupled thermal, hydrological, mechanical, and chemical (THMC) models to interpret the geochemical data collected in the in situ test and then extended the THMC model to 200 years to make long-term prediction of the geochemical evolution of bentonite. The interpretive coupled THMC model shows that the geochemical profiles were strongly affected by THM processes such as evaporation/condensation, porosity change caused by swelling, permeability change, and the shape of concentration profiles for major cations were largely controlled by transport processes, but concentration levels were regulated by chemical reactions, and the profiles of some species such as pH, bicarbonate, and sulfate were dominated by these reactions. The long-term THMC model showed that heating prolongs the time that bentonite becomes fully saturated in the area close to the heater/canister; however, once the bentonite becomes fully saturated, high concentrations of ions in bentonite near the heater, which was observed in the field test, will disappear; illitization continues for 50 years but will not proceed further.

Zheng, Liange↗

DOE OSTI2023

Time-temperature-stress superposition of PBX 9502 compressive creep data for lifetime predictions

The plastic-bonded explosive (PBX) 9502 is a viscoelastic, high-solids loaded polymer bound composite comprised of 95 weight% (wt%) TATB explosive crystals and 5 wt% FK-800 polymer binder. The uniaxial quasi-static mechanical properties have been studied and characterized extensively over 25+ years, including creep. Creep is the strain evolution over time as a result of an asymmetric load typically at temperatures above ambient. Creep measurements to failure can take excessively long periods of time depending on various factors including applied stress, temperature, and loading rate that render a single test to failure impossible. Using the principles of time-temperature-stress superposition (TTSSP), short-term creep tests at various applied stresses and temperatures can be used for long-term creep predictions. The TTSSP model shifts short-term test data using two factors, one for temperature and stress, creating a master curve at a reference test condition. The master curve can be shifted to predict the creep response at any desired test condition. PBX 9502 compression specimens were tested at three temperatures and various applied stresses. This work discusses the TTSSP analysis of PBX 9502 compressive creep data to create a single comprehensive master curve.

36 MATERIALS SCIENCE↗

DOE OSTI2023

Time-Temperature-Stress Superposition of PBX 9502 Compressive Creep Data for Lifetime Predictions

36 MATERIALS SCIENCE↗

DOE OSTI2024

Reverse-Bias Resilience of Monolithic Perovskite/Silicon Tandem Solar Cells

Metal halide perovskites have rapidly enabled a range of high-performance photovoltaic technologies. However, catastrophic failure under reverse voltage bias hinders their commercialization. In this work, we demonstrate that by employing a monolithic perovskite/silicon tandem structure, the perovskite subcell can be effectively protected by the silicon subcell under reverse bias, owing to the low reverse-bias diode current of the silicon subcell. As a result, the tested perovskite/silicon tandem devices show superior reverse-bias resilience compared to perovskite single-junction devices in both long-term reverse voltage biasing tests at the single-cell level and partial shading tests at the module level. These results highlight that, compared to other perovskite technologies, monolithic perovskite/silicon tandems are at a higher technology readiness level in terms of tackling the reverse-bias and partial shading challenge, which is a considerable advantage towards commercialization.

commercialization↗