Two types of long microextensions from cultivated liver cells.
Long microextensions on cultivated human liver cells, using scanning electron microscope
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Long microextensions on cultivated human liver cells, using scanning electron microscope
Burning solid ammonium perchlorate composite propellants surface structure observation to assess heterogeneous or subsurface reactions, using scanning electron microscope
Al and Be single particles combustion in various oxidizers, using pulsed Nd-glass laser and Xe flash heating device and scanning electron microscope
Electron optical metallographic instruments including electron microprobe X ray analyzer, scanning electron microscope, and transmission electron microscope
Auger electron velocity analyzer for use with scanning electron microscope to identify low concentrations of elements on surfaces of semiconductor devices
Scanning electron microscope and petrographic observations of glass particles from Apollo 12 lunar soil sample, revealing surface features and origin
Scanning electron microscope for poor metallization detection in manufacturing cycle of semiconductor devices
Particle size and shape distributions of Apollo 12 lunar fines by computer evaluation of scanning electron microscope images
Tin was melted in a heating assembly secured to the arm of a centrifuge. The furnace was allowed to pivot and reach its equilibrium angle of swing for the gravity force being experienced. The crucible was cooled during rotation to allow the growth of single crystals. The crystals were etched for the purpose of observing the growth striations. Slices were removed from some of the crystals to permit observation of the striations in the interior. Visual analyses were made with a scanning electron microscope. Preliminary conclusions relating the appearance of the striations to gravity forces and the affected growth mechanisms are presented. Further experiments that will verify these conclusions and determine other gravity effects are proposed.
Determination of the number of micrometeoroid impact craters on the camera provided an opportunity to make a sensitive direct measurement of the flux of interplanetary dust particles impacting the lunar surface. Optical and scanning electron microscope studies were performed. Low velocity impact and flux analyses are presented.
Screws 9 and 23 from Surveyor 3 were examined with a scanning electron microscope for micrometeorite impact features. Six craters on one of the screws appear to be low velocity impact craters, and a flux for about 0.12 sq cm was calculated to be 0.005/sq m/sec for particle diameter or = 1 micron. Two interpretations are considered: (1) The impacts were produced by interplanetary particles and the flux indicates that deviation from the normal distribution exists only for particles below 1 micron in diameter. (2) Most of the craters were produced by secondary lunar debris, and the flux represents the upper limit for interplanetary particles.
Discussion of two new techniques used to measure the lattice damage produced in GaAs by the implantation of 60 keV cadmium ions. In the first method, optical reflection spectra of the ion-implanted samples were measured in the wavelength range from 2000 to 4600 A. The decrease in reflectivity resulting from ion-implantation was used to determine the relative amount of lattice damage as a function of ion dose. The second technique employed the scanning electron microscope. Patterns very similar in appearance to Kikuchi electron diffraction patterns are obtained when the secondary and/or backscattered electron intensity is displayed as a function of the angle of incidence of the electron beam on a single crystal surface. The results of measurements made by both methods are compared with each other and with data obtained by the method of measuring lattice damage by Rutherford scattering of 1 MeV helium ions.
Four classified types of particles in stratospheric balloon collections include chains, aggregates, crystals, and irregular solids which are often liquid coated. An analysis has been made of many individual particles using an X-ray detector on a scanning electron microscope. Chain type particles are composed entirely of elements lighter than sodium. All other particle types are composed mostly of various combinations of the elements Al, Si, Na, K, Ca, Fe, Mg, Ti, and S. The most common element group is Al, Si, Ca or K, and Fe, followed by sulfur or calcium alone. At lower altitudes (12-15 km), liquid is usually associated with the particles and sulfur is prominent. At higher altitudes (23-36 km), liquids and sulfur are usually absent. However, when liquids are occasionally found, so is sulfur. Particles collected with NASA aircraft at 12 km also contain mostly the Al, Si, Ca, Fe element group with associated sulfur, or sulfur alone.
Data accumulated during 4 years of research and evaluation of ceramic chip capacitors, ceramic carrier mounted active devices, beam-lead transistors, and chip resistors are presented. Life and temperature coefficient test data, and optical and scanning electron microscope photographs of device failures are presented and the failure modes are described. Particular interest is given to discrete component qualification, power burn-in, and procedures for testing and screening discrete components. Burn-in requirements and test data will be given in support of 100 percent burn-in policy on all NASA flight programs.
Three types of CVD tungsten (fluoride-produced, chloride-produced and the combination of the two which is termed duplex) were evaluated to determine their weldability, high temperature strength and structural stability during 5000 hour exposure to temperatures of 1540 C and 1700 C. Each type of CVD tungsten could be successfully electron beam welded but the results for the chloride product were not as satisfactory as those of the other two materials. The high temperature strength behavior of the three materials did not differ greatly. However a large difference was noted for the grain growth behavior of the two basic CVD tungsten materials. Fluoride tungsten was found to be relatively stable while for the most part the grain size of chloride tungsten increased appreciably. The examination of freshly fractured surfaces with a scanning electron microscope revealed numerous bubbles in the fluoride material following its exposure to 1700 C for 5000 hours. Less severe thermal treatments produced relatively few bubbles in this material. Only at certain locations within the chloride material associated with the interruption of tungsten were bubbles noted.
The NASA nickel-base alloy WAZ-20 was analyzed by advanced metallographic techniques to qualitatively and quantitatively characterize its phases and stability. The as-cast alloy contained primary gamma-prime, a coarse gamma-gamma prime eutectic, a gamma-fine gamma prime matrix, and MC carbides. A specimen aged at 870 C for 1000 hours contained these same constituents and a few widely scattered high W particles. No detrimental phases (such as sigma or mu) were observed. Scanning electron microscope, light metallography, and replica electron microscope methods are compared. The value of quantitative electron microprobe techniques such as spot and area analysis is demonstrated.
This investigation deals in detail with the three recognized stages of plastic fracture in high strength steels, namely, void initiation, void growth, and void coalescence. The particular steels under investigation include plates from both commercial purity and high purity heats of AISI 4340 and 18 Ni, 200 grade maraging steels. A scanning electron microscope equipped with an X-ray energy dispersive analyzer, together with observations made using light microscopy, revealed methods of improving the resistance of high strength steels to plastic fracture.
Quantitative size and shape analyses have been carried out on six lunar fines from Apollo 14 and 15 by computer evaluation of scanning electron microscope images (CESEMI). For the size range of 0.50 to 30 microns diameter, the distributions are log-normal on a number count basis. This finding is in contrast with results for coarser materials in the fines reported by King et al. suggesting the operation of a different process. Aspect ratios range from 0.1 to 1.0 with an average value of about 0.6. Only slight differences are observed among samples. A shape complexity factor (ratio of particle perimeter to ellipse perimeter) also varies only slightly among the six samples.