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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 379 records · Page 21

High-resolution imaging with a tip-tilt Cassegrain secondary

A prototype adaptive secondary mirror has been developed on a 2.3-m telescope to stabilize rapid motion caused by atmospheric turbulence. The instantaneous position of an image's centroid, or brightest speckle, is measured by a near-infrared camera system which enables the tip-tilt mirror to recenter the image. Correction is accomplished at closed-loop frequencies of less than or = 100 Hz on guide stars with K (2.2 micrometers) magnitudes less than or = 8. Image motion is reduced to less than 0.1 sec rms, removing over 90% of low-frequency (f less than or = 5 Hz) tilt power, leaving less than or = 1 rad exp 2 mean square wave front tilt phase error. In seeing conditions where D/r sub o approximately = 4, long exposures in the H band (1.6 micrometers) exhibit a nearly diffraction-limited resolution of 0.19 sec full width at half maximum (FWHM) (Strehl ratio aprroximately = 0.14)-a factor of 4 improvement over uncorrected images. Reduction of the present static optical errors will improve the Strehl ratio another factor of 2, leading to approximately 70% of the maximum possible Strehl ratio.

Close, L. M.↗

The Next Generation of NASA Rapid Response: Worldview Snapshots

The NASA Rapid Response system started in 2001 by serving static subsets of Near Real Time MODIS (Moderate Resolution Imaging Spectroradiometer) imagery acquired from the Terra satellite. Over this time, Rapid Response has been used to support near real time applications such as wildfire and sea ice mapping for hundreds of thousands of users. In 2011, the toolset expanded to include GIBS, the Global Imagery Browse Services, which provides a web map tiling service of over 700 imagery products, and Worldview (https://worldview.earthdata.nasa.gov/), an interactive web application that showcases the products available in GIBS. This year a new application, Worldview Snapshots, has been added to complete the toolset by providing a flexible, low bandwidth method to download personalized subsets for those who do not need or cannot use a fully featured web mapping application. The original Rapid Response subset tool has been retired and we thank it for its seventeen years of service. Stop by to learn more about the next generation of NASA Rapid Response.

Rapid response system↗

Combined speckle- and propagation-based single shot two-dimensional phase retrieval method

Single-shot two-dimensional (2D) phase retrieval (PR) can recover the phase shift distribution within an object from a single 2D x-ray phase contrast image (XPCI). Two competing XPCI imaging modalities often used for single-shot 2D PR to recover material properties critical for predictive performance capabilities are: speckle-based (SP-XPCI) and propagation-based (PB-XPCI) XPCI imaging. However, PR from SP-XPCI and PB-XPCI images are, respectively, limited to reconstructing accurately slowly and rapidly varying features due to noise and differences in their contrast mechanisms. Herein, we consider a combined speckle- and propagation-based XPCI (SPB-XPCI) image by introducing a mask to generate a reference pattern and imaging in the near-to-holographic regime to induce intensity modulations in the image. We develop a single-shot 2D PR method for SPB-XPCI images of pure phase objects without imposing restrictions such as object support constraints. It is compared against PR methods inspired by those developed for SP-XPCI and PB-XPCI on simulated and experimental images of a thin glass shell before and during shockwave compression. Reconstructed phase maps show improvements in quantitative scores of root-mean-square error and structural similarity index measure using our proposed method.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Crack detection in fuel cell electrodes using a spatial filtering technique for overcoming noisy backgrounds

Image processing is a powerful tool that allows for rapid and automated data parsing in settings that occupy large variable spaces and require large data sets. Feature detection on difficultly discerned backgrounds is a subset of image processing that facilitates the extraction of quantitative metrics from otherwise subjective data. Crack detection and quantification is an important capability in polymer electrolyte membrane fuel cell quality control, failure analysis, and optimization. This work presents a technique to perform crack detection and quantification which overcomes challenges faced by commonly used image segmentation techniques. We demonstrate the use of a geometrically filtered noise‐level detection technique to select a binary threshold value from which we then quantify how cracked a sample is. Furthermore, we demonstrate the accuracy of our technique using programmatically generated test images of known crack amounts and their performance on real‐world fuel cell catalyst layer samples.

30 DIRECT ENERGY CONVERSION↗

Neural Learning Based Blind Source Separation for Detection of Material Defects in Pulsed Thermography Images

In this paper, we introduce a neural learning-based approach to blind source separation for detection of material flaws in pulsed thermography (PT) images. This approach can be used to detect internal defects (pores) in metallic Additively Manufactured (AM) materials. Such defects occur in high-strength alloys produced with direct laser sintering AM method for nuclear energy applications. Pulsed thermal imaging system utilizes a high intensity flash lamp to rapidly heat surface of sample, a high sensitivity infrared camera to capture data of surface temperature variations. The data cube obtained with PT (stack of surface temperature images at different times) can be analyzed with image processing algorithms to detect material defects. Compared with conventional nondestructive evaluation (NDE) methods, such as digital radiography and ultrasonic testing, the PT pulsed infrared thermal detection technique has advantages of one-sided non-contact measurements, fast processing of large sample areas captured in one image. Detection of small material defects requires finding features in thermal images, which have signal contrast levels approaching sensitivity limit of IR camera. In this study, an optimized Neural Learning based Blind Source Separation (NLBSS) algorithm, including Principal Component Analysis (PCA), and Independent Component Analysis (ICA) is demonstrated to automatically extract principal temporal and spatial features of thermography frames to enhance flaw detection. By using the NLBSS algorithm, material internal defects can be automatically detected. Furthermore, this processing approach compensates for experimental thermal imaging artifacts, such as noise and uneven heating. By merging artificial intelligence with the photothermic, the NDE system detects internal calibrated defects of various sizes and depths in AM nuclear-grade metallic alloys.

Zhang, Xin↗

Non-contact rapid reader system for reflective particle tags

A reflective particle tag reader system includes a read head assembly having a camera, illuminators, and a rigid frame portion for supporting the camera and the illuminators. The illuminators illuminate a focal point located opposite the camera where a reflective particle tag is placed. A computer in data communication with the camera receives and store images of the reflective particle tag that are acquired by the camera. The computer is programmed to process video images and to quantify a positional alignment parameter and an angular alignment parameter of the reader with respect to the reflective particle tag. A rapid burst of image frames is obtained in response to the positional alignment and the angular alignment parameters being within a predetermined tolerance and identity of the reflective tag is established between a first image set and a second image set.

42 ENGINEERING↗

Automated thematic mapping and change detection of ERTS-1 images

A system that inventories and updates resources must be capable of recognizing resources and their changes rapidly, using imagery acquired by a resources satellite such as ERTS-1. The conversion of ERTS images to thematic maps showing the distribution of resources is the first step in the data reduction process. To accomplish this task, the resources must be recognized from spatial and multispectral signatures. In addition, resource boundaries must be accurately established, and the data from different acquisition dates must be registered. This paper describes a system that combines multispectral and spatial pattern recognition techniques to produce thematic maps. This system has been applied to ERTS-1 MSS images, and the results obtained are discussed.

Gramenopoulos, N.↗

High-Resolution Three-Dimensional Sculpting of Two-Dimensional Graphene Oxide by E-Beam Direct Write

On demand switchable additive/subtractive patterning of 2D nanomaterials is an essential capability for developing new concepts of functional nanomaterials and their device realizations. Traditionally, this is performed via a multi-step process using photoresist coating and patterning by conventional photo or electron beam lithography, which is followed by bulk dry/wet etch or deposition. This limits the range of functionalities and structural topologies that can be achieved, as well as increases the complexity, cost, and possibility of contamination which are significant barriers to device fabrication from highly sensitive 2D materials. Focused electron beam induced processing (FEBIP) enables a material chemistry/site-specific, high-resolution multi-mode atomic scale processing and provides unprecedented opportunities for direct-write, single-step surface patterning of 2D nanomaterials with an in-situ imaging capability. It allows for realizing a rapid multi-scale/multi-mode approach, ranging from an atomic scale manipulation (e.g., via targeted defect introduction as an active site) to a large-area surface modification on nano and micro scales, including patterned doping and material removal/deposition with 2D (in-plane)/3D (out-of-plane) control. In this work, we report on a new capability of FEBIP for nanoscale patterning of graphene oxide via removal of oxygenated carbon moieties with no use of reactive gas required for etching complemented by carbon atom deposition using focused electron beam. The mechanism of experimentally observed phenomena is explored using the density functional theory (DFT) calculations, revealing that interactions of e-beam liberated reactive oxygen radicals with carbon atoms on graphene basal plane lead to creation of atomic vacancies in the material. The reaction by-products are volatile carbon di-oxides, which are dissociated and volatilized from the graphene oxide surface functional groups by interactions with an energetic focused electron beam. Along with selective “subtractive” patterning of graphene oxide, the same electron beam with increased irradiation doses can deposit out-of-plane 3D carbon nanostructures on top of or around the 2D etched pattern, thus forming a hybrid 2D/3D nanocomposite with feature control down to a few nanometers. Furthermore, this in-operando dual nanofabrication capability of FEBIP is unmatched by any other nanopatterning techniques and opens a new design window for forming 2D/3D complex nanostructures and functional nanodevices.

36 MATERIALS SCIENCE↗

Cryo-FIB for TEM Investigation of Soft Matter and Beam Sensitive Energy Materials

Primarily driven by structural biology, the rapid advances in cryogenic electron microscopy techniques are now being adopted and applied by materials scientists. Samples that inherently have electron transparency can be rapidly frozen (vitrified) in amorphous ice and imaged directly on a cryogenic transmission electron microscopy (cryo-TEM), however this is not the case for many important materials systems, which can consist of layered structures, embedded architectures, or be contained within a device. Cryogenic focused ion beam (cryo-FIB) lift-out procedures have recently been developed to extract intact regions and interfaces of interest, that can then be thinned to electron transparency and transferred to the cryo-TEM for characterization. Several detailed studies have been reported demonstrating the cryo-FIB lift-out procedure, however due to its relative infancy in materials science improvements are still required to ensure the technique becomes more accessible and routinely successful. Here, we review recent results on the preparation of cryo-TEM lamellae using cryo-FIB and show that the technique is broadly applicable to a range of soft matter and beam sensitive energy materials. We then present a tutorial that can guide the materials scientist through the cryo-FIB lift-out process, highlighting recent methodological advances that address the most common failure points of the technique, such as needle attachment, lift-out and transfer, and final thinning.

36 MATERIALS SCIENCE↗

Remote operation of the DIII-D National Fusion Facility

Abstract Full remote scientific operation of the DIII-D National Fusion Facility is now possible through significant advances in the computer science hardware and software infrastructure made over the last decade. Capabilities around information visualization, data movement, and communication have all been enhanced. The level of capability deployed to remotely operate DIII-D required an infrastructure advancement over what had previously been achieved in the fusion community. The large quantity of real-time data that is automatically displayed on DIII-D’s control room screens can now be visualized by remote participants via web-based applications. New audio/video solutions using the VoIP and instant messaging application Discord have been implemented to mimic the dynamic and ad-hoc scientific conversations that are critical in successfully operating an experimental campaign. Discord’s ability for a user to rapidly move between audio channels, text with images, and share screens is a significant enhancement over traditional videoconferencing tools. In addition, multiple combinations of broadcast audio are made available via a web-based application to allow remote participants to simultaneously listen to general announcements/sounds while conducting their own specific conversations. Secure methodologies have been put into place to allow remote control of hardware including DIII-D’s plasma control system application. Secure methods also included the ability of the on-site team to closely coordinate their work with remote team members which has been enhanced through extensions to the wireless network and the use of tablet computers for audio/video/screen sharing. However, no amount of software can fully replace the need for ‘hands on hardware.’ This infrastructure was severely stress tested during the COVID-19 pandemic where occupancy of the DIII-D control room was restricted. Operational efficiency during the pandemic, measured in discharges per hour, remained high (3.8 ± 0.8) compared to values obtained pre-pandemic (3.7 ± 0.8).

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Total internal reflection enabled wide-field coherent anti-Stokes Raman scattering microscopy

Wide-field coherent anti-Stokes Raman scattering (CARS) microscopy offers an attractive means for the rapid and simultaneous acquisition of vibrationally resolved images across a large field of view. A major challenge in the implementation lies in how to achieve sufficiently strong excitation fields necessary to drive the third-order optical responses over the large focal region. Here, we report a new wide-field CARS microscope enabled by a total internal reflection excitation scheme using a femtosecond Ti:Sapphire oscillator to generate pump and broadband near-infrared Stokes pulses. The spectrally broad Stokes pulse, in combination with its inherent chirp, offers not only access to a wide range of Raman modes spanning ∼ <#comment/> 1000 to ∼ <#comment/> 3500 c m − <#comment/> 1 but also a straightforward means to select vibrational transitions within this range by simply varying the time delay between the pulses. The unique capabilities of this wide-field CARS microscope were validated by acquiring high-quality CARS images from the model and complex biological samples on conventional microscope coverslips.

Doughty, Benjamin (ORCID:0000000164299329)↗

Total internal reflection enabled wide-field coherent anti-Stokes Raman scattering microscopy

Wide-field coherent anti-Stokes Raman scattering (CARS) microscopy offers an attractive means for the rapid and simultaneous acquisition of vibrationally resolved images across a large field of view. A major challenge in the implementation lies in how to achieve sufficiently strong excitation fields necessary to drive the third-order optical responses over the large focal region. Here, we report a new wide-field CARS microscope enabled by a total internal reflection excitation scheme using a femtosecond Ti:Sapphire oscillator to generate pump and broadband near-infrared Stokes pulses. The spectrally broad Stokes pulse, in combination with its inherent chirp, offers not only access to a wide range of Raman modes spanning ${\sim}{1000}$ to ${\sim}{3500}\;{{\rm cm}^{- 1}}$ but also a straightforward means to select vibrational transitions within this range by simply varying the time delay between the pulses. The unique capabilities of this wide-field CARS microscope were validated by acquiring high-quality CARS images from the model and complex biological samples on conventional microscope coverslips.

36 MATERIALS SCIENCE↗

Cryo-FIB for TEM Investigation of Soft Matter and Beam Sensitive Energy Materials

Primarily driven by structural biology, the rapid advances in cryogenic electron microscopy techniques are now being adopted and applied by materials scientists. Samples that inherently have electron transparency can be rapidly frozen (vitrified) in amorphous ice and imaged directly on a cryogenic transmission electron microscopy (cryo-TEM), however this is not the case for many important materials systems, which can consist of layered structures, embedded architectures, or be contained within a device. Cryogenic focused ion beam (cryo-FIB) lift-out procedures have recently been developed to extract intact regions and interfaces of interest, that can then be thinned to electron transparency and transferred to the cryo-TEM for characterization. Several detailed studies have been reported demonstrating the cryo-FIB lift-out procedure, however due to its relative infancy in materials science improvements are still required to ensure the technique becomes more accessible and routinely successful. Here, we review recent results on the preparation of cryo-TEM lamellae using cryo-FIB and show that the technique is broadly applicable to a range of soft matter and beam sensitive energy materials. We then present a tutorial that can guide the materials scientist through the cryo-FIB lift-out process, highlighting recent methodological advances that address the most common failure points of the technique, such as needle attachment, lift-out and transfer, and final thinning.

36 MATERIALS SCIENCE↗

The sources of material comprising a mass ejection coronal transient

The origin of the material ejected during a white-light coronal transient on August 26 and 27, 1973, is investigated using simultaneous observations of a slowly ascending prominence and the more rapid accompanying coronal transient. Nearly identical simultaneous images of the prominence were obtained over a six-hour period in the H-alpha and He II (304 A) emission lines; contemporaneous Skylab coronograph observations over approximately 1.5 hours showed that the mass-ejection coronal transient rose above the ascending prominence. Based on analysis of these observations, it is concluded that: (1) the bulk of the ejected material originated in the lower corona, despite the lack of an observed depletion there; (2) the material in the transient was at coronal temperature and was visible in polarized radiation due to Thomson scattering of photospheric light by free electrons; and (3) the total event was far larger, more energetic, and longer lasting than would have been inferred from the prominence observations alone.

Hildner, E.↗

Near-infrared spectral imaging Michelson interferometer for astronomical applications

The design and operation of an imaging Michelson interferometer-spectrometer used for near-infrared (0.8 micron to 2.5 microns) spectral imaging are reported. The system employs a rapid scan interferometer modified for stable low resolution (250/cm) performance and a 42 element PbS linear detector array. A microcomputer system is described which provides data acquisition, coadding, and Fourier transformation for near real-time presentation of the spectra of all 42 scene elements. The electronic and mechanical designs are discussed and telescope performance data presented.

Wells, C. W.↗

Satellite-derived reflectance of snow-covered surfaces in northern Minnesota

The reflectance of snow-covered surfaces in Minnesota is analyzed using Landsat-5 Thematic Mapper satellite data. Calculations are performed for satellite-derived reflectances integrated over the spectral region (0.45-0.9 micron). Corrections are applied for atmospheric effects and integrated reflectances (R1) are compared over agricultural and forested areas and over a lake using TM scenes acquired in November 1984 and January 1985. Integrated reflectances are then mapped and inter- and intra-scene comparisons of surface reflectance are compared. Temporal analysis of reflectance changes can then be performed rapidly and efficiently using color-coded images. It is noted that the average R1 within the November 1984 subscene was 0.429 + or - 0.176, whereas R1 within the January 1985 subscene was 0.669 + or - 0.236.

Hall, D. K.↗

Algorithms For Detection Of Correlation Spots

Three algorithms provide for improved postprocessing of outputs of optical correlators based on binary phase-only filters. Detect correlation spots. Function in presence of noise and executed rapidly. First algorithm starts processing correlation-image data while data fed out of video camera and digitized for subsequent analysis. Second involves convolution of correlation image with small-window two-dimensional impulse-response function followed by threshold operation in which negative values of convolution integral set to zero. Third affects generation as well as postprocessing of correlation image.

Scholl, Marija S.↗

Exploratory geological analysis of AVIRIS data

The size and complexity of AVIRIS data sets makes analysis difficult. We present a technique that allows the researcher to rapidly scan the full data set in image form in order to empirically find significant spatial patterns anywhere across the spectrum. Our approach takes advantage of the speed and power of computer graphics workstations to allow real-time, interactive data manipulation and display. Empirical data selection avoids the bias inherent in theoretical selection criteria, and allows discovery of unexpected relationships within the data set. Link Winds, a prototype data analysis system under development, provides the visualization tools used in this study. We are applying this approach to geological studies in the eastern Mojave Desert.

Beratan, K. K.↗