Some investigations of refractory metal systems of thermionic interest
Investigating interdiffusion of W-Ta, W-Mo, and W-Nb systems in refractory temperature range
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Investigating interdiffusion of W-Ta, W-Mo, and W-Nb systems in refractory temperature range
Angular distributions for /alpha,t/ reactions on Zr-90, Mo-92 and 96 at 41.5 MeV
Thermionic converter tests, discussing W emitter with Nb and Mo-on-Nb collectors, surface and electrode combinations
Maximum efficiency of cylindrical thermionic converters with Mo emitter and collector over temperature range
Polyatomic organic adsorbates effect on field emission total energy distribution from W and Mo surfaces, discussing electronic and phononic spectra
Compact fast reactor design for space power with rotating fuel drums, Mo alloy reflectors and honeycomb support structure
Stress effect on hydrogen distribution at high temperatures in titanium and Ti-Al-Mo-V alloy
Mass transport at high current densities in Al and Mo thin film conducting stripes, noting effect on IC life
A zero-power critical assembly was designed, constructed, and operated for the purpose of conducting a series of benchmark experiments dealing with the physics characteristics of a UN-fueled, Li-7 cooled, Mo-reflected, drum-controlled compact fast reactor for use with a space-power electric conversion system. The experimental program consisted basically of measuring the differential neutron spectra and the changes in critical mass that accompanied the stepwise addition of (Li-7)3N, Hf, Ta, and W to a basic core fueled with U metal in a pin-type Ta honeycomb structure. In addition, experimental results were obtained on power distributions, control characteristics, neutron lifetime, and reactivity worths of numerous absorber, structural, and scattering materials.
A simple analytical procedure is described for accurately and precisely determining the zirconium or hafnium content of molybdenum-base alloys. The procedure is based on the reaction of the reagent Arsenazo III with zirconium or hafnium in strong hydrochloric acid solution. The colored complexes of zirconium or hafnium are formed in the presence of molybdenum. Titanium or rhenium in the alloy have no adverse effect on the zirconium or hafnium complex at the following levels in the selected aliquot: Mo, 10 mg; Re, 10 mg; Ti, 1 mg. The spectrophotometric measurement of the zirconium or hafnium complex is accomplished without prior separation with a relative standard deviation of 1.3 to 2.7 percent.
Examination is made of the influence of temperature on the strainrange partitioning approach to creep-fatigue. Results for Cr-Mo steel and Type 316 stainless steel show the four partitioned strainrange-life relationships to be temperature insensitive to within a factor of two on cyclic life. Monotonic creep and tensile ductilities were also found to be temperature insensitive to within a factor of two. The approach provides bounds on cyclic life that can be readily established for any type of inelastic strain cycle. Continuous strain cycling results obtained over a broad range of high temperatures and frequencies are in excellent agreement with bounds provided by the approach. The observed transition from one bound to the other is also in good agreement with the approach.
A description is given of the design and fabrication of candidate flame-resistant woven and knitted fabrics, tapes, webbings, and cords as replacements for those items used in the Apollo spacecraft which were previously made of nylon and polyester. Structures made from Chromel R metal fibers (74% Ni, 20% Cr, 2-1/2% Fe, 2-1/2% Al, 1/2% Si, 1/2% Mo), Beta glass fibers and high-temperature organic fibers such as PBI (polybenzimidazole) were developed and evaluated. The feasibility of improving the performance of selected fabrics by using CNR (carboxy nitroso rubber) or other nonflammable coatings were also investigated.
Using NASA IIb as a base composition, the effects of five key elements (carbon, tungsten, tantalum, aluminum, and hafnium) on resultant properties were investigated in an effort to optimize the composition and derive new wrought high temperature alloys with improved strength characteristics. A total of nineteen compositions were melted, extruded, and rolled to bar stock using thermomechanical processing. Both full and partial solution heat treatments were developed for the compositions. Tensile properties from room temperature to 1800 deg F, stress and creep rupture properties to 1800 deg F, and thermal stability characteristics were evaluated. NASA IIb-7 exhibited the best response to the partial solution heat treatment for optimum properties up to 1200 deg F. The alloy contained 0.13C, 9.0 Cr, 9.0 Co, 2.0 Mo, 7.5 W, 10.0 Ta, 3.5 Al, 0.75 Ti, 0.02 B, 0.10 Zr, 0.50 V, 1.0 Hf, and balance nickel.
A zero-power critical assembly was designed, constructed, and operated for the purpose of conducting a series of benchmark experiments dealing with the physics characteristics of a UN-fueled, Li-cooled, Mo-reflected, drum-controlled compact fast reactor for use with a space-power electric conversion system. The range of the previous experimental investigations has been expanded to include the reactivity effects of:(1) surrounding the reactor with 15.24 cm (6 in.) of polyethylene, (2) reducing the heights of a portion of the upper and lower axial reflectors by factors of 2 and 4, (3) adding 45 kg of W to the core uniformly in two steps, (4) adding 9.54 kg of Ta to the core uniformly, and (5) inserting 2.3 kg of polyethylene into the core proper and determining the effect of a Ta addition on the polyethylene worth.
Silicon ribbon growth experiments were conducted using orifices (dies) fabricated from SiC-SiO2 mixtures, fused quartz, SiC, and fine-grained, high density graphite. The best results were obtained from graphite dies. A number of different approaches was tried in modifying the thermal gradient in the dies and in holding the dies. The best results here were obtained from a 0.25-in. thick Mo disc holding a graphite die directly and fitting the die quite closely. Ribbon growths as wide as 9 mm were obtained, while the longest ribbon was 450 x 3.5 x 0.5 mm. Resistivities of ribbons grown from graphite dies have been measured over the range of 0.03 to 1.6 ohm-cm. Some thoughts and literature findings are presented regarding refractory oxide materials as potential orifices.
Investigation of longitudinal sound attenuation in superconducting Mo-Re alloys as a function of temperature, magnetic field, and frequency. Evaporated thin film CdS transducers were used for the measurements at frequencies up to 3 GHz. The normal state attenuation coefficient was found to be proportional to the square of frequency over this frequency range. Measurements in zero magnetic field yielded a value of the energy gap parameter close to the threshold value of 3.56 kTc, appropriate to a weakly coupled dirty limit superconductor.
Rats were chronically centrifuged in excess of 2.0 g for 6 or 12 mo. They were given four 24-hr gravity-preference tests in a spiral centrifuge in which they could adjust the gravity level imposed by locomoting inward or outward radially along a track. Chronically centrifuged rats (Group CC) spent as much time at 2.0 g as at 1.0 g while normally raised controls (Group NC) selecdonly 1.0 g. Group CC initially selected 2.0 g and a preference for 1.0 g developed over the four test sessions. These results suggest that hypergravity is not necessarily an aversive stimulus and that gravity preference may depend initially upon the reference level involved. The ultimate selection of 1.0 g by chronically centrifuged animals suggests that a preference for a familiar gravity environment is replaced by a preference for low-gravity stimuli.
The framework of a new method is outlined for treating creep-fatigue behavior of metals. Inelastic strain-ranges are partitioned into the components of (1) completely reversed plasticity, (2) tensile plasticity reversed by compressive creep, or tensile creep reversed by compressive plasticity, and (3) completely reversed creep. Each of these components is shown to be related to cyclic life by a Manson-Coffin type power-law equation. A linear life fraction rule is used to combine the damaging effects of the individual components enabling the prediction of life. Test results are presented for a 2.25 Cr-1 Mo steel as well as limited information for a Type 316 stainless steel.