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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 379 records · Page 21
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Investigation of Lubricant Additive Interactions on Gasoline Particulate Filters

To understand how the composition of novel lubricant additives and their ash interact with gasoline particulate filters (GPFs), an accelerated aging protocol was conducted using three lubricant additive formulations and two GPF types. The additive packages (adpaks) consisted of Ca+Mg detergent in a 3:1 or 0:1 ratio and an anti-wear component—either zinc dialkyl dithiophosphate (ZDDP) or a novel phosphonium-phosphinate ionic liquid (IL) substitute. The particulate sampling captured amount/compositions of particulate matter (PM) generated, total particulate number, and size distribution. Five ash loadings were completed. GPF position and adpak composition affected the backpressure, ash composition, ash morphology, and captured mass. The particulate sampling indicated that the ash component consisted primarily of particles less than 50 nm in size and that the Mg-only adpak resulted in more particulate of 50–400 nm in size. Postmortem materials characterization indicated GPFs in the underfloor position had deeper penetration of ash into the walls compared to the close-coupled position. Additionally, the Mg-only adpak had a higher filter collection efficiency (>90%) and the ash particles consisted of a higher concentration of dense ash material. In contrast, four of the 3:1 Ca:Mg lubricant adpaks resulted in a collection efficiency of only 40–50%. Although the collection efficiency was higher with the Mg-only adpak, the ash layer in the GPF was not thicker, nor was the penetration into the wall more significant, and surprisingly the full useful life (FUL) backpressure was lower than with Ca:Mg adpaks. The higher density of the Mg-derived ash was the only detectable difference. A possible explanation of this observation is that Mg ash has a lower melting point and is more susceptible to densification during combustion or GPF regeneration. The substitution of IL in place of the ZDDP did not lead to any notable changes in collection efficiency or location of the ash.

42 ENGINEERING↗
NASA NTRS1951

Preliminary Investigation of Molybdenum Disulfide-air-mist Lubrication for Roller Bearings Operating to DN Values of 1 x 10(exp 6) and Ball Bearings Operating to Temperatures of 1000 F

The effectiveness of molybdenum disulfide MoS2 as a bearing lubricant was determined at high temperature and at high speeds. A 1-inch-bore ball bearing operated at temperatures to 1000 F, a speed of 1725 rpm, and a thrust load of 20 pounds when lubricated only with MoS2-air mist. A 75-millimeter-bore cageless roller bearing, provided with a MoS2-syrup coating before operation, operated at DN values to 1 x 10(exp 6) with a load of 368 pounds.

BEARINGS, ANTI - FRICTION↗
DOE OSTI2016

Effects of star-shape poly(alkyl methacrylate) arm uniformity on lubricant properties

Star-shaped poly(alkyl methacrylate)s (PAMAs) were prepared and blended into an additive-free engine oil to assess the structure property relationship between macromolecular structure and lubricant performance. These additives were designed with a comparable number of repeating units per arm and the number of arms was varied between 3 and 6. Well-defined star-shaped PAMAs were synthesized by atom transfer radical polymerization (ATRP) via a core-first strategy from multi-functional headgroups. Observations of the polymer-oil blends suggest that stars with less than four arms are favorable as a viscosity index improver (VII), and molecular weight dominates viscosity-related effects over other structural features. Star-shaped PAMAs, as oil additives, effectively reduce the friction coefficient in both mixed and boundary lubrication regime. Several analogs outperformed commercial VIIs in both viscosity and friction performance. Furthermore, increased wear rates were observed for these star-shaped PAMAs in the boundary lubrication regime suggesting pressure-sensitive conformations may exist.

36 MATERIALS SCIENCE↗
DOE OSTI2018

The Sliding Wear and Frictional Behavior of M50-10 wt.%(Sn-Ag-Cu) Self-Lubricating Materials at Elevated Temperatures

As the main steel used in the aero-engine main shaft bearings, the tribological properties of M50 can directly affect the performance of aero-engine. The purpose of this study is to design the reasonable composition of Sn-Ag-Cu alloy and investigate the wear mechanisms of M50-10 wt.%(Sn-Ag-Cu) composites (MSACC) prepared by SPS sliding against Si{sub 3}N{sub 4} ball from 25 to 550 °C at 12 N-0.25 m/s. XRD, EPMA, FESEM and EDS mappings are conducted to understand the major mechanisms leading to the improvement in the sliding behavior of MSACC. The results indicate that MSACC with different specifications of Sn-Ag-Cu alloy shows excellent friction and wear properties from 25 to 550 °C compared to M50. M50-10 wt.%(50Sn40Ag10Cu) (MSACC-2) shows the distinguished tribological performance for the lower friction coefficients of 0.22-0.61 and less wear rates of 1.7-4.1 × 10{sup −6} mm{sup 3} N{sup −1} m{sup −1}, which is attributed to the formed excellent lubricating structure consisting of the lubricating film with massive Sn-Ag-Cu alloy and intermetallic compounds formed during the friction process, as well as the underneath mixed layer who can well support the lubricating film due to the good intersolubility between the designed Sn-Ag-Cu alloy and M50 (Fe).

36 MATERIALS SCIENCE↗
DOE OSTI2017

Lubricated immersed boundary method in two dimensions

Many biological examples of fluid-structure interaction, including the transit of red blood cells through the narrow slits in the spleen and the intracellular trafficking of vesicles into dendritic spines, involve the near-contact of elastic structures separated by thin layers of fluid. Motivated by such problems, we introduce an immersed boundary method that uses elements of lubrication theory to resolve thin fluid layers between immersed boundaries. We demonstrate 2nd-order accurate convergence for simple two-dimensional flows with known exact solutions to showcase the increased accuracy of this method compared to the standard immersed boundary method. Motivated by the phenomenon of wall-induced migration, we apply the lubricated immersed boundary method to simulate an elastic vesicle near a wall in shear flow. We also simulate the dynamics of a vesicle traveling through a narrow channel and observe the ability of the lubricated method to capture the vesicle motion on relatively coarse fluid grids.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2020

Competitive Adsorption of Lubricant Base Oil and Ionic Liquid Additives at Air/Liquid and Solid/Liquid Interfaces

Oil-soluble ionic liquids (ILs) have been proved as effective additives in lubricant oils through tribological experiments and post-test analytical analyses. Here, surface structures of lubricant base oil, oil-soluble ILs, and their mixtures at the air/liquid and solid/liquid interfaces have been studied using sum frequency generation (SFG) vibrational spectroscopy. At the air/base oil and air/IL interfaces, the alkyl chains of the studied compounds were shown to be conformationally disordered and their terminal methyl groups point outward at the liquid surface. The base oil dominates the air/(base oil + IL) interface due to its higher surface excess propensity and larger bulk concentration. At the solid (silica) surface, ILs adopt a structure with their charged headgroups in contact with the silica surface, while their alkyl chains are more conformationally ordered or packed compared to the air/IL interface. At the interface between silica and (base oil + IL) mixtures, ILs also preferentially adsorb to the silica surface with their layer structures somewhat different from those of ILs alone. These results showed that ILs can adsorb onto the solid surface even before tribological contacts are made. The insights obtained from this SFG study provide a better understanding of the role of ionic liquids in lubrication.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2016

Production of renewable lubricants via self-condensation of methyl ketones

Self-condensation of biomass-derived methyl ketones catalyzed by solid bases or acids produces corresponding cyclic trimers exclusively in excellent yields. Condensates containing 24–45 carbon atoms are shown to be suitable lubricant base-oils after the removal of residual unsaturation and oxygen. Properties of cycloalkanes produced from biomass are very similar to those of conventional lubricant base-oils. Here, the process reported here offers an environmentally benign alternative to the current non-selective production of lubricant base-oils from α-olefins, and avoids the production of corrosive waste products.

Balakrishnan, Madhesan↗
DOE OSTI2018

Multivalent counterions diminish the lubricity of polyelectrolyte brushes

Polyelectrolyte brushes provide wear protection and lubrication in many technical, medical, physiological, and biological applications. Wear resistance and low friction are attributed to counterion osmotic pressure and the hydration layer surrounding the charged polymer segments. However, the presence of multivalent counterions in solution can strongly affect the interchain interactions and structural properties of brush layers. We evaluated the lubrication properties of polystyrene sulfonate brush layers sliding against each other in aqueous solutions containing increasing concentrations of counterions. The presence of multivalent ions (Y 3+ , Ca 2+ , Ba 2+ ), even at minute concentrations, markedly increases the friction forces between brush layers owing to electrostatic bridging and brush collapse. Furthermore, our results suggest that the lubricating properties of polyelectrolyte brushes in multivalent solution are hindered relative to those in monovalent solution.

47 OTHER INSTRUMENTATION↗
DOE OSTI2018

A Novel Lubricant Formulation Scheme for 2% Fuel Efficiency Improvement. EE0006449_Final Technical Report

Novel lubricant formulations for improving vehicle fuel efficiency by at least 2% without adversely impacting vehicle performance or durability. In particular, this objective is to be achieved through: (1) reducing friction due to asperity rubbing in start-up and low-speed operations, (2) temporarily reducing the lubricant viscosity (temporary shear-thinning) in medium- to high-speed cruise operations, and (3) suppressing oil aeration or foaming responsible for lubrication breakdown in high-speed operations.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2020

Development of Ionic Liquid-Additized, GF-5/6 Compatible Low-Viscosity Oils for Automotive Engine and Rear Axle Lubrication for 4% Improved Fuel Economy

This joint project among ORNL, GM, and DRO successfully developed ionic liquid-additized low viscosity lubricants, SAE 0W-12 and 70W-80, for both IC engine and rear axle lubrication, respectively, and demonstrated combined vehicle fuel economy improvement (FEI). Phosphonium-alkylphosphate ILs have been found to be the most effective among the candidates in protecting surface damage from both sliding wear and rolling contact fatigue, and optimal IL concentrations have been determined. The IL’s impact on three-way catalyst seems to be significantly less adverse than the conventional ZDDP. Oil formulations were optimized for both energy efficiency and wear protection. Tribological bench testing of the IL-additized low-viscosity oils showed at least 40% lower boundary friction, more than 60% lower elastohydrodynamic friction, and greater than 50% less wear compared with commercial baselines. IL-additized lubricants have demonstrated FEI by 9.9% in engine dynamometer tests under extreme conditions and 6.9% increased power output in gear rig tests. Prototype IL-additized engine oil and rear axle fluid exhibited combined FEI of 1.39% and 3.24% benchmarked against the state-of-the-art baselines in vehicle testing of fresh oils under the Federal Test Procedure (FTP) city cycle and Highway Fuel Economy Driving Schedule (HWFET), respectively. Used oil analysis suggested that the IL-additized low-viscosity oils produced less wear than the commercial baselines. The gained fundamental understanding and demonstrated FEI in this work pave the way for future development and implementation of the ionic liquid technology.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1968

Bearings use dry self-lubricating cage materials

Rolling element bearings in spacecraft mechanical systems use solid lubricant composites of polytetrafluoroethylene in the bearing cage which functions as the lubricant reservoir. The cage spaces the rolling elements equally and provides the lubricant at the bearing load-carrying surface.

Anderson, W. J.↗
NASA NTRS1970

Liquid cryogenic lubricant

Fluorinated polyethers are suitable lubricants for rolling-element bearings in cryogenic systems. Lubrication effectiveness is comparable to that of super-refined mineral oil lubricants operating at room temperature.

Dietrich, M. W.↗
NASA NTRS1971

Applications of aerospace technology in industry, a technology transfer profile: Lubrication

Technology transfer in the lubrication field is discussed in terms of the movement of NASA-generated lubrication technology into the private sector as affected by evolving industrial requirements. An overview of the field is presented, and NASA technical contributions to lubrication technology are described. Specific examples in which these technologies have been used in the private sector are summarized.

Kottenstette, J. P.↗
NASA NTRS1972

Comparative lubrication studies of OH-58A tail rotor drive shaft bearings

Comparative lubrication tests were run with OH-58A helicopter tail rotor drive shaft bearings. The tests were run in an outdoor environment with ambient temperatures ranging from 10 to 75 F. Dust was periodically applied to the bearings to simulate field conditions. The cause of bearing failure was associated with dust penetration. Rotor shaft failure was found to be caused by the shaft rotating in the standard rubber collar due to seizure of the bearings. Bearings with a positive rubbing seal having a MIL-G-81322 grease produced lives greater than with bearings having labyrinth seals and a mineral oil paste lubricant. An elongated collar prevented failure of the rotor shaft during bearing seizure. In a limited test, installation of tail boom shrouds over the bearings which excluded dust and water resulted in bearing lives in excess of 1800 hours or 1200 hours greater than the current 600 hours TBO, regardless of the lubricant-bearing combination used.

Dietrich, M. W.↗
NASA NTRS1973

Lubrication handbook

Information on lubricants from government reports, military specifications, qualified parts lists, and suppliers of commercial lubricants has been consolidated in one source. Handbook includes data on chemical and physical properties of solid, bonded solid, and liquid lubricants; dispersions and composites; and greases, oils, and hydraulic fluids.

Campbell, M. E.↗
NASA NTRS1972

Development and characterization of lubricants for use near nuclear reactors in space vehicles

The synthesis and evaluation program was conducted to develop wide-temperature range lubricants suitable for use in space vehicles particularly in the vicinity of nuclear reactors. Synthetic approaches resulted in nonpolymeric, large molecular weight materials, all based on some combination of siloxane and aromatic groups. Evaluation of these materials indicated that certain tetramethyl and hexamethyl disiloxanes containing phenyl thiophenyl substituents are extremely promising with respect to radiation stability, wide temperature range, good lubricity, oxidation resistance and additive acceptance. The synthesis of fluids is discussed, and the equipment and methods used in evaluation are described, some of which were designed to evaluate micro-quantities of the synthesized lubricants.

Robinson, G. L.↗