ToF-SIMS Imaging and Analysis of Light Isotopes in Irradiated Materials
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Yu, Xiao-Ying [ORNL] (ORCID:0000000298613109)↗
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Use of Computer Vision for Analysis of Image Data Sets from High Temperature Plasma Experiments [Slides]
Abstract not provided.
70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
Statistical Analysis of Imaging Laser Scan Data of an Exhaust Tunnel at the SRS
• The SRS H-Canyon Building is a critical facility under the responsibility of DOE-EM. • It includes an Air Exhaust Tunnel (HCAEX) that allows for ventilation of the process airflow. • Inspections are performed remotely because of hazards, e.g. radioactivity, debris, high airflow, and nitric acid vapors.
Wells, William Willie [Savannah River National Lab↗
3013 Baseline Inner Container Report: Description, Imaging, and Analysis
This report presents consolidated findings from three microscopy studies of baseline Bagless Transfer Containers (BTCs), which are the inner containers used in DOE Standard 3013-compliant plutonium storage packages. The studies were conducted by Los Alamos National Laboratory (LANL), Savannah River National Laboratory (SRNL), and DNV, a subcontractor specializing in corrosion science. The baseline BTCs examined had not been exposed to corrosive environments, serving as control samples for comparison with destructively examined (DE) containers. Additionally, the Background section provides an overview of the BTC design, including manufacturing methods, material properties, and container configurations that may influence corrosion behavior. The primary objective of the LANL and SRNL studies was to establish reference characteristics of BTCs to distinguish manufacturing artifacts from corrosion-induced features observed in DE containers. Both laboratories used advanced microscopy techniques, including Wide Area Microscopy (WAMS), Laser Confocal Microscopy (LCM), Scanning Electron Microscopy (SEM), and Focused Ion Beam (FIB), to reveal that most surface anomalies were shallow and attributable to flow-forming processes, not corrosion. Subsurface impurities, identified as non-metallic inclusions, were also observed. DNV’s investigation focused on characterizing the mechanical and chemical properties of the BTC material to support crack growth modeling. Their findings indicate higher hardness and strength but reduced ductility—consistent with flow-formed 304L stainless steel and a higher-than-expected martensite content, in contrast to manufacturer claims. Ongoing and future studies, including Electron Backscatter Diffraction (EBSD), aim to further understand the microstructural factors influencing crack initiation and propagation. The combined studies provide a crucial baseline for distinguishing corrosion effects in DE containers, contributing to the safe and reliable long-term storage of plutonium-bearing materials.
36 MATERIALS SCIENCE↗
Laboratory Hail Damage of Photovoltaic Modules: Electroluminescence and High-speed Digital Image Correlation Analysis
This work experimentally investigates hail-related failures in Glass/Backsheet and Glass/Glass PV modules with varying ice ball diameters and velocities.
DiGregorio, Steven John↗
Imaging and Analysis of Insoluble Electrorefiner Material
Throughout pyroprocessing efforts at the Hot Fuel Examination Facility (HFEF), insoluble material has accumulated in the Electrorefiner (ER) vessel. The objective of this effort was to analyze the accumulated material to determine its origin. Material was removed from the ER salt bath and distilled to remove excess salt prior to performing analysis. Three samples were sent for chemical and isotopic analysis and underwent an ethyl acetate-bromine dissolution to segregate the oxide fraction from the metal fraction. Actinide concentrations were determined using a quadrupole–inductively coupled plasma–mass spectrometer (Q-ICP-MS). Three additional samples were sent for morphologic and elemental analysis by scanning electron microscopy (SEM) with Energy Dispersive X-ray (EDX) analysis at the Irradiated Materials Characterization Laboratory (IMCL). Analyses suggest that the material is primarily composed of UO2. with a small fraction of metal. This study draws no single conclusion as to the origin of the insoluble material in the ER. The particle sizes and morphologies observed in SEM micrographs indicate that the larger particles observed may be a result of introducing material to the ER that has not been completely reduced in Oxide Reduction (OR) operations, which precede electrorefining. Smaller particles may be due to reactions with oxygen and moisture present in HFEF. This research suggests that microscopic analysis of fuel particles before and after OR operations (including after distillation) as well as the uranium product collected on the cathode in the ER would increase understanding about particle morphology within the pyrochemical process.
11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
Application of ERTS-1 data to the protection and management of New Jersey's coastal environment
The author has identified the following significant results. This catalogue was prepared as a part of the joint ERTS-1 New Jersey coastal mapping experiment. First look analysis of ERTS-1 images indicates that numerous coastal oceanographic patterns can be mapped on a sequential basis using ERTS-1 images. Analysis of imagery indicates a predominant southwesterly drift of dumped wasted in the surface waters. Initial analysis of imagery indicates that the effects of tidal flushing of New York harbor extend as far south as Long Branch, New Jersey. Analysis of imagery from 3 September, 1972, indicates a wide band of turbid water extending several miles offshore around Barnegat Inlet. First look analysis of imagery from 10 October, 1972, illustrates the increased reflectance of turbid waters within the bays, sounds, and thoroughfares behind the barrier islands in the southern New Jersey shore area. The estuarine waters emanating from both Brigantine and Absecon Inlets are very turbid relative to the waters further offshore and to the north and south. The tidal prism appears to be quite large but the movement of water once outside the inlets is not very rapid. The waters are not moving away from the coastline but rather along the coast.
Yunghans, R. S.↗
Geology of the Valles Marineris - First Analysis of Imaging from the Viking 1 Orbiter Primary Mission
The Valles Marineris on the planet Mars constitute an enormous group of steep-walled equatorial canyons extending over an area more than 4000 km long and up to 700 km wide. An overview of Valles Marineris is provided, taking into account canyon system subdivisions, imaging and topographic data, Noctis Labyrinthus, western troughs, central troughs, east central troughs, and eastern canyons. Aspects of canyon wall and canyon floor morphology are discussed, giving attention to erosional features, layered rocks in canyon walls, tectonic features, plains, landslide deposits, hilly terrain, fractured floor, and floor plateaus and ridges. Upland pits and closed depressions in the canyons are considered along with regional tectonics and regional erosional styles.
Blasius, K. R.↗
Photometry and polarimetry of Jupiter at large phase angles. I - Analysis of imaging data of a prominent belt and a zone from Pioneer 10
Photopolarimetric observations of a prominent bright zone and a dark belt of Jupiter in red and blue light are analyzed which were performed by Pioneer 10 at phase angles of 12, 23, 34, 109, 120, 127, and 150 deg. Geometric and photometric reductions of the imaging data are described, the instrument sensitivity at various times is evaluated, and the data are referred to an absolute scale. The observations are analyzed in detail by comparing the data with results of radiative-transfer calculations for specific scattering models of Jupiter's atmosphere. These models include those with a vertical structure consisting of a layer of Rayleigh-scattering gas above a semiinfinite mixture of cloud particles and gas, those having a small quantity of aerosols in the gas above either the diffuse cloud in a reflecting-scattering model or the top cloud of a two-cloud-layer model, those in which a forward-scattering haze is mixed uniformly with gas, and those containing dust layers. It is found that in both the belt and the zone in red as well as blue light, cloud phase functions are required which provide both strong forward scattering and some backscattering.
Tomasko, M. G.↗
Digital image data sets for remote sensing instruction
Several sets of LANDSAT image segments and a set of simple image processing programs operating in batch mode are being used to teach an introductory course in digital image analysis and classification. The image data sets contain only a small number of pixels and can be run quickly on most university computing systems. A number of image data sets derived from the raw spectral bands (smoothed data sets, band ratios and texture data sets) allows the student to examine and include these extracted variables in the classification process. Another data set consists of three registered LANDSAT image segments for three different dates so that the student may experiment with multitemporal data processing. The three LANDSAT scenes used in the class are described and the image data sets available for class exercises are listed.
Eyton, J. R.↗
Performance analysis of image processing algorithms for classification of natural vegetation in the mountains of southern California
The earth's forests fix carbon from the atmosphere during photosynthesis. Scientists are concerned that massive forest removals may promote an increase in atmospheric carbon dioxide, with possible global warming and related environmental effects. Space-based remote sensing may enable the production of accurate world forest maps needed to examine this concern objectively. To test the limits of remote sensing for large-area forest mapping, we use Landsat data acquired over a site in the forested mountains of southern California to examine the relative capacities of a variety of popular image processing algorithms to discriminate different forest types. Results indicate that certain algorithms are best suited to forest classification. Differences in performance between the algorithms tested appear related to variations in their sensitivities to spectral variations caused by background reflectance, differential illumination, and spatial pattern by species. Results emphasize the complexity between the land-cover regime, remotely sensed data and the algorithms used to process these data.
Yool, S. R.↗
SPECTRUM - A system for the analysis of imaging spectrometer data
This paper examines several design issues related to the development of SPECTRUM, a knowledge-based system for the geological interpretation of imaging spectrometer data. SPECTRUM is implemented using a combination of the programming languages STAR and C, which are coupled both at the level of procedures - involving function calls between the two languages - and at the level of data structures - involving the formation of a hybrid knowledge base shared by the two languages. Aspects of the coupling relating to each level of the implementation are described, followed by a listing of general observations regarding the coupling of symbolic and numerical techniques as extracted from the SPECTRUM project.
Borchardt, Gary C.↗
Software Graphical User Interface For Analysis Of Images
CAMTOOL software provides graphical interface between Sun Microsystems workstation and Eikonix Model 1412 digitizing camera system. Camera scans and digitizes images, halftones, reflectives, transmissives, rigid or flexible flat material, or three-dimensional objects. Users digitize images and select from three destinations: work-station display screen, magnetic-tape drive, or hard disk. Written in C.
Leonard, Desiree M.↗
Dosimetry of heavy ions by use of CCD detectors
The design and the atomic composition of Charge Coupled Devices (CCD's) make them unique for investigations of single energetic particle events. As detector system for ionizing particles they detect single particles with local resolution and near real time particle tracking. In combination with its properties as optical sensor, particle transversals of single particles are to be correlated to any objects attached to the light sensitive surface of the sensor by simple imaging of their shadow and subsequent image analysis of both, optical image and particle effects, observed in affected pixels. With biological objects it is possible for the first time to investigate effects of single heavy ions in tissue or extinguished organs of metabolizing (i.e. moving) systems with a local resolution better than 15 microns. Calibration data for particle detection in CCD's are presented for low energetic protons and heavy ions.
Schott, J. U.↗
Multi-Scale Fractal Analysis of Image Texture and Pattern
Fractals embody important ideas of self-similarity, in which the spatial behavior or appearance of a system is largely scale-independent. Self-similarity is a property of curves or surfaces where each part is indistinguishable from the whole. The fractal dimension D of remote sensing data yields quantitative insight on the spatial complexity and information content contained within these data. Analyses of Normalized Difference Vegetation Index (NDVI) images of homogeneous land covers near Huntsville, Alabama revealed that the fractal dimension of an image of an agricultural land cover indicates greater complexity as pixel size increases, a forested land cover gradually grows smoother, and an urban image remains roughly self-similar over the range of pixel sizes analyzed(l0 to 80 meters). The forested scene behaves as one would expect-larger pixel sizes decrease the complexity of the image as individual clumps of trees are averaged into larger blocks. The increased complexity of the agricultural image with increasing pixel size results from the loss of homogeneous groups of pixels in the large fields to mixed pixels composed of varying combinations of NDVI values that correspond to roads and vegetation. The same process occur's in the urban image to some extent, but the lack of large, homogeneous areas in the high resolution NDVI image means the initially high D value is maintained as pixel size increases. The slope of the fractal dimension-resolution relationship provides indications of how image classification or feature identification will be affected by changes in sensor resolution.
Emerson, Charles W.↗
Global Distribution of Dissected Duricrust on Mars
Evidence for dissected duricrust was identified in high resolution MOC images. Analysis of all available images was used to map the global distribution of this terrain. It is apparently restricted to two latitude bands: 30-60 deg. N and 30-60 deg. S.
Mustard, J. F.↗
Investigations into the Contamination of Lunar Return Material: Surface Analysis and Imaging Investigations - Part 1
A suite of lunar soils has been investigated by imaging and in-situ spectroscopy techniques. A suite of contaminant plastics and potential microbes has been found. Additional information is contained in the original extended abstract.
Steele, A.↗
Microstructural Evaluations of Baseline HSR/EPM Disk Alloys
Six alloys representing two classes of powder metallurgy nickel-based superalloys were examined by transmission electron microscopy (TEM) and phase extraction. Alloys KM4, CH98, IN-100 and 456 are based on a Ni-18Co-12Cr composition while alloys Rene' 88 DT and SR 3 have lower Al and Co and higher Cr contents. The lambda size distributions were determined from quantitative image analysis of the TEM images. The volume fraction of lambda and carbides and the composition of the phases were determined by a combination of phase extraction and TEM. The results showed many similarities in lambda size distributions, grain boundary serrations, and grain boundary carbide frequencies between alloys KM4, CH98, 456, Rene' 88 DT and SR 3 when heat treated to give an approximate grain size of ASTM 6. The density of grain boundary carbides in KM4 was shown to substantially increase as the grain size increased. IN-100 and 456 subjected to a serration cooling heat treatment had much more complex lambda size distributions with very large intergranular and intragranular secondary lambda as well as finer than average cooling and aging lambda. The grain boundary carbides in IN-100 were similar to the other alloys, but 456 given the serration cooling heat treatment had a more variable density of grain boundary carbides. Examination of the phases extracted from the matrix showed that there were significant differences in the phase chemistries and elemental partitioning ratios between the various alloys.
Gabb, Timothy P.↗