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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 379 records · Page 21
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Model-based approaches to calibration and certification of nondestructive assay systems - 15615

Increasingly, model-based methods founded in physics are employed to calibrate, or extend the calibration of, nondestructive assay (NDA) systems used to characterize materials contaminated with plutonium, uranium, and other radioactive isotopes. In addition, modeling and mathematical methods are used to establish system parameters, correction factors, and measurement uncertainty components in NDA measurements. The methods combine the characteristics of the measurement configuration (detector structure, object shape and dimensions, source-detector distance and orientation, and collimation), generator knowledge of the waste composition, and known physical properties of the system in order to establish these parameters, factors, and components. These methods offer several important benefits over traditional methods used to test, calibrate, operate, and certify radiation measurement systems. First, instruments can be set up and put into service more quickly and correctly using a model-based approach. Second, calibrations can be performed, tested, and modified with reduced use of plutonium and uranium standards when modeling and mathematical methods are employed. Also, modeled approaches avoid calibration error resulting from heterogeneous source distribution. Moreover, the parameters can be installed quickly and simply in an office setting without the need for the safety, security, and safeguards considerations that are present when standards are used. Calibrations can also be tailored to fit unique or nonstandard container configurations (for example, over-packed drums), new container types, or specialized matrices. Finally, when modeling methods are applied, correction factors and measurement uncertainty elements can be developed, tested, and validated relatively quickly and without the need for surrogate matrix materials and a large number of test measurements. A combined gamma and neutron NDA system has recently been moved from Idaho National Laboratory to the TA 55 facility at Los Alamos National Laboratory (LANL). The system will be used to assay transuranic waste packaged in drums. After the move, the system was modified to replace degraded components and improve system performance. Afterwards, it was set up to assay different container types and to extend the calibration range. Model-based approaches were used to adapt the system to its new purpose at LANL. This report will describe the setup, calibration, and certification of the combined system at LANL Included in this discussion will be the measurement applications and details of the measurement methods. The steps in these processes that involved the use of modeling and mathematical calculations to replace or supplement more traditional methods will be identified and discussed. Finally, an overarching discussion of the methods and advantages of model-based methods to establish the properties of NDA systems will be presented. We conclude that validated mathematical methods offer a robust, flexible, and mature approach which is technically defensible from first principle physics. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2020

Low Level Calibration of Liquid Scintillation Counting

Liquid Scintillation Counting (LSC) is an analytical laboratory method that quantifies the concentrations of alpha and beta emitting isotopes. The LSC method can be utilized for the detection of tritium, both environmentally and at nuclear facilities. Most LSC samples are aqueous-based and prepared as a radioactive sample dissolved or suspended in a high efficiency scintillation cocktail that converts radioactive energy into light pulses. When placed in counting vials, the liquid scintillation cocktail allows for optical coupling in which energy is released from the samples radioactive decay, and transferred to the scintillator. That energy is then absorbed to produce excited electrons that fall back to their ground-state and emit a pulse of light that is detected by the liquid scintillation analyzers photomultiplier tubes. Quench is a signal attenuation due to physical, chemical, or color interferences. To compensate for quench, quench standards of a known concentration are implemented at increasing increments of quench per vial to create a quench curve. Quench standards can be purchased pre-made or customized from the manufacturer, however, there are several issues that arise from purchasing the pre-made quench standards. The main issues with ordering pre-made quench standards is that they use higher count values, between 30,000 and 250,000 disintegrations per minute (dpm) of tritium per vial and only come in glass vials. Using higher counting standards in glass vials makes it hard to see lower concentrations in plastic vials. Additionally, when using higher energy standards the accuracy of the calibration readings tend to be lower. On the other hand, making a set of quench standards in-house allows for the customization of the dpm concentration to roughly 1,500-3,000 and preparation in plastic vials. This allows for lower activity readings that results in closer precision of the samples' true concentration. Technical Objectives: Create a quench curve and calibrate the LSA for tritium. Verify the calibration of the quench curve prior to cross sample runs. Check calibration against Quality Control (QC) reference value. Conclusion: a tritium quench curve calibration was performed using a scintillation cocktail with ultima gold (AB and AB/F), acetone (only with AB), and water (only with AB/F). By performing the tritium quench curve calibration, the counting efficiency was correlated to various levels of quench. Calibration checks with quality control standards were also performed to verify that the calibration was correct. The observed results provided acceptable values that matched the quality control standard reference values with an acceptable uncertainty. The next step will be fine tuning and cross comparison checks with legacy instrumentation.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2020

Calibration, measurement, and characterization of soil moisture dynamics in a central Amazonian tropical forest

Soil moisture plays a key role in hydrological, biogeochemical, and energy budgets of terrestrial ecosystems. Accurate soil moisture measurements in remote ecosystems such as the Amazon are difficult and limited because of logistical constraints. Time domain reflectometry (TDR) sensors are widely used to monitor soil moisture and require calibration to convert the TDR's dielectric permittivity measurement (K a ) to volumetric water content (θ v ). In this study, our objectives were to develop a field-based calibration of TDR sensors in an old-growth upland forest in the central Amazon, to evaluate the performance of the calibration, and then to apply the calibration to determine the dynamics of soil moisture content within a 14.2 -m-deep vertical soil profile. Depth-specific TDR calibration using local soils in a controlled laboratory setting yielded a novel K a –θ v third-degree polynomial calibration. The sensors were later installed to their specific calibration depth in a 14.2-m pit. The widely used K a –θ v relationship (Topp model) underestimated the site-specific θ v by 22–42%, indicating significant error in the model when applied to these well-structured, clay-rich tropical forest soils. The calibrated wet- and dry-season θ v data showed a variety of depth and temporal variations highlighting the importance of soil textural differentiation, root uptake depths, as well as event to seasonal precipitation effects. Data such as these are greatly needed for improving our understanding of ecohydrological processes within tropical forests and for improving models of these systems in the face of changing environmental conditions.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2014

Planck 2013 results. V. LFI calibration

We discuss the methods employed to photometrically calibrate the data acquired by the Low Frequency Instrument on Planck. Our calibration is based on a combination of the orbital dipole plus the solar dipole, caused respectively by the motion of the Planck spacecraft with respect to the Sun and by motion of the solar system with respect to the cosmic microwave background (CMB) rest frame. The latter provides a signal of a few mK with the same spectrum as the CMB anisotropies and is visible throughout the mission. In this data releasewe rely on the characterization of the solar dipole as measured by WMAP. We also present preliminary results (at 44 GHz only) on the study of the Orbital Dipole, which agree with the WMAP value of the solar system speed within our uncertainties. We compute the calibration constant for each radiometer roughly once per hour, in order to keep track of changes in the detectors’ gain. Since non-idealities in the optical response of the beams proved to be important, we implemented a fast convolution algorithm which considers the full beam response in estimating the signal generated by the dipole. Moreover, in order to further reduce the impact of residual systematics due to sidelobes, we estimated time variations in the calibration constant of the 30 GHz radiometers (the ones with the largest sidelobes) using the signal of an internal reference load at 4 K instead of the CMB dipole. We have estimated the accuracy of the LFI calibration following two strategies: (1) we have run a set of simulations to assess the impact of statistical errors and systematic effects in the instrument and in the calibration procedure; and (2) we have performed a number of internal consistency checks on the data and on the brightness temperature of Jupiter. Errors in the calibration of this Planck/LFI data release are expected to be about 0.6% at 44 and 70 GHz, and 0.8% at 30 GHz. Both these preliminary results at low and high ℓ are consistent with WMAP results within uncertainties and comparison of power spectra indicates good consistency in the absolute calibration with HFI (0.3%) and a 1.4σ discrepancy with WMAP (0.9%).

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2025

Validation of the ESPRESSO wavelength calibration using iodine absorption cell spectra

ABSTRACT High-quality wavelength calibration is crucial for science cases like radial-velocity studies of exoplanets, the search for a possible variation of fundamental constants, and the redshift drift experiment. However, for state-of-the-art spectrographs, it has become difficult to verify the wavelength calibration on sky because no astrophysical source provides spectra with sufficiently stable or accurate wavelength information. We therefore propose to use iodine absorption cells to validate the wavelength calibration. Observing a bright and featureless star through the iodine cell emulates an astrophysical target with exactly known spectral features that can be analysed like any other science target, allowing to verify the wavelength calibration derived from the internal calibration sources and to identify systematics in the data processing. As demonstration, we temporarily installed an $\mathrm{I_2}$ absorption cell at ESPRESSO. Employing a full forward modelling approach of the $\mathrm{I_2}$ spectrum, including the instrumental line-spread function, we demonstrate wavelength calibration accuracy at the level of a few $\mathrm{m\,s^{-1}}$. We also show that wavelength measurements do depend on the geometry of the light-injection into the spectrograph fibers. This highlights the importance of probing exactly the same light path as science targets, something not possible with internal calibration sources alone. We also demonstrate excellent radial-velocity stability at the ${{< 20\, \mathrm{cm\,s^{-1}}}}$ level in a full end-to-end fashion, from sky to data product. Our study therefore showcases the great potential of absorption cells for the verification and long-term monitoring of the wavelength calibration as well as the unique insights they can provide.

Schmidt, Tobias M. (ORCID:0000000248337273)↗
DOE OSTI2024

Automated Calibration of Parallel and Distributed Computing Simulators: A Case Study

Many parallel and distributed computing research results are obtained in simulation, using simulators that mimic real-world executions on some target system. Each such simulator is configured by picking values for parameters that define the behavior of the underlying simulation models it implements. The main concern for a simulator is accuracy: simulated behaviors should be as close as possible to those observed in the real-world target system. This requires that values for each of the simulator's parameters be carefully picked, or “calibrated,” based on ground-truth real-world executions. Examining the current state of the art shows that simulator calibration, at least in the field of parallel and distributed computing, is often undocumented (and thus perhaps often not performed) and, when documented, is described as a labor-intensive, manual process. In this work we evaluate the benefit of automating simulation calibration using simple algorithms. Specifically, we use a real-world case study from the field of High Energy Physics and compare automated calibration to calibration performed by a domain scientist. Our main finding is that automated calibration is on par with or significantly outperforms the calibration performed by the domain scientist. Furthermore, automated calibration makes it straightforward to operate desirable tradeoffs between simulation accuracy and simulation speed.

Mc donald, Jesse↗
DOE OSTI2022

Sequentially calibrating a Bayesian microsimulation model to incorporate new information and assumptions

Background: Microsimulation models are mathematical models that simulate event histories for individual members of a population. They are useful for policy decisions because they simulate a large number of individuals from an idealized population, with features that change over time, and the resulting event histories can be summarized to describe key population-level outcomes. Model calibration is the process of incorporating evidence into the model. Calibrated models can be used to make predictions about population trends in disease outcomes and effectiveness of interventions, but calibration can be challenging and computationally expensive. Methods: This paper develops a technique for sequentially updating models to take full advantage of earlier calibration results, to ultimately speed up the calibration process. A Bayesian approach to calibration is used because it combines different sources of evidence and enables uncertainty quantification which is appealing for decision-making. We develop this method in order to re-calibrate a microsimulation model for the natural history of colorectal cancer to include new targets that better inform the time from initiation of preclinical cancer to presentation with clinical cancer (sojourn time), because model exploration and validation revealed that more information was needed on sojourn time, and that the predicted percentage of patients with cancers detected via colonoscopy screening was too low. Results: The sequential approach to calibration was more efficient than recalibrating the model from scratch. Incorporating new information on the percentage of patients with cancers detected upon screening changed the estimated sojourn time parameters significantly, increasing the estimated mean sojourn time for cancers in the colon and rectum, providing results with more validity. Conclusions: A sequential approach to recalibration can be used to efficiently recalibrate a microsimulation model when new information becomes available that requires the original targets to be supplemented with additional targets.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2017

Experimentally Enhanced Computation (ExEC): Traditional Calibration of Anisotropic Yield Functions

This memo addresses the calibration of anisotropic yield functions based on data obtained from a series of uniaxial tension specimens extracted from a tubular Al 7079 circular cylindrical extrusion. Achieving the calibrations completed an important step in the Experimentally Enhanced Computations (ExEC) project. The focus of the project is on novel calibration approaches that will be based on advanced diagnostics and numerical simulations with the intention of reducing the overall calibration effort. The test data used here resulted from traditional tensile tests on specimens cut at 12 orientations within the extrusion. Two anisotropic yield surfaces — Hill’s (1948) and Barlat’s (2005) — were calibrated based on the test data. The methods used to conduct the calibrations are described, and the results show that the material exhibited significant yield anisotropy. The larger number of parameters in Barlat’s yield function allowed it to fit the test data more accurately than Hill’s. Although work remains to assess the sensitivity of the calibrated model parameters to various factors, the methods implemented and the results obtained here provide bases for further work and useful benchmarks for future calibrations to be conducted using the novel approach.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Forward Global Photometric Calibration of the Dark Energy Survey

Many scientific goals for the Dark Energy Survey (DES) require the calibration of optical/NIR broadband b = grizY photometry that is stable in time and uniform over the celestial sky to one percent or better. It is also necessary to limit to similar accuracy systematic uncertainty in the calibrated broadband magnitudes due to uncertainty in the spectrum of the source. Here we present a "Forward Global Calibration Method (FGCM)" for photometric calibration of the DES, and we present results of its application to the first three years of the survey (Y3A1). The FGCM combines data taken with auxiliary instrumentation at the observatory with data from the broadband survey imaging itself and models of the instrument and atmosphere to estimate the spatial and time dependences of the passbands of individual DES survey exposures. "Standard" passbands that are typical of the passbands encountered during the survey are chosen. The passband of any individual observation is combined with an estimate of the source spectral shape to yield a magnitude in the standard system. This "chromatic correction" to the standard system is necessary to achieve subpercent calibrations and in particular, to resolve ambiguity between the broadband brightness of a source and the shape of its SED. The FGCM achieves a reproducible and stable photometric calibration of standard magnitudes of stellar sources over the multiyear Y3A1 data sample with residual random calibration errors of per exposure. The accuracy of the calibration is uniform across the DES footprint to within . The systematic uncertainties of magnitudes in the standard system due to the spectra of sources are less than for main-sequence stars with .

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2016

Sky camera geometric calibration using solar observations

A camera model and associated automated calibration procedure for stationary daytime sky imaging cameras is presented. The specific modeling and calibration needs are motivated by remotely deployed cameras used to forecast solar power production where cameras point skyward and use 180° fisheye lenses. Sun position in the sky and on the image plane provides a simple and automated approach to calibration; special equipment or calibration patterns are not required. Sun position in the sky is modeled using a solar position algorithm (requiring latitude, longitude, altitude and time as inputs). Sun position on the image plane is detected using a simple image processing algorithm. The performance evaluation focuses on the calibration of a camera employing a fisheye lens with an equisolid angle projection, but the camera model is general enough to treat most fixed focal length, central, dioptric camera systems with a photo objective lens. Calibration errors scale with the noise level of the sun position measurement in the image plane, but the calibration is robust across a large range of noise in the sun position. In conclusion, calibration performance on clear days ranged from 0.94 to 1.24 pixels root mean square error.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2015

Hydrologic calibration of paired watersheds using a MOSUM approach

Paired watershed studies have historically been used to quantify hydrologic effects of land use and management practices by concurrently monitoring two neighboring watersheds (a control and a treatment) during the calibration (pre-treatment) and post-treatment periods. This study characterizes seasonal water table and flow response to rainfall during the calibration period and tests a change detection technique of moving sums of recursive residuals (MOSUM) to select calibration periods for each control-treatment watershed pair when the regression coefficients for daily water table elevation (WTE) were most stable to reduce regression model uncertainty. The control and treatment watersheds included 1–3 year intensively managed loblolly pine ( Pinus taeda L. ) with natural understory, same age loblolly pine intercropped with switchgrass ( Panicum virgatum ), 14–15 year thinned loblolly pine with natural understory (control), and switchgrass only. Although monitoring during the calibration period spanned 2009 to 2012, silvicultural operational practices that occurred during this period such as harvesting of existing stand and site preparation for pine and switchgrass establishment may have acted as external factors, potentially shifting hydrologic calibration relationships between control and treatment watersheds. Results indicated that MOSUM was able to detect significant changes in regression parameters for WTE due to silvicultural operations. This approach also minimized uncertainty of calibration relationships which could otherwise mask marginal treatment effects. All calibration relationships developed using this MOSUM method were quantifiable, strong, and consistent with Nash–Sutcliffe Efficiency (NSE) greater than 0.97 for WTE and NSE greater than 0.92 for daily flow, indicating its applicability for choosing calibration periods of paired watershed studies.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1986

Further investigation into calibration techniques for a magnetic suspension and balance system

Calibrations performed on three different magnetic cores for wind tunnel models suspended in the Southampton University Magnetic Suspension and Balance System (SUMSBS) are detailed. The first core investigated was the Southampton University pilot Superconducting Solenoid model, first flown in July 1983. Static calibrations of lift force, drag force and pitching moment, together with lift force and pitching moment calibrations determined by the dynamic method are detailed in this report. Other types of core investigated in a similar manner were conventional permanent magnets, Alnico and samarium-cobalt. All static calibrations gave a linear dependence of force on electromagnet current as expected. Dynamic calibrations are faster to perform but are proving to be not as easily analyzed as static calibrations. There are still some effects to be explained but dynamic lift calibration results were obtained agreeing to within 2 percent of the static calibration value.

Eskins, J.↗
NASA NTRS1989

Evaluating Statistical Process Control (SPC) techniques and computing the uncertainty of force calibrations

In recent years there has been a push within NASA to use statistical techniques to improve the quality of production. Two areas where statistics are used are in establishing product and process quality control of flight hardware and in evaluating the uncertainty of calibration of instruments. The Flight Systems Quality Engineering branch is responsible for developing and assuring the quality of all flight hardware; the statistical process control methods employed are reviewed and evaluated. The Measurement Standards and Calibration Laboratory performs the calibration of all instruments used on-site at JSC as well as those used by all off-site contractors. These calibrations must be performed in such a way as to be traceable to national standards maintained by the National Institute of Standards and Technology, and they must meet a four-to-one ratio of the instrument specifications to calibrating standard uncertainty. In some instances this ratio is not met, and in these cases it is desirable to compute the exact uncertainty of the calibration and determine ways of reducing it. A particular example where this problem is encountered is with a machine which does automatic calibrations of force. The process of force calibration using the United Force Machine is described in detail. The sources of error are identified and quantified when possible. Suggestions for improvement are made.

Navard, Sharon E.↗
NASA NTRS1992

Ground and flight calibration assessment of HiRAP accelerometer data from missions STS-35 and STS-40

A method of removing non-aerodynamic signals and calibrating the High Resolution Accelerometer Package (HiRAP) flight data was developed and is discussed for Shuttle Orbiter missions STS-35 and STS-40. These two mission data sets were analyzed using ground (dynamic) calibration data and flight calibrations using a flight calibration technique that was developed and refined over the HiRAP operational lifetime. This technique evolved early in the flight program, since it was recognized that ground calibration factors are insufficient to determine absolute low acceleration levels. The application of flight calibration factors to the data sets from these missions produced calibrated acceleration levels within an accuracy of less than plus or minus 1.5 micro-g of zero during a time in the flight when the acceleration level was known to be less than 1 micro-g. This analysis further confirms the theory that flight calibrations are required in order to obtain the absolute measurement of low-frequency, low-acceleration flight signals.

Blanchard, Robert C.↗
NASA NTRS1992

COBE differential microwave radiometers - Calibration techniques

The COBE spacecraft was launched November 18, 1989 UT carrying three scientific instruments into earth orbit for studies of cosmology. One of these instruments, the Differential Microwave Radiometer (DMR), is designed to measure the large-angular-scale temperature anisotropy of the cosmic microwave background radiation at three frequencies (31.5, 53, and 90 GHz). This paper presents three methods used to calibrate the DMR. First, the signal difference between beam-filling hot and cold targets observed on the ground provides a primary calibration that is transferred to space by noise sources internal to the instrument. Second, the moon is used in flight as an external calibration source. Third, the signal arising from the Doppler effect due to the earth's motion around the barycenter of the solar system is used as an external calibration source. Preliminary analysis of the external source calibration techniques confirms the accuracy of the currently more precise ground-based calibration. Assuming the noise source behavior did not change from the ground-based calibration to flight, a 0.1-0.4 percent relative and 0.7-2.5 percent absolute calibration uncertainty is derived, depending on radiometer channel.

Bennett, C. L.↗
NASA NTRS1992

Calibration of the ARID robot

The author has formulated a new, general model for specifying the kinematic properties of serial manipulators. The new model kinematic parameters do not suffer discontinuities when nominally parallel adjacent axes deviate from exact parallelism. From this new theory the author develops a first-order, lumped-parameter, calibration-model for the ARID manipulator. Next, the author develops a calibration methodology for the ARID based on visual and acoustic sensing. A sensor platform, consisting of a camera and four sonars attached to the ARID end frame, performs calibration measurements. A calibration measurement consists of processing one visual frame of an accurately placed calibration image and recording four acoustic range measurements. A minimum of two measurement protocols determine the kinematics calibration-model of the ARID for a particular region: assuming the joint displacements are accurately measured, the calibration surface is planar, and the kinematic parameters do not vary rapidly in the region. No theoretical or practical limitations appear to contra-indicate the feasibility of the calibration method developed here.

Doty, Keith L↗
NASA NTRS1993

Goddard Space Flight Center (GSFC) Flight Dynamics Facility (FDF) calibration of the Upper Atmosphere Research Satellite (UARS) sensors

Flight Dynamics Facility (FDF) responsibilities for calibration of Upper Atmosphere Research Satellite (UARS) sensors included alignment calibration of the fixed-head star trackers (FHST's) and the fine Sun sensor (FSS), determination of misalignments and scale factors for the inertial reference units (IRU's), determination of biases for the three-axis magnetometers (TAM's) and Earth sensor assemblies (ESA's), determination of gimbal misalignments of the Solar/Stellar Pointing Platform (SSPP), and field-of-view calibration for the FSS's mounted both on the Modular Attitude Control System (MACS) and on the SSPP. The calibrations, which used a combination of new and established algorithms, gave excellent results. Alignment calibration results markedly improved the accuracy of both ground and onboard Computer (OBC) attitude determination. SSPP calibration results allowed UARS to identify stars in the period immediately after yaw maneuvers, removing the delay required for the OBC to reacquire its fine pointing attitude mode. SSPP calibration considerably improved the pointing accuracy of the attached science instrument package. This paper presents a summary of the methods used and the results of all FDF UARS sensor calibration.

Hashmall, J.↗
NASA NTRS1993

Cross-calibration between airborne SAR sensors

As Synthetic Aperture Radar (SAR) system performance and experience in SAR signature evaluation increase, quantitative analysis becomes more and more important. Such analyses require an absolute radiometric calibration of the complete SAR system. To keep the expenditure on calibration of future multichannel and multisensor remote sensing systems (e.g., X-SAR/SIR-C) within a tolerable level, data from different tracks and different sensors (channels) must be cross calibrated. The 1989 joint E-SAR/DC-8 SAR calibration campaign gave a first opportunity for such an experiment, including cross sensor and cross track calibration. A basic requirement for successful cross calibration is the stability of the SAR systems. The calibration parameters derived from different tracks and the polarimetric properties of the uncalibrated data are used to describe this stability. Quality criteria for a successful cross calibration are the agreement of alpha degree values and the consistency of radar cross sections of equally sized corner reflectors. Channel imbalance and cross talk provide additional quality in case of the polarimetric DC-8 SAR.

Zink, Manfred↗