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DOE OSTI2025

LDRD conclusion poster - Synthesizing Heterometallic Uranium Single Crystals to Understand the Influence of the Secondary Metals on Uranyl Axial Bond Strength

Understanding how transition metals influenced the chemistry of lanthanide and actinide (f-element) materials is critical for advancing separation technologies, materials design, and coordination chemistry. This project examined how incorporating first-row transition metals affected the structural and spectroscopic properties of f-element coordination polymers. In uranium(VI)-based systems synthesized with 2,6-pyridinedicarboxylic acid (PDC) ligands, single-crystal X-ray diffraction and Raman spectroscopy revealed that the presence of transition metals shortened the uranyl axial bond and induced a blue shift in its symmetric stretching vibration—evidence of increased bond strength. Electronic structure analysis, including Density of States (DOS) calculations using density functional theory (DFT), revealed altered orbital overlaps and highlighted the role of transition metal d-orbitals in modulating bonding. Raman modes were modeled using truncated structural fragments in collaboration with the University of Notre Dame, and although the predicted frequencies were lower than experimental values, they remained within expected ranges. In parallel, similar experiments with cerium (Ce) in the presence of cobalt (Co) and PDC demonstrated multi-step single-crystal-to-single-crystal transformations—behavior not observed in the uranium systems. Initial products included light yellow, orange, and polycrystalline materials. Single-crystal X-ray diffraction studies, conducted in collaboration with the Colorado School of Mines, identified the yellow phase as monometallic Ce(PDC)2(H2O)2·4H2O and the orange phase as heterometallic Ce2Co(PDC)4(H2O)6. After standing in solution for one week, both phases fully transformed into a dark yellow crystalline phase, [Ce3(PDC)5(H2O)8].6(H2O). Remarkably, this transformation was reversible—disturbing the equilibrium by removing some crystals caused reversion to the initial Ce(PDC)2(H2O)2·4H2O phase, highlighting dynamic behavior. All three structures were previously unreported. Solid-state UV-visible and Raman spectroscopy further distinguished these phases, revealing ligand-to-metal charge transfer involving Ce and characteristic d–d transitions from Co(II). The precise mechanism driving these transformations remained unclear; however, pH-dependent experiments confirmed that the transformation did not occur when the pH decreased. Overall, the project demonstrated that transition metals could be employed to tune bonding interactions, structural dimensionality, and optical properties in f-element materials, establishing new pathways for designing functional heterometallic systems. The work resulted in several novel structural discoveries and fostered productive collaborations with the University of Notre Dame and the Colorado School of Mines.

37 - INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL C↗

DOE OSTI2024

Occupancy schedule development and its effect on OpenStudio prototype college building model

College buildings have unique characteristics compared with school buildings. Therefore, defining the realistic occupancy schedule in a prototype college building has significant research opportunities. In this study, the actual operating schedules of each space type were collected and generated based on the class reservation schedule and compared with the previous reference schedule (primary/secondary school). Here, the schedules were analyzed for their effect on the OpenStudio prototype college building model. The findings highlight that the use of a typical school building schedule in a college building impairs the granularity of information. The analysis shows significant differences between the previous occupancy schedule and the updated occupancy schedule of the college building, leading to a considerable decrease in occupancy density. Furthermore, the effect of these occupancy pattern changes on the prototype building model is examined. The variations were observed in minimum ventilation requirements, the average mechanical ventilation rate, and energy consumption attributed to changes in occupancy density.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

DOE OSTI2023

Bridging Place-Based Astrobiology Education with Genomics, Including Descriptions of Three Novel Bacterial Species Isolated from Mars Analog Sites of Cultural Relevance

Democratizing genomic data science, including bioinformatics, can diversify the STEM workforce and may, in turn, bring new perspectives into the space sciences. In this respect, the development of education and research programs that bridge genome science with “place” and world-views specific to a given region are valuable for Indigenous students and educators. Through a multi-institutional collaboration, we developed an ongoing education program and model that includes Illumina and Oxford Nanopore sequencing, free bioinformatic platforms, and teacher training workshops to address our research and education goals through a place-based science education lens. High school students and researchers cultivated, sequenced, assembled, and annotated the genomes of 13 bacteria from Mars analog sites with cultural relevance, 10 of which were novel species. Students, teachers, and community members assisted with the discovery of new, potentially chemolithotrophic bacteria relevant to astrobiology. This joint education-research program also led to the discovery of species from Mars analog sites capable of producing N-acyl homoserine lactones, which are quorum-sensing molecules used in bacterial communication. Whole genome sequencing was completed in high school classrooms, and connected students to funded space research, increased research output, and provided culturally relevant, place-based science education, with participants naming three novel species described here. Students at St. Andrew's School (Honolulu, Hawai‘i) proposed the name Bradyrhizobium prioritasuperba for the type strain, BL16A T , of the new species (DSM 112479 T = NCTC 14602 T ). The nonprofit organization Kauluakalana proposed the name Brenneria ulupoensis for the type strain, K61 T , of the new species (DSM 116657 T = LMG = 33184 T ), and Hawai‘i Baptist Academy students proposed the name Paraflavitalea speifideiaquila for the type strain, BL16E T , of the new species (DSM 112478 T = NCTC 14603 T ).

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2020

New Frontiers in Geoengineering Research

In late summer 2019, the ninth annual workshop of the Geoengineering Model Intercomparison Project (GeoMIP; http://climate.envsci.rutgers.edu/GeoMIP) convened at Beijing Normal University (Fig. 1). This meeting was held in conjunction with a summer school in which 89 participants from five continents learned about climate modeling of solar geoengineering, also known as climate engineering or climate intervention. Solar geoengineering refers to “radiation management” methods, which involve deliberate manipulations of the radiation budget through potential technologies such as stratospheric sulfate aerosols, marine cloud brightening, and cirrus thinning, but not CO2 removal. The students at the summer school were mainly physical science majors, with many from China, but also included some social science people. The summer school was focused on impact modeling (e.g., on agriculture and the cryosphere) and consideration of extremes, rather than just looking at climate modeloutput. There were also lectures on governance and economics. This event signifies the first major international geoengineering meeting held in Asia.

Kravitz, Benjamin S.↗

DOE OSTI2021

Technology assessment to reduce aerosol transmission risk in naturally ventilated K12 classrooms (CRADA Final Report)

LBNL provided technical assistance to Oakland Unified School District (OUSD) through this project in their selection of technologies to support in-person instruction. OUSD considered different technologies to mitigate the aerosol transmission risks of COVID-19: a) Upgrade to higher efficiency air filters in buildings that are served by heating, ventilation, and air conditioning (HVAC) systems. b) Install portable air cleaners with HEPA (high efficiency particulate air) filters. c) Install ultraviolet germicidal irradiation (UVGI) systems. d) Install bipolar ionization air cleaning systems. LBNL met with OUSD facilities staff to discuss the pros and cons of options a) and c), and cited the lack of proven data on efficacy and discouraged option d). LBNL provided practical guidance on how to select portable air cleaners for classrooms. LBNL met with the boarder school communities to explain OUSD approach to ventilation and filtration, and produced FAQs to answer their questions about the science behind the selected approaches. In addition, LBNL helped OUSD facilities staff to acquire five indoor air quality (IAQ) monitors (AirVisual Pro by IQAir) for measuring carbon dioxide (CO2) and particulate matter (PM) concentrations. These monitors were installed in an elementary school in West Oakland.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2026

SUSY 2025 at UC Santa Cruz (Final Technical Report)

The 32nd International Conference on Supersymmetry and the Unification of Fundamental Interactions (SUSY 2025) took place from August 18--23, 2025. During the week preceding the SUSY 2025 conference, the associated pre-SUSY school took place from August 11--15, 2025. Both events were organized and hosted by the Santa Cruz Institute for Particle Physics at the University of California, Santa Cruz. The SUSY 2025 conference brought together theorists and experimentalists specializing in particle physics, astroparticle physics, cosmology, mathematical physics, and string theory to discuss recent developments in these areas, with a focus on theoretical aspects and experimental searches associated with phenomena that lie beyond the Standard Model of particle physics and the standard mathematical framework of modern cosmology. The pre-SUSY school provided advanced pedagogical lectures for graduate students and early-career postdoctoral researchers on many of the foundational topics that were subsequently addressed in the main SUSY 2025 conference that followed. DOE support helped increase accessibility for early-career scientists by covering conference support costs that enabled free participation in the pre-SUSY school and substantially reduced registration fees for students attending the conference.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2022

Likeness: a toolkit for connecting the social fabric of place to human dynamics

The ability to produce richly-attributed synthetic populations is key for understanding human dynamics, responding to emergencies, and preparing for future events, all while protecting individual privacy. The Likeness toolkit accomplishes these goals with a suite of Python packages: pymedm/pymedm\_legacy, livelike, and actlike. This production process is initialized in pymedm (or pymedm\_legacy) that utilizes census microdata records as the foundation on which disaggregated spatial allocation matrices are built. The next step, performed by livelike, is the generation of a fully autonomous agent population attributed with hundreds of demographic census variables. The agent population synthesized in livelike is then attributed with residential coordinates in actlike based on block assignment and, finally, allocated to an optimal daytime activity location via the street network. We present a case study in Knox County, Tennessee, synthesizing 30 populations of public K–12 school students \& teachers and allocating them to schools. Validation of our results shows they are highly promising by replicating reported school enrollment and teacher capacity with a high degree of fidelity.

Tuccillo, Joe↗

NASA NTRS1971

Computer program for the automated attendance accounting system

The automated attendance accounting system (AAAS) was developed under the auspices of the Space Technology Applications Program. The task is basically the adaptation of a small digital computer, coupled with specially developed pushbutton terminals located in school classrooms and offices for the purpose of taking daily attendance, maintaining complete attendance records, and producing partial and summary reports. Especially developed for high schools, the system is intended to relieve both teachers and office personnel from the time-consuming and dreary task of recording and analyzing the myriad classroom attendance data collected throughout the semester. In addition, since many school district budgets are related to student attendance, the increase in accounting accuracy is expected to augment district income. A major component of this system is the real-time AAAS software system, which is described.

Poulson, P.↗

NASA NTRS1977

NASA Space Sciences Symposium-1977

The primary objective of the symposium was to motivate American Indians and other minority youths and women to select science and engineering as viable career choices, thereby making them available to the technical work force. Other objectives were: (1) to determine how aerospace technology careers and aerospace activities can be made more relevant to minorities and women; (2) to provide an opportunity for key NASA officials to interact with teachers and counselors of the participating schools; (3) to stimulate a greater interest among American Indian organizations and students in NASA's research and development programs; (4) to help NASA's efforts in the recruiting of minorities and women into its work force; and (5) to provide opportunities for minority aerospace scientists and engineers to interact with the minority community, particularly with youths at the junior high school and high school levels.

Source record↗

NASA NTRS1977

The MINE project: Minority Involvement in NASA Engineering

The Mine Project developed by Lewis Research Center (LRC) along with Tennessee State University and Tuskegee Institute, is described. The project calls for LRC to assemble on-going NASA university affairs programs aimed at benefiting the school, its faculty, and its student body. The schools receive grants to pursue research and technology projects that are relevant to NASA's missions. Upon request from the universities, LRC furnishes instructors and lecturers. The schools have use of surplus government equipment and access to NASA research facilities for certain projects. Both the faculty and students of the universities are eligible for summer employment at LRC through special programs. The MINE Project is designed to establish a continuing active relationship of 3 to 5 years between NASA and the universities, and will afford LRC with an opportunity to increase its recruitment of minority and women employees.

Allen, H., Jr.↗

NASA NTRS1984

Caribbean tectonics and relative plate motions

During the last century, three different ways of interpreting the tectonic evolution of the Gulf of Mexico and the Caribbean have been proposed, taking into account the Bailey Willis School of a permanent pre-Jurassic deep sea basin, the Edward Suess School of a subsided continental terrain, and the Alfred Wegener School of continental separation. The present investigation is concerned with an outline of an interpretation which follows that of Pindell and Dewey (1982). An attempt is made to point out ways in which the advanced hypotheses can be tested. The fit of Africa, North America, and South America is considered along with aspects of relative motion between North and South America since the early Jurasic. Attention is given to a framework for reconstructing Caribbean plate evolution, the evolution of the Caribbean, the plate boundary zones of the northern and southern Caribbean, and the active deformation of the Caribbean plate.

Burke, K.↗

NASA NTRS1985

To catch a comet: Technical overview of CAN DO G-324

The primary photographing of aboard STS 61-E. INTRODUCTION objective of the C.E. Williams Middle School Get Away Special "CAN DO" is the Comet Halley. As it is currently scheduled, G-324 will fly in March of 1986 The project will involve middle school students, grades 6 through 8, in the study and interpretation of astronomical photographs and techniques. -The-objectives of these studies are detailed in another paper to be presented at this symposium. 6-324 is contained in a 5 cubic foot G.A.S. Canister with an opening door and pyrex window for photography. It will be pressurized with one atmosphere of dry nitrogen. Three 35mm still cameras with 250 exposure film backs and different focal length lenses will be fired by a combination of automatic timer and an active comet detector. A lightweight 35mm movie camera will shoot single exposures at about 4 minute intervals to give an overlapping "skymap" of the mission. The fifth camera is a solid state television camera specially constructed for detection of the comet by the microprocessor. In addition to the photographic goals of CAN DO, the canister also contains a separate package of middle school student designed passive experiments. These-projects will be described in detail in the accompanying paper on educational goals.

Thomas J. O'Brien↗

NASA NTRS1992

The continuous plankton recorder survey: A long-term, basin-scale oceanic time series

In the 1920s, before the advent of echo sounders, fishery biologists were greatly concerned with assisting the fisherman to locate schools of pelagic fish. One of the approaches they developed was to relate the distribution of the planktonic food organisms to the presence of the schools of predators such as herring (Clupea harengus). The British planktologist, Alister Hardy, who had already carried out extensive studies on the feeding preferences of herring (Hardy, 1926a), initiated a program to examine the fishermen's contention that herring schools avoided 'green', i.e., phytoplankton-rich, water but could be correlated with high concentrations of zooplankton. This practical program was centered on the use of a specially developed instrument, the 'Plankton Indicator', designed to be used by the fisherman to assist in the search for suitable waters. It had limited success in its main aim but, as a collecting device, it embodied several profoundly important features. It was a simple instrument which was robust enough to be deployed and recovered by the crew of commercial vessels (in this case fishing vessels) while they were underway. The Indicator however, was no more than a high speed net which integrated the plankton over the area of sampling, but Hardy had also become interested in describing the patchiness of planktonic populations. He thus developed the Continuous Plankton Recorder (CPR) where he substituted the fixed filter screen of the Indicator by a continually moving length of silk mesh. The screen traversed at constant speed across the path of the incoming water and the trapped organisms were retained in place by sandwiching beneath an additional second mesh screen. Thus, knowing the speed of the towing vessel and the shooting and hauling positions, the spatial patterns of the plankton could be determined. Hardy took the first CPR to the Antarctic where he used it in the Southern Atlantic (Hardy, 1926b) and later deployed it in the North Sea to make some of the earliest contiguous records of plankton patchiness.

Gamble, John C.↗

NASA NTRS1992

Propellant production and useful materials: Hardware data from components and the systems

During the past year significant progress included: a major breakthrough in oxygen production through discs (instead of tubes) that resulted in two orders-of-magnitude increase in the yield rates, proving that oxygen production from any iron-bearing silicate (avoiding costly beneficiation) in lunar in-situ resource utilization (ISRU); construction of a half-scale robotic soil processor; production of melt-spun fibers in a solar furnace; and the culmination of first-stage research in the construction (and delivery to NASA LaRC) of a self-contained portable oxygen plant that incorporates the first generation ISRU technologies developed at UA SERC. In addition, further reductions in mass and power needs were achieved in two smaller oxygen plants, which, however, have far greater production rates. SERC continued to attract bright students both at the undergraduate and graduate levels, and several area high school students through the Professional Internship Program (PIP) administered by the local school district. Invited lectures at elementary schools continue to draw enthusiastic response. Another important first was the creation of the Freshman Colloquium, 'Space in Our Future, and Our Future in Space,' geared toward women and minority students. This course proved to be a success, with more than one-half of the enrollment composed of women. In recognition of these important contributions, the author was appointed to the NRC Committee on Space Science Technologies.

Ramohalli, Kumar↗

NASA NTRS1996

Investigation of the High Latitude Magnetosphere and its Response to the Solar Wind

INSPIRE is a non-profit scientific, educational corporation whose objective is to bring the excitement of observing natural and manmade radio waves in the audio region to high school students. Stimulating students to learn and understand science and technology is the key to them fulfilling their potential in the best interests of our society. INSPIRE also is an innovative, unique opportunity for students to actively gather data that might be used in a basic research project. INSPIRE began with a test bed project, ACTIVE/HSGS, which involved 100 high schools, with a centerpiece of making observations of 10.5 kHz transmissions from the Soviet ACTIVE satellite. A large number of ground receiving sites was needed, both to enhance the probability of receiving the radio waves from ACTIVE, and to determine the propagation paths to the ground. The second major project was support to SEPAC (Space Experiments using Particle ACcelerators), a payload on the ATLAS I Spacelab mission, flown in March/April 1992. With its electron accelerator SEPAC performed many experiments in the ionosphere, including producing an artificial aurora and the electromagnetic waves produced by pulsing the electron beam. INSPIRE/SEPAC provided more than 1000 ground stations to receive the radio waves, and, at the same time, allowed high school students the opportunity to take data that would be used in a published basic research project. The third major project is to make observations of the effects of a pulsed electron beam and plasma generator on the MIR Space Station. On request, these instruments are operated over INSPIRE observers.

Taylor, William W. L.↗

NASA NTRS1995

Three two-week enhancement institutes: Design and implementation of the technology and telecomputing component

The Teacher Enhancement Institute (TEI), under the direction of the Center Education Programs Officer offered three two-week workshops to 58 elementary and middle school teachers in science, math, and technology using the Problem Based Learning Model. The 1995 program was designed with input from evaluations and recommendations from previous TEI participants and faculty. The TEI focused on Aviation and Aeronautics as the unifying theme. Four specific objectives were developed. After completing the requirements for the TEI, the participants should be able to: (1) Increase their content knowledge, particularly in aeronautics, science, math, and technology; (2) Design and implement lessons that use scientific inquiry through Problem Based Learning; (3) Demonstrate knowledge of instructional technologies, their uses, and applications to curricula; and (4) Disseminate to their school communities the information acquired through the TEI. Thirty percent of the program was devoted to the effective use of computer technology. SpaceLink, the NASA telecomputing service for educators, was the primary tool used in the technology component of the institute. The training focused on the use of SpaceLink and its many educational services, and Internet tools because of its universal, nongraphical link to any computer plafform the participant may use at his or her school or home. All participants were given Educator Accounts to facilitate the use of E-mail, and access to the Internet and the World Wide Web using their SpaceLink accounts. Classroom demonstrations used videotaped guides and handouts to support concepts presented followed by intensive hands-on activities. Each participant was assigned to an individual Power Mac networked workstation and introduced to the state of the art, graphical, Word Wide Web with the Netscape browser. The methodology proved very effective in reaching the program's goals for technology integration by having the participants learn to use the computer as a tool for communication and research rather than teaching the use of any particular software application alone. However, because of the skill level of the majority of the participants, more hands-on computer time is recommended for future Teacher Enhancement Institutes.

Hale, L. Vincent↗

NASA NTRS1997

Education and Training Report. Performance Report, FY 1997

During FY 97, 152 MUREP education and training projects were conducted at OMU institutions. The institutions conducted precollege and bridge programs, education partnerships with other universities and industry, NRTS, teacher training, and graduate and/or PI undergraduate programs. These programs reached a total of 23,748 participants, with the predominant number at the precollege level and achieved major goals of heightening students' interest and awareness of career opportunities in MSET fields, and exposing students to the NASA mission, research and advanced technology through role models, mentors, and participation in research and other educational activities. Also in FY 1997, NASA continued a very meaningful relationship with the Hispanic Association of Colleges students and Universities (HACU) through Proyecto Access, a consortium through which HACU links seven HSI's together to conduct 8-week summer programs. OMU Institutions reported 4,334 high school student in NASA programs and 3,404 of those students selected college preparatory MSET courses. Three hundred and forty-nine (349) graduated from high school, 343 enrolled in college, and 199 selected MSET majors. There were 130 high school graduates (bridge students) in NASA programs, 57 of whom successfully completed their freshman year. There were 307 teachers in teacher programs and 48 teachers received certificates. Of the 389 undergraduate students, 75 received under graduate degrees, and eight students are employed in a NASA-related field.

Source record↗

NASA NTRS1996

The Chemistry of Early Self-Replicating Systems

The NASA Specialized Center of Research and Training (NSCORT) in Exobiology is a consortium of scientists at the University of California at San Diego (UCSD), The Salk Institute for Biological Studies (Salk) and The Scripps Research Institute (TSRI). All three institutions are located in close geographical proximity in La Jolla, California. The NSCORT/Exobiology is administered through the Scripps Institution of Oceanography. Since its inception in January 1992, the NSCORT in Exobiology has made major contributions with respect to the question of how life began on Earth. The Principal Investigators (PIs) and their associated Fellows have published numerous articles in peer reviewed journals on topics relevant to Exobiology. They have presented papers and sponsored symposia at several meetings of national and international scientific societies. A total of 30 undergraduate, 12 graduate and 15 postdoctoral Fellows have been supported by the NSCORT. The Fellows have met on their own at least once a month to discuss Exobiology topics and research progress. The NSCORT has arranged seminars and evening discussion meetings, and offered an undergraduate class on "Biochemical Evolution" as well as graduate courses dealing with topics in Exobiology. A visiting scientist program has allowed 11 scientists from the U.S. and 4 foreign countries to conduct cooperative research with the various PIs. An active outreach program has been initiated, which includes an Exobiology high school level teaching module and curriculum guide, and an elementary school level booklet about basic atomic structure and formation of the universe, Sun and Earth. A World Wide Web Homepage (http://www-chem.ucsd.edu/-nscort/ NSCORT.html) has been developed, which describes the NSCORT activities, research programs and Fellowship opportunities. The various activities of the NSCORT in Exobiology have received wide-spread coverage in both the scientific and public media. The major function of the NSCORT is the training of young scientists in the field of Exo- biology. Thus, the bulk of the $1,000,000 annual budget is used to support the research and training of undergraduate, graduate and post-doctoral Fellows who are selected on a competitive basis. About five Fellows at each level are supported each year. Our goal is to train scientists whose major research interest is Exobiology, but whose mastery in the classical fields of chemistry, biology and earth science is so strong that they outstanding candidates for either graduate school or academic tenure-track positions in departments at leading national and international Universities. Applicants for these Fellowships are solicited by advertisements in journals such as Science and Nature and in organizational newsletters such as the one published by the International Society for the Study of the Origin of Life (ISSOL), by contacting academic and NASA colleagues working in Exobiology or related fields and by recruiting students who have already been admitted into the various academic programs with which the PIs are affiliated.

Bada, Jeffrey L.↗